• Title/Summary/Keyword: 최적기준법

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Development and Validation of a Simultaneous Analytical Method for 5 Residual Pesticides in Agricultural Products using GC-MS/MS (GC-MS/MS를 이용한 농산물 중 잔류농약 5종 동시시험법 개발 및 검증)

  • Park, Eun-Ji;Kim, Nam Young;Shim, Jae-Han;Lee, Jung Mi;Jung, Yong Hyun;Oh, Jae-Ho
    • Journal of Food Hygiene and Safety
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    • v.36 no.3
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    • pp.228-238
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    • 2021
  • The aim of this research was to develop a rapid and easy multi-residue method for determining dimethipin, omethoate, dimethipin, chlorfenvinphos and azinphos-methyl in agricultural products (hulled rice, potato, soybean, mandarin and green pepper). Samples were prepared using QuEChERS (Quick, Easy, Cheap, Effective, Rugged and Safe) and analyzed using gas chromatography-tandem mass spectrometry (GC-MS/MS). Residual pesticides were extracted with 1% acetic acid in acetonitrile followed by addition of anhydrous magnesium sulfate (MgSO4) and anhydrous sodium acetate. The extracts were cleaned up using MgSO4, primary secondary amine (PSA) and octadecyl (C18). The linearity of the calibration curves, which waas excellent by matrix-matched standards, ranged from 0.005 mg/kg to 0.3 mg/kg and yielded the coefficients of determination (R2) ≥ 0.9934 for all analytes. Average recoveries spiked at three levels (0.01, 0.1, 0.5 mg/kg) and were in the range of 74.2-119.3%, while standard deviation values were less than 14.6%, which is below the Codex guideline (CODEX CAC/GL 40).

Research Trend of High-Efficiency Charging Method for Lithium Rechargeable Batteries (리튬이차전지의 고효율 충전법 연구 동향)

  • Kim, K.M.;Lee, Y.G.;Yang, Y.S.;Kim, J.
    • Electronics and Telecommunications Trends
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    • v.25 no.5
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    • pp.11-19
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    • 2010
  • 유비쿼터스 시대의 모바일 전력원으로서 가장 유용한 리튬이차전지의 충전방식은 1991년 리튬이온전지의 상용화 이후 정전류-정전압 방식의 충전법이 고수되어 왔다. 그러나 압전, 열전 등 신재생에너지에 의한 에너지 하베스팅으로 생성되는 전력의 성질이 전압과 전류의 범위가 매우 다양하므로 효율적으로 저장할 수 있는 에너지 매니지먼트 체계가 필요하다. 이에 대한 기반연구로서 리튬이차전지의 고효율 충전을 위한 다양한 방식이 고려되어 왔으며, 본 동향분석서에서는 이러한 충전방식에 따라 리튬이차전지 내부 소재가 받는 영향과 여러 충전방식의 장단점을 분석하고, 최적 충전방식의 기준을 정리한다.

고능솔.고정도를 위한 연삭가공

  • 송지복
    • Journal of the KSME
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    • v.26 no.4
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    • pp.290-296
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    • 1986
  • 좋은 품질의 제품을 높은능률 낮은원가로 생산하는 것이 가공의 목표이다. 연삭가공은 이 목 표에 도달할 수 있는 가공기술의 하나이며 현재 기계부품의 제작에 있어서 최종공정으로 널리 활용되고 있으나 아직도 해명되어야 할 과제들(예를 들면 연삭입력조건의 형식화, 연삭결과의 예측기술 확립, 숫돌의 선택기준의 설정, 연삭가공의 고능률화 고정도화를 위한 최적기술등)이 적지 않다. 이들 문제를 해결하고 연삭가공 기술을 고도화하기 위해 연삭현상을 파악하여야 한다. 이러한 관점에서 본고에서는 먼저 연삭가공 시스템과 연삭과정의 몇가지 현상을 고찰하고 나아가 고능률 고정도화를 위한 연삭가공기술로서 연삭입자의 절인속도를 증가하는 고속연삭법, 절인과 공작물과의 간섭현상을 크게하는 중연삭법, 유효숫돌의 절대량과 연삭량을 제어하는 정 밀연삭에 관하여 기술코져 한다.

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Network Design and Measurement Frequency of Water Quality in Kyoung-An Stream Basin (경안천 유역의 수질관측망 구성과 적정 측정 빈도)

  • Kyoung, Min-Soo;Kim, Sang-Dan;Kim, Hung-Soo;Kim, Duck-Gil
    • Proceedings of the Korea Water Resources Association Conference
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    • 2006.05a
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    • pp.2011-2015
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    • 2006
  • 본 연구에서는 시공간을 고려하여 경안천유역의 최적 수질 측정망을 구성하였다. 분석을 위해서 필요한 수 질 데이터는 QUAL2E 모형을 이용하여 모의하였으며, 매개변수의 추정을 위하여 HEC-RAS모형과 민감도 분석 기법인 1차 신뢰성 분석(FORA)를 사용하였다. QUAL2E 모형의 모의 결과를 바탕으로 크리깅 기법과 Branch and Boundary Method를 이용하여 평수량 일때와 갈수량 일때로 구분하여 관측지점의 개수와 위치를 제시하였다. 선정된 지점을 기준으로 비례표본추출법(proportional sampling method)을 이용하여 각각의 지점별 측정 빈도를 제시하였다.

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Parameter Determination of Rainfall Runoff Model by Storage Function Model (저유함수법에 의한 강우-유출모형의 변수추정)

  • 남궁달
    • Water for future
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    • v.18 no.2
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    • pp.175-185
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    • 1985
  • This paper discusses the posibility of synthesizing flood hudrographs by the stroage function model. Eight small watersheds from Han, Gum, Nakdong, Youngsan river system were selected for this purpose. The optimum constants are computed from the chi square criterion by the SDFP methods Based on these constants, equations for the storage constant and Lag time are derived from the kinematic wave theory and storage function theory. These relations are examined by using optimum constants of the storage function model and assumptive constant of the kinematic wave model. Main results are sumarized as follows. 1. Constants of the storage function model are closely related to those of the kinematic wave model. The formula obtained theoretically is difficult to use practically because of the unclaified definition of factors. 2. In order to estimate constants of the storage function model for the practical purpose, new equations are also proposed for mountaneous area. 3. The verification of proposed equation is made for several recorded floods for mountaeous areas.

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Optimum Slab-Lifting Positions for Precast Concrete Pavement Construction (프리캐스트 콘크리트 포장 시공 시 최적 슬래브 리프팅 위치)

  • Kim, Seong-Min;Cho, Byoung-Hooi;Han, Seung-Hwan
    • International Journal of Highway Engineering
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    • v.9 no.2 s.32
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    • pp.27-37
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    • 2007
  • This research was conducted to determine the optimum lifting positions on precast concrete slabs for precast concrete pavement construction, based on the analysis of concrete stress distribution under various lifting conditions. To analyze stresses in concrete slabs, the finite element method was implemented and a numerical model of the precast slab that was going to be used in the experimental construction was developed. Changes in the stress distribution due to the lifting angle were investigated because slab lifting is not always performed in the perpendicular direction to the slab surface. In addition, the effect of the lifting level, the distance between the neutral axis of the slab and the lifting point, on the stress distribution was investigated since the lifting point is not always at the neutral axis of the slab. To consider the actual steel design of the precast slab, the effect of the reinforcement near the lifting point was also investigated. From this study, the optimum lifting positions of the precast slabs were determined according to the lifting angle and level, and the results were compared with the lifting positions used in the PCI standards.

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Adsorption Characteristics of Reverse Stratified Tapered Adsorber (역층상 점증형 흡착탑에서의 흡착특성)

  • Lee, Seung-Mok;Kim, Dae-Hyun;Lee, II-Young
    • Journal of Korean Society of Environmental Engineers
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    • v.22 no.10
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    • pp.1861-1867
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    • 2000
  • Granular activated carbon(GAC) adsorption is one of the best available technology to remove synthetic organic chemicals(SOCs) from water supplies and wastewater. In order to satisfy enviromental criteria and reduce GAC treatment cost, optimal study of reverse stratified tapered adsorber(RSTA) has been conducted. The RSTA was found to provide on increase in breakthrough time when compared to a conventional cylindrical adsorber(CA). Through the RSTA optimal experiment, optimal mean bed velocity was decided 19.10cm/min and optimal angle was decided RSTA($3.0^{\circ}$). Adsorption efficiency was increased with increasing activated carbon doses and the number of activated carbon layers.

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A Study on the Vibration Analysis and Optimization for the Composite Optical Structure of an Aircraft (복합재료를 적용한 항공기용 카메라 구조 경량화 설계 및 최적조건 선정에 관한 연구)

  • Kim, Byeong-Jun;Lee, Jun-Ho;Lee, Haeng-Bok;Jung, Dae-Yoon;Cheon, Seong-Sik
    • Composites Research
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    • v.25 no.6
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    • pp.230-235
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    • 2012
  • This paper presents the vibration characteristics and the optimization using the orthogonal array about applied composite optical structure of an aircraft. To acquire the vibration characteristics for stable line of sight, modal analysis are performed by using multi-body program ADAMS. And to optimize optical structure, for design variables were selected, larger-the-better characteristics were considered using results of S/N ratio and orthogonal array $L_9(3^4)$. When bearing constraints are selected, radial, axial and moment stiffness value are used to analysis for optimization until now. But B.S.R which is non-dimensional parameter is proposed, structures including bearings can be used for optimization. And then having a result of lager-the-better, the optimized values of each design variable were successfully suggested.

Minimum Weight Design of the Boom of an Ecavator (굴삭기 붐의 최적 설계)

  • 임오강;신양범;이병우
    • Computational Structural Engineering
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    • v.6 no.1
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    • pp.91-98
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    • 1993
  • Minimum weight design of the boom of an excavator with stress and displacement constraints was performed. The procedure of analysis consists of the following steps. The finite element model of the boom was built up by using 227 triangular plate elements each of which has three nodes. And then the finite element program was implemented and its accuracy was verified by comparing its results with those of the commercial structural analysis package-ANSYS 4.4A. For the constraints of stresses and displacements, the design sensitivities of those were computed using direct differentiation method. To verify the reliability of them the results were compared with those of the finite difference method. The optimum design value was obtained by using PLBA(Pshenichny-Lim-Belegundu-Arora)non-linear optimization program which adopts the active set strategy. Using the above results, minimum weight design of an excavator boom showed an effect of 27% reduction in weight.

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An Experimental Study on the Optimum Design Conditions of Curtain-wall Flame in Fire (화재시 커튼월 프레임 최적설계조건 도출을 위한 실험적 연구)

  • Kim, Hyung-Jun;Kim, Jung-Hyun;Kim, Heoung-Youl;Lee, Jae-Sung;Lim, Hyun-Chang
    • Proceedings of the Korea Institute of Fire Science and Engineering Conference
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    • 2011.04a
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    • pp.351-356
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    • 2011
  • 본 연구에서는 국외 커튼월 내화 Code인 EN 13830, EN 13501-1, EN 1364-3을 사용하여 알루미늄과 스틸프레임에 대해 화재시 최적설계조건 도출을 위한 실험을 실시하였다. 현재 국내 커튼월의 내화 법규는 2008년 '내화 충전구조 세부 운영지침'에서 조인트 부분에 대해서만 내화규정이 정립되어 있다. 따라서 본 연구에서는 EN 13830과 그 하위법을 이용하여 알루미늄과 스틸 커튼월의 최적설계조건 도출을 위한 실험을 실시하였다. 실험 결과 차염성은 알루미늄 커튼월과 스틸 커튼월의 성능시간이 각각 10분 26분으로 약 16분의 차이가 발생하였고, 차열성은 알루미늄 커튼월과 스틸 커튼월이 최고온도에서 6분과 9분으로 약 3분정도의 차이를 보였고 평균온도에서는 9분, 24분으로 약 15분의 차이를 보였다. 그리고 복사열은 성능기준 $15Kw/m^2$를 통과하는데 알루미늄 커튼월은 16분 스틸 커튼월은 24분을 기록하였다.

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