• Applied Chemistry for Engineering
• /
• v.29 no.5
• /
• pp.565-570
• /
• 2018

In this study, the antioxidant was extracted from Broussonetia kazinokii using ultrasound-assisted extraction (UAE) and optimized by using a response surface methodology. The response value of the central composite design model establishes the extraction yield and the DPPH radical scavenging activity. The extraction time and temperature and volume ratio of ethanol/ultrapure water were selected as quantitative factors. When considering both the main and interaction effects, the factor having the greatest influence on the extraction yield and 2,2-diphenyl-1-picrylhydrazyl (DPPH) radical scavenging activity was the volume ratio of ethanol/ultrapure water. The results of optimal extraction conditions were the extraction time (19.92 min), volume ratio of ethanol/ultrapure water (54.23%), and ultrasonic irradiation power (557.65 W). We could also obtained expected results of the yield = 38.93 wt% and DPPH radical scavenging activity = 55.33% under these conditions.

• Elastomers and Composites
• /
• v.40 no.3
• /
• pp.174-180
• /
• 2005

Sonochemical synthesis of fullerene oxides $[C_{70}O_n](n=1{\sim}2)$ by fullerene$[C_{70}]$ and metal hexacarbonyl complexes $M(CO)_6$(M=Cr, Mo, W) took place under air atmosphere. The reactivity of fullerene$[C_{70}]$ and several metal hexacarbonyl complexes $M(CO)_6$(M=Cr, Mo, W) under same ultrasonic condition increased in the order of $Mo(CO)_6$ > $W(CO)_6$ > $Cr(CO)_6$. The MALDI-TOF-MS, UV-visible spectra, and HPLC analysis confirmed that the products of sonochemical reaction were $[C_{70}O_n](n=1{\sim}2)$.

• Proceedings of the Materials Research Society of Korea Conference
• /
• 2007.11a
• /
• pp.79.2-79.2
• /
• 2007

• Journal of the Korean Society for Nondestructive Testing
• /
• v.35 no.5
• /
• pp.299-306
• /
• 2015

A conventional phased array system can control an ultrasonic beam electronically by adjusting the excitation time delay of individual elements in a multi-element probe and produce an ultrasonic image. In Contrast, full matrix capture (FMC) is a data acquisition process that allows receiving ultrasonic signals from one single shot of the phased array transducer element through all the other elements and captures the complete dataset from every possible transmit-receive combination. This FMC data can be used to create the ultrasonic image in post processing. It is possible to produce not only images equivalent to conventional phased array image but also total focusing method (TFM) images with improved resolution and sharpness, which is virtually focused at any point in a region of interest. In this paper, the system that can perform FMC by using a conventional phased array instrument is developed, and a study was conducted on the imaging algorithms to reconstruct sector B-scan and TFM images from FMC dataset.

• Journal of Biomedical Engineering Research
• /
• v.25 no.5
• /
• pp.403-414
• /
• 2004

In the accompanying paper, we proposed a real. time volumetric imaging method using a cross array based on receive dynamic focusing and synthetic aperture focusing along lateral and elevational directions, respetively. But synthetic aperture methods using spherical waves are subject to beam spreading with increasing depth due to the wave diffraction phenomenon. Moreover, since the proposed method uses only one element for each transmission, it has a limited transmit power. To overcome these limitations, we propose a new real. time volumetric imaging method using cross arrays based on synthetic aperture technique with linear wave fronts. In the proposed method, linear wave fronts having different angles on the horizontal plane is transmitted successively from all transmit array elements. On receive, by employing the conventional dynamic focusing and synthetic aperture methods along lateral and elevational directions, respectively, ultrasound waves can be focused effectively at all imaging points. Mathematical analysis and computer simulation results show that the proposed method can provide uniform elevational resolution over a large depth of field. Especially, since the new method can construct a volume image with a limited number of transmit receive events using a full transmit aperture, it is suitable for real-time 3D imaging with high transmit power and volume rate.

• Journal of Biomedical Engineering Research
• /
• v.23 no.2
• /
• pp.87-99
• /
• 2002

This paper describes a method for overcoming the motion artifacts inherent in synthetic aperture(SA) imaging. based on the investigation results as to the influence of a target motion on synthetic aperture techniques. This method uses a region-based motion compensation approach in which only the axial motion is estimated and compensated for a given region of interest(ROI) under the assumption that the whole ROI moves uniformly The estimated axial motion is calculated with a crosscorrelation(CC) method at the Point where the focused signal has the maximum energy within the ROI. We also presents a method for estimating the axial motion using the autocorrelation(AC) method that is widely used to estimate average Doppler frequency Both computer simulations and in vivo experiments show that the proposed methods can improve greatly the spatial resolution and SNR of ultrasound imaging by implementing the SA techniques for two-way dynamic focusing without motion artifacts. In addition the AC-barred motion compensation method provides almost the same results as the CC-based one, but with a dramatically reduced computational complexity.

• Journal of the Korean Crystal Growth and Crystal Technology
• /
• v.2 no.2
• /
• pp.11-19
• /
• 1992

$SrTiO_3$powders were synthesized from the chloride and the nitrate aqueous solution by spray pyrolysis method using ultrasonic vibrator. The concentration of mother solution was prepared 0.05M and O.lM. The carrier gas flow rate was 0.5cm/sec and 1.5cm/sec, respectively. The formation processing was investigated in the 0.05M and 0.05cm/sec. The $SrTiO_3$powders could not be synthesized from chloride aqueous solution. The prepared powders from nitrate aqueous solution was SrTi03 with cubic structure and nearly sphere particle for all samples. Mean particle size was increased from $0.49{\mu}m$ to $0.67{\mu}m$ by changing the carrier gas flow rate from O.5cm/sec to 1.5cm/sec. Also, mean particle size increased from $0.49{\mu}m$to $0.55{\mu}m$by changing the concentration of mother solution from O.05M to O.1M. Atomizing droplet size was $14.3{\mu}m$. The shape of particles was very porous by evaporation of solvent at the initial step. But through the each step upwards, shape of particles was formed themselves into a nearly roundish.

• Journal of the Korean Crystal Growth and Crystal Technology
• /
• v.4 no.2
• /
• pp.178-189
• /
• 1994

Fine $BaTiO_3$ powder was synthesized from the various starting solution with 0.05 M by ultrasonic spray pyrolysis method. The conditions of synthesis were fixed on flow rate was 0.5 cm/sec, low temperature furnace was $300^{\circ}C$, and high temperatures furnace was $700^{\circ}C$. The formation procedure was investigated directly by SEM with the collected particle from the each reaction step. Also, the trace of particle in reaction tube was researched theoretically. Fine $BaTiO_3$ was synthesized only in the case of nitrate aqueous solution. The synthesized $BaTiO_3$ powder was porous and spherical which was consist of primary particle at the size of 19.1 nm. The formation procedure was as follows : the particle size decreased in drying step and then increased in initial thermal decomposition step. Finally, particle size was decreased to $0.42 {mu}m$. The trace of particle in reaction tube was also theoretically simulated and discussed.

• Journal of Biomedical Engineering Research
• /
• v.25 no.3
• /
• pp.201-206
• /
• 2004

The bone formation and re-formation are regulated by two factors that are the synthesis of bone matrix by osteoblast and reabsorption by osteoclast. Recently, there are many studies about regeneration and healing of bone tissue by activation of osteoblast. In general, it is known that the activation of osteoblast is influenced by not only biological stimulus but physical stimulus. In this study, we verified that ostoeblast activation was influenced by low intensity ultrasound. Various ultrasonic properties were used to find out the most appropriate condition on cell activation. From this study, we could confirm that 0.3W/$\textrm{cm}^2$ intensity of ultrasound was the most appropriate to tell activation over whole duty cycles and the increasing rate of tell was the highest at 50％ duty cycle. Thus, it is expected that optimal ultrasonic characteristics on regeneration of bone matrix may be applied to fracture and osteoporosis healing.

• Proceedings of the Korean Ceranic Society Conference
• /
• 2003.04a
• /
• pp.79.2-79
• /
• 2003