Development and Validation of a Simultaneous Analytical Method for 5 Residual Pesticides in Agricultural Products using GC-MS/MS
![]() |
Park, Eun-Ji
(Pesticide and Veterinary Drug Residues Division, Food Safety Evaluation Department, National Institute of Food and Drug Safety Evaluation, Ministry of Food and Drug Safety)
Kim, Nam Young (Pesticide and Veterinary Drug Residues Division, Food Safety Evaluation Department, National Institute of Food and Drug Safety Evaluation, Ministry of Food and Drug Safety) Shim, Jae-Han (College of Agriculture and Life Sciences, Chonnam National University) Lee, Jung Mi (Pesticide and Veterinary Drug Residues Division, Food Safety Evaluation Department, National Institute of Food and Drug Safety Evaluation, Ministry of Food and Drug Safety) Jung, Yong Hyun (Pesticide and Veterinary Drug Residues Division, Food Safety Evaluation Department, National Institute of Food and Drug Safety Evaluation, Ministry of Food and Drug Safety) Oh, Jae-Ho (Pesticide and Veterinary Drug Residues Division, Food Safety Evaluation Department, National Institute of Food and Drug Safety Evaluation, Ministry of Food and Drug Safety) |
1 | Metzger, J.D., Keng, J., Effects of dimethipin, a defoliant and desiccant, on stomatal behavior and protein synthesis. J. Plant Growth Regul., 3, 141-156 (1984). DOI |
2 | Metzger, J.D., Keng, J., Cellular basis for dimethipin-induced loss of leaf turgor and desiccation. J. Plant Growth Regul., 6, 33-40 (1987). DOI |
3 | Macdonald, R.S., Surgeoner, G.A., Solomon, K.R., Harris, C.R., Effect of four spray regimes on the development of permethrin and dichlorvos resistance, in the laboratory, by the house fly (Diptera: Muscidae). J. Econ. Entomol., 76, 417-422 (1983). DOI |
4 | Han, J., Kim, G.H., Susceptibilities of german cockroach, Blattella germanica to insecticides according to application methods. Korean J. Appl. Entomol., 43, 241-247 (2004). |
5 | Beynon, K.I., Edwards, M.J., Elgar, K., Wright, A.N., Analysis of crops and soils for residues of chlorfenvinphos insecticide and its breakdown products. J. Sci. Food Agric., 19, 302-307 (1968). DOI |
6 | Suett, D.L., Influence of formulation on chlorfenvinphos uptake and cabbage root fly control on radish. Ann. Appl. Biol., 92, 173-184 (1979). DOI |
7 | Lee, H., Han, J., Yoon, E., Kim, H., Hwang, I.G., Choi, D.M., Lee, K.B., Won, K.P., Song, I.S., Park, S.E., Shin, D.C., Cumulative risk assessment of organophosphorus pesticides in the diet. J. Food Hyg. Saf., 16, 21-26 (2001). |
8 | Huff, J., Benzene-induced cancers: abridged history and occupational health impact. Int. J. Occup. Environ. Health, 13, 213-221 (2007). DOI |
9 | Anastassiades, M., Lehotay, S.J., Stajnbaher, D., Schenck, F.J., Fast and easy multiresidue method employing acetonitrile extraction/partitioning and "dispersive solid-phase extraction" for the determination of pesticide residues in produce. J. AOAC Int., 86, 412-431 (2003). DOI |
10 | Ministry of Food Drug Safety, (2021, June 18). Pesticides MRLs in agricultural commodities. Retrieved from https://www.foodsafetykorea.go.kr/foodcode/02_01.jsp |
11 | Lehotay, S.J., Son, K.A., Kwon, H., Koesukwiwat, U., Fu, W., Mastovska, K., Hoh, E., Leepipatpiboonc, N., Comparison of QuEChERS sample preparation methods for the analysis of pesticide residues in fruits and vegetables. J. Chromatogr. A, 1217, 2548-2560 (2010). DOI |
12 | CODEX Alimentarius Commission, 2003. Guidelines on good laboratory practice in residue analysis, CAC/GL 40-1993. CAC, Rome, Italy. |
13 | Cengiz, M.F., Certel, M., Gocmen, H., Residue contents of DDVP (Dichlorvos) and diazinon applied on cucumbers grown in greenhouses and their reduction by duration of a pre-harvest interval and post-harvest culinary applications. Food Chem., 98, 127-135 (2006). DOI |
14 | Stan, H.J., Pesticide residue analysis in foodstuffs applying capillary gas-chromatography with mass spectrometric detection state-of-the-art use of modified DFG-multimethod S19 and automated data evaluation. J. Chromatogr. A, 892, 347-377 (2000). DOI |
15 | Lehotay, S.J., Determination of pesticide residues in foods by acetonitrile extraction and partitioning with magnesium sulfate: collaborative study. J. AOAC Int., 90, 485-520 (2007). DOI |
16 | Ministry of Food and Drug Safety, (2021, June 18). Guidelines on standard procedures for preparing analysis method. Retrieved from http://www.nifds.go.kr/brd/m_15/view.do?seq=8215 |
17 | Suett, D.L., Persistence and degradation of chlorfenvinphos, diazinon, fonofos and phorate in soils and their uptake by carrots. Pest. Sci., 2, 105-112 (1971). DOI |
18 | Athanasopoulos, P.E., Pappas, C., Effects of fruit acidity and storage conditions on the rate of degradation of azinphos methyl on apples and lemons. Food Chem., 69, 69-72 (2000). DOI |
19 | Edokpolo, B., Yu, Q.J., Connell, D., Health risk assessment of ambient air concentrations of benzene, toluene and xylen (BTX) in service station environments. Int. J. Environ. Res. Public Health, 11, 6354-6374 (2014). DOI |
![]() |