• Title/Summary/Keyword: 최적선정

Search Result 3,152, Processing Time 0.037 seconds

Isolation and HPLC-DAD validation of xanthoangelol in Lespedeza bicolor extract (싸리나무 추출물의 Xanthoangelol 분리 및 HPLC-DAD 밸리데이션)

  • Woo, Hyun Sim;Kim, Yeong-Su;Oh, Yu Jin;Cho, Hae Jin;Song, Se-Kyu;Kim, Dae Wook
    • Korean Journal of Food Science and Technology
    • /
    • v.52 no.1
    • /
    • pp.26-30
    • /
    • 2020
  • This study was undertaken to determine the characteristics of xanthoangelol, the major chalcone constituent derived from the extracts of different parts of Lespedeza bicolor. Xanthoangelol was isolated from the root extract using column chromatography and used as a standard for quantitative analysis. The structure of the isolated compound was established based on spectroscopic evidence. The HPLC-DAD method was validated for specificity, linearity, precision, accuracy, limit of detection, and limit of quantitation. The calibration curve of xanthoangelol had significant linearity (R2>0.9999). Limit of detection and limit of quantitation 0.018 and 0.059 ㎍/mL, respectively. The relative standard deviation values of precision test, and intra- and inter-day tests were less than 0.22 and 0.40%, respectively. In the recovery test, the accuracy ranged from 98.98-102.78% with RSD values less than 0.13%. The method validation parameters indicate the applicability of the HPLC method for quality control of food or drug formulations containing L. bicolor.

An Application of Design of Experiments for Optimization of MOF-235 Synthesis for Acetylene Adsorption Process (아세틸렌 흡착공정용 MOF-235 합성 최적화를 위한 실험 계획법 적용)

  • Cho, Hyungmin;Yoo, Kye Sang
    • Applied Chemistry for Engineering
    • /
    • v.31 no.4
    • /
    • pp.377-382
    • /
    • 2020
  • A sequential design of experiments was employed to optimize MOF-235 synthesis for acetylene adsorption process. Two experimental designs were applied: a two-level factorial design for screening and a central composite design, one of response surface methodologies (RSM). In this study, 23 factorial design of experiment was used to evaluate the effect of parameters of synthesis temperature and time, and also mixing speed on crystallinity of MOF-235. Experiments were conducted 16 times follwing MINITAB 19 design software for MOF-235 synthesis. Half-normal, pareto, residual, main and interaction effects were drawn based on the XRD results. The analysis of variance (ANOVA) of test results depicts that the synthesis temperature and time have significant effects on the crystallinity of MOF-235 (response variable). After screening, a central composite design was performed to optimize the acetylene adsorption capacity of MOF-235 based on synthesis conditions. From nine runs designed by MINITAB 19, the result was calculated using the second order model equation. It was estimated that the maximum adsorption capacity (18.7 mmol/g) was observed for MOF-235 synthesized at optimum conditions of 86.3 ℃ and 28.7 h.

Field Applicability Evaluation of SB Latex-Modified Concrete for Concrete Bridge Deck Overlay (콘크리트 교면 덧씌우기를 위한 SB 라텍스개질 콘크리트의 현장적용성 평가)

  • Yun, Kyong-Ku;Lee, Joo-Hyung;Hong, Chang-Woo;Kim, Ki-Hyun;Kim, Tae-Kyong
    • International Journal of Highway Engineering
    • /
    • v.3 no.4 s.10
    • /
    • pp.93-103
    • /
    • 2001
  • This study focused on the field applicability evaluation of SB latex-modified concrete (LMC) for concrete bridge deck overlay using mobile mixer. The main experimental factors were water-cement ratio(31, 33, 35 37%), latex contents(0, 5, 10, 15, 20%), and fine aggregate ratio(55, 56, 57, 58%) in order to evaluate the workability, mechanical properties, and durability property of LMC. The slump loss, air content, compressive and flexible strength tests were used to evaluate LMC workability and strength properties. Also, the rapid chloride permeability test was used to evaluate the relative permeability of LMC. As a results, the LMC with enough workability and good quality was produced when it was mixed in field using mobile mixer, satisfying the target compressive strength and flexural strength. The required water-cement ratio of LMC for same workability when mixing with mobile mixer was less than that when mixing in laboratory. Increasing the amount of latex produced concrete with increased flexural strength by mobile mixer. The required cement-water ratios for same initial $19{\pm}3cm$ slump were 37% and 33% at laboratory and mobile mixer, respectively. The mobile mixer was accurately calibrated satisfying the required specification.

  • PDF

A Study on the Optimal Installation of Ducted Fan Ventilation System in Long Mine Airways - Focused on the Wall Separation Distance and the Gap Length between Ducts (장대 광산갱도내 풍관 접속 통기선풍기 최적 설치 방안연구 - 벽면과 풍관간의 이격거리 중심으로)

  • Lee, Chang Woo;Nguyen, Van Duc
    • Tunnel and Underground Space
    • /
    • v.27 no.1
    • /
    • pp.12-25
    • /
    • 2017
  • In local underground mines heavily depending on the natural ventilation, ducted fan auxiliary ventilation system is strongly recommended instead of the total mine ventilation system requiring large capital and operating costs. Optimizing the installation of ducted fans in series in long large-opening mines is required to assure the economy and efficiency of the ventilation system. The two most critical design parameters for optimization are the wall separation distance and gap length between adjoining ducts. This study aims at deriving the optimal values for those two parameters concerning the economic and environmental aspects through the extensive CFD analysis, which minimizes pressure loss, leakage and entrainment of the contaminated air in the gap space. The ranges of the wall separation distance and gap length for study are selected by taking into consideration the existing recommendations and guidelines. The ultimate goal is to optimize the auxiliary ventilation system using ducted fans in series to provide a reliable and efficient solution to maintain clean and safe workplace environment in local long underground mines.

A Study on the Polychaete Community Kwangyang Bay, Southern Coast of Korea (光陽灣의 多毛類群集에 관한 硏究)

  • Choi, Jin Woo;Koh, Chul Hwan
    • 한국해양학회지
    • /
    • v.19 no.2
    • /
    • pp.153-162
    • /
    • 1984
  • This study was conducted to interpret the relations between the polychaete community and its environments in Kwangyang Bay during July, 1982. The type of sediments in the study area varies from sand to clay and the organic content obtained by ignition was in the ranges of 0.3% to 15.4%. The polychaetes which occurred at 25 stations comprised 70 species representing 63 genera and had an average density of 490 animals/m$\^$2/. The most abundant species were Lagis bocki (20%), Lumbrineris longifolia (10%), Chohe teres (7%), and Sternaspis scutata (5%). The polychaete populations show the highest density in muddy sand sediments and have a tendency to decrease their abundance in finer sediments such as bud and clay. The individual numbers of each feeding type show the same tendency. Kwangyang Bay consists of three distinct characteristic communities, representing different physical and biological factors: delta community, muddy flat community and channel community. Delta community has very poor organisms and seems to be determined by physical factors such as tidal current, and by sediment conditions and seems to be determined by physical factors such as tidal current, and by sediment conditions and by the food availability. Muddy flat community shows more diverse and higher abundance than delta community but seems to be impoverished by the stress of oxygen deficiency in sediments. Channel community has the highest density in the study area and comprises more various feeding types. This is probably due to the supply of allochthonous materials from the Seomjin River and offshore as food, the heterogeneous sediments and some biological interactions within habitats.

  • PDF

Comparison of Image Quality in Magnetic Resonance Imaging of the Abdominal Organ at 1.5T and 3.0T before the Gadolinium Injection (조영제 주입 전 1.5T 와 3.0T를 이용한 복부장기 자기공명영상에서 영상의 질 비교)

  • Goo, Eun-Hoe
    • Journal of the Korean Society of Radiology
    • /
    • v.11 no.7
    • /
    • pp.619-625
    • /
    • 2017
  • The sudy was intended to evaluate the optimal equipment selection by quantitatively assessing the SNR(signal to noise ratio) and CNR(contrast to noise ratio) on the abdominal organ. This study performed on 1.5 T and 3.0 T MRI units focusing on HASTE, HASTE(f/s) and FFE(in of phase), FFE(out of phase) without using the contrast medium(Gadolinium). The data analysis was performed by randomly selecting on 1.5 T and 3.0 T abdominal MRI images. As a results, SNR and CNR values of 3.0 T is higher than 1.5 T at liver, kidney and spleen(p<0.05). Stomach, abdominal fat and pancreas was obtained a higher value at 1.5 T(p<0.05). On conclusion, the organs of outer part in the body showed generally a high value at 3.0 T, and the organs of inner part in the body including the gas showed a high value at 3.0 T because of a large difference on magnetic susceptibility.

Wall Tie Member Force Curve for the Construction Tower Crane (건축용 타워크레인 마스트의 횡방향 지지요소인 월타이 부재력 특성곡선)

  • Ko, Kwang IL;Oh, W.H.;Lee, E.T.
    • Journal of Korean Society of Steel Construction
    • /
    • v.18 no.6
    • /
    • pp.697-706
    • /
    • 2006
  • Tower crane's wall tie is generally used for extending of mast height according to rising of lifting height. In order to get wall tie member force this problem, this study concerning wall tie is based on load data described in manual book of 290HC model. This study made the equation of wall tie member force and computer programming for calculating wall tie member force and then get ${\theta}-P$ curves(angle-wall tie force). After considering the ${\theta}-P$ curves, optimum angle range ($48.4^{\circ}{\sim}77.2^{\circ}$) about wall ties (A), (C) members was obtained. Member force of wall tie (B) was changed from tension to compression or from compression to tension at $74^{\circ}$ in service and $54^{\circ}$ in out of service. When both horizontal force($H_A$) and torsional moment ($M_D$) were varied from (+) to (-), wall tie force(A, B, C) were changed almost symmetrically about ${\theta}$-axis. Because this study was based on wall tie analysis conditions, wall tie members in symmetric and ideal geometry shape used for analizing wall tie of tower crane, it is necessary to have more careful verification in order to apply generally the results of this study.

The Quality Characteristics of Cookies Prepared with Agaricus blazei Murill (아가리쿠스 버섯 가루를 첨가한 쿠키의 최적화 연구)

  • Lee, Heejeong;Jeong, Hee Sun;Joo, Nami
    • Korean journal of food and cookery science
    • /
    • v.31 no.2
    • /
    • pp.175-184
    • /
    • 2015
  • The purpose of this study was to determine the optimal mixing ratio of Agaricus blazei Murill powder and butter in the preparation of cookies. The experimental design utilized herein was based on central composite design for response surface methodology, which included 10 experimental points, including 2 replicates for Agaricus blazei Murill and butter. The physical, mechanical, and sensory properties of the test were measured, and these values were applied to the mathematical models. A canonical form and perturbation plot showed the influence of each ingredient on the final mixed product. The spread ratio increased significantly with an increase in Agaricus blazei Murill powder and butter (p<0.05). The response surface methodology was applied to evaluate the effect of Agaricus blazei Murill powder and butter on cookie moisture and color (L, a) (p<0.001). Sensory evaluation showed significant values for color (p<0.05), flavor (p<0.05), texture (p<0.05) and overall quality (p<0.01) in the predicted model. The optimum formulation by numerical and graphical methods was calculated as follows: Agaricus blazei Murill powder 3.63 g, butter 55.37 g.

Development and Effectiveness of Private Parking Information Algorithm (복합용도 초고층빌딩에 대한 개별주차정보제공 알고리즘 개발)

  • Kim, Young-Sun;Nam, Baek;Lee, Choul-Ki;OH, Young-Tae
    • The Journal of The Korea Institute of Intelligent Transport Systems
    • /
    • v.12 no.5
    • /
    • pp.13-21
    • /
    • 2013
  • Super high-rise buildings of combined use such as large shopping malls and multiplex etc. have larger parking facilities than general buildings and are characteristic of an increase in the number of the entrance and the exit connecting internal external space of the parking lot. These features cause a congestion of internal traffic by increasing car driving distance in the parking lot, and vehicle idling increases by drivers wander the parking lot in order to find parking space. In addition, they make drivers suffer from lots of difficulties due to parking including increasing their walking line after parking. Therefore, in this study, we developed individual parking information provision algorithm to specify the optimal parking place for drivers according to the purpose of visiting a building and the drivers' moving path, and selected new construction site for the second lotte world in order to evaluate the algorithm developed and performed evaluation. As a result of the evaluation, it was analyzed that in the case of applying the individual parking information provision algorithm compared to the existing parking information provision algorithm, moving distance in the parking lot decreases around 7.43~83.4%, and that in the case of $CO_2$ emission, it decreased about 47.7% on average, which indicates that the efficiency resulted from application of the individual parking information provision algorithm is very high as the application effects are tested.

Study on Corrosion and Structural Performance in Hot-Dip Galvanizing Steel (용융아연도금 철근의 부식 특성 및 구조적 특성에 대한 연구)

  • Kwon, Seung-Jun;Lee, Sang-Min;Lee, Myung-Hoon;Park, Sang-Soon
    • Journal of the Korea Concrete Institute
    • /
    • v.24 no.5
    • /
    • pp.613-621
    • /
    • 2012
  • Steel corrosion is one of the most critical deteriorations in concrete structures due to the problems associated with both durability and structural safety issues. For protection of steel against corrosion problems, researches to improve concrete durability and steel corrosion protection such as rebar coating by hot-dip galvanizing steel have been carried out. This study was performed to quantitatively evaluate anti-corrosion and structural performance of concrete structures reinforced with hot-dip galvanizing steel rebar. Preliminary tests for several metal coatings such as zinc, aluminum, and their alloy (Zn 45% + AL 55%) were performed. After evaluation of corrosive characteristics, Zn was selected for the coating material and the corrosion behaviors in Zn-coated steel were evaluated in various conditions. Furthermore, tensile and adhesive strengths were evaluated for the normal and the hot-dip galvanized steel. The crack patterns and structural behaviors of RC specimens with the normal and coated steel were investigated. Also, corrosion characteristics including corrosion in various coating metal and potential change in metal with notch were evaluated. Structural performances of tensile and adhesive strengths as well as RC beam behavior under flexural/shear loading were evaluated. The test and evaluation results showed that the applicability of hot-dip galvanized steel rebar can be used as corrosion resistant reinforcements for RC structures.