• Title/Summary/Keyword: 진공진

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CHARACTERISTICS OF THE CONTAMINATED LANGMUIR PROBE (오염된 LANGMUIR 탐침의 특성)

  • Pyo, Y. S.;Min, K. W.;Choi, Y. W.;Lee, D. H.;Kang, K. M.;Hwang, S. M.;Kim, B. C.;Kim, J.;Lee, S. J.
    • Journal of Astronomy and Space Sciences
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    • v.12 no.2
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    • pp.234-243
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    • 1995
  • Korea's third rocket, which is currently under development for launch in 1997, is expected to reach as high as 160km and thus, it will provide a good opportunity for the direct measurement of the plasmas in the E-region ionosphere of the Korean peninsula. Langmuir probe techniques, which are the basic tools of the plasma experiment, may yield inaccurate results if they are applied in the conventional form as they are used in the laboratory experiments because of the contamination. In the present paper we study the contamination problem by performing the ground experiments in the vacuum chamber using the contaminated probe. The result show that the contamination effect is reduced when the plasma density is low or when the frequency of the sweep voltage is fast. We propose a modified Langmuir probe based upon our experiments which is suitable for the rocket experiments.

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Study on 1,200 N-class bipropellant rocket engine using decomposed $H_2O_2$ and kerosene (분해된 과산화수소와 케로신을 이용한 1,200 N 급 이원추진제 로켓 엔진의 연구)

  • Jo, Sung-Kwon;An, Sung-Yong;Kim, Jong-Hak;Yoon, Ho-Sung;Kwon, Se-Jin
    • Journal of the Korean Society of Propulsion Engineers
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    • v.14 no.6
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    • pp.69-78
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    • 2010
  • As part of preliminary study for development of 1,200 N-class bipropellant rocket engine with the concentrated hydrogen peroxide, bipropellant engine elements were designed and experimentally tested. The catalysts of $MnO_2$ and $MnO_2$ added Pb as an additive were compared to achieve high decomposition performance and the catalytic reactor with $MnO_2$ added Pb was designed and its decomposition efficiency of 97.2% was achieved. The autoignition tests of kerosene by decomposed hydrogen peroxide were carried out under various equivalence ratios to ignite without additional ignition sources. Autoignition were achieved in all experimental conditions and $C^*$ efficiencies at each condition were at or above 90%. From the measured thrust results, the highest value was 830 N which is in corresponds with 1,035 N at vacuum level assuming $C^*$ efficiency equals $I_{sp}$ efficiency.

Fabrication and Mechanical Properties of STS316L Porous Metal for Vacuum Injection Mold (진공사출금형용 STS316L 금속 다공체 제조 및 기계적 특성)

  • Kim, Se Hoon;Kim, Sang Min;Noh, Sang Ho;Kim, Jin Pyeong;Shin, Jae Hyuck;Sung, Si-Young;Jin, Jin Kwang;Kim, Taean
    • Journal of Powder Materials
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    • v.22 no.3
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    • pp.197-202
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    • 2015
  • In this study, porous stainless steel (STS316L) sintered body was fabricated by powder metallurgy method and its properties such as porosity, compressive yield strength, hardness, and permeability were evaluated. 67.5Fe-17Cr- 13Ni-2.5Mo (wt%) powder was produced by a water atomization. The atomized powder was classified into size with under $45{\mu}m$ and over $180{\mu}m$, and then they were compacted with various pressures and sintered at $1210^{\circ}C$ for 1 h in a vacuum atmosphere. The porosities of sintered bodies could be obtained in range of 20~53% by controlling the compaction pressure. Compressive yield strength and hardness were achieved up to 268 MPa and 94 Shore D, respectively. Air permeability was obtained up to $79l/min{\cdot}cm^2$. As a result, mechanical properties and air permeability of the optimized porous body having a porosity of 25~40% were very superior to that of Al alloy.

Building of Large Triaxial Testing Apparatus and Static Triaxial Testing for Railway Ballast (대형삼축압축시험장비 구축과 도상자갈의 정적압축시험 평가)

  • Lee, Sung-Jin;Kim, Yun-Ki;Lee, Il-Wha;Lee, Jun-S.;Park, Jae-Jun
    • Journal of the Korean Society for Railway
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    • v.13 no.1
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    • pp.84-91
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    • 2010
  • We built multi-purpose large triaxial testing system that can test and evaluate various geotechnical design parameters such as shear strength, deformation modulus and stress-strain behaviour for large diameter granular materials, which are the most commonly used construction materials in the railway, road embankments. The details of the built testing system and the results obtained from static triaxial test carried out for gneiss ballast material are discussed within the scope of this paper. Ballast is hardly saturated and is confined at low overburden pressure, since the depth is shallow and the permeability is very high. Herein we ascertained that the confining pressure can effectively be controlled by vacuum. The rational trend could be checked up through triaxial test results such as shear strength, deformation, and particle breakage. And the shear strength envelope could be non-linearly represented with the parent rock strength, confining pressure of the triaxial test and proper parameters.

Processing of Powdered Seasoning Material from Sea Tangle (다시마를 이용한 분말 조미료 소재 개발)

  • 배태진;강동수
    • The Korean Journal of Food And Nutrition
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    • v.13 no.6
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    • pp.521-528
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    • 2000
  • Conditions for processing dried condiments with powdered sea tangle were investigated. The most appropriate method for sea tangle extraction was two-stage extraction, that extracted with addition of 70% ethyl alcohol at $25^{\circ}C$ for 1 hour and residue was re-extracted with water(1:15, w/w) at 7$0^{\circ}C$ for 3 hours. The yield of soluble solids under above-mentioned conditions was 14.9%. As a result of omission tests, free amino acids were predominated in the taste compounds of sea tangle extracts rather than nucleotides, and the contribution of free amino acids and nucleotides to the taste of sea tangle extracts was remarkable. The major flavoring components of sea tangle extracts were matters of low molecular weight such as free amino acids and oligopeptides below 5,700 dalton. Contents of carbohydrate, total nitrogen and amino nitrogen in dried condiments prepared with sea tangle extracts were 64.9%, 3.7% and 2.1%, respectively. And drying yield, solubility and absorption rates at Aw 0.88 were 14.7%, 98.3% and 8.4%, respectively.

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Microstructure Control of Porous Ceramics by Freeze-Drying of Aqueous Slurry (동결건조공정을 이용한 다공성 세라믹스의 미세구조 제어)

  • 황해진;문지웅
    • Journal of the Korean Ceramic Society
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    • v.41 no.3
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    • pp.229-234
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    • 2004
  • In this study, we proposed new forming process for a porous ceramic body with unique pore structure. h tubular-type porous NiO-YSZ body with radially aligned pore channels was prepared by freeze-drying of aqueous slurry. A NiO-YSZ slurry was poured into the mold, which was designed to control the crystallization direction of the ice, followed by freezing. Thereafter the ice was sublimated at a reduced pressure. SEM observations revealed that the NiO-YSZ porous body showed aligned large pore channels parallel to the ice growth direction, and fine pores are formed around the outer surface of the tube. It was considered that the difference in the ice growth rate during the freezing process resulted in such a characteristic microstructure. Bilayer consisting of dense thin electrolyte film of YSZ onto the tubular type porous body has been successfully fabricated using a slurry-coating process followed by co-firing. It was regarded that the obtained bilayer structure is suitable for constructing electrode-support type electrochemical devices such as solid oxide fuel cells.

Atomic Layer Deposition of Silicon Oxide Thin Film on $TiO_2$ nanopowders (원자층증착법에 의한 $TiO_2$ 나노파우더 표면의 실리콘 산화물 박막 증착)

  • Kim, Hee-Gyu;Kim, Hyung-Jong;Kang, In-Gu;Kim, Doe-Hyoung;Choi, Byung-Ho;Jung, Sang-Jin;Kim, Min-Wan
    • 한국신재생에너지학회:학술대회논문집
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    • 2009.11a
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    • pp.381-381
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    • 2009
  • 염료감응형 태양전지의 효율 향상을 위한 다양한 방법들 중 $TiO_2$ 나노 파우더의 표면 개질 및 페이스트의 분산성 향상을 위한 연구가 활발하게 진행되고 있다. 기존 나노 파우더의 표면 개질법으로는 액상 공정인 졸겔법이 있으나 표면 처리 공정에서의 응집현상은 아직 해결해야 할 과제 중 하나이다. 이에 본 연구에서는 진공증착방법인 ALD법을 이용하여 염료감응형 태양전지용 $TiO_2$ 나노 파우더의 $SiO_2$ 산화물 표면처리를 통한 분산특성을 파악하였다. 기존 ALD법의 경우 reactor의 온도가 $300{\sim}500^{\circ}C$ 정도의 고온에서 공정이 이루어졌지만 본 실험에서는 2차 아민계촉매(pyridine)을 사용하여 reactor의 온도를 $30^{\circ}C$정도의 저온공정에서 $SiO_2$ 산화물을 코팅을 하였다. MO source로는 액체상태의 TEOS$(Si(OC_2H_5)_4)$를, 반응가스로는 $H_2O$를 사용하였고, 불활성 기체인 Ar 가스는 purge 가스로 각각 사용 하였다. ALD 공정에 의해 표면처리 된 $TiO_2$ 나노 파우더의 분산특성은 각 공정 cycle에 따라 FESEM을 통하여 입자의 형상 및 분산성을 확인하였으며 입도 분석기를 통하여 부피의 변화 및 분산 특성을 확인하였다. 공정 cycle 이 증가함에 따라 입자간의 응집현상이 개선되는 것을 확인 할 수 있었으며, 100cycles에서 응집현상이 가장 많이 감소하는 것을 확인할 수 있었다. 또한 표면 처리된 $SiO_2$ 산화막은 XRD를 통한 결정 분석 및 EDX를 통한 정성 분석을 통하여 확인하였다.

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AES Analysis of Au, Au/Cr, Au/Ni/Cr and Au/Pd/Cr Thin Films by the Change of Substrate Temperature and Annealing Temperature (기판온도와 열처리온도의 변화에 따른 Au/Cr, Au/Ni/Cr 및 Au/Pd/Cr 다층박막의 AES 분석)

  • Yoo, Kwang Soo;Jung, Hyung Jin
    • Analytical Science and Technology
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    • v.6 no.2
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    • pp.217-223
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    • 1993
  • Thin films of the Au/Cr, Au/Ni/Cr and Au/Pd/Cr systems were deposited on alumina substrates at ambient temperature and $250^{\circ}C$ in a high-vacuum resistance heating evaporator and annealed at $300^{\circ}C$, $450^{\circ}C$ and $600^{\circ}C$ for 1 hour in air, respectively. The film thicknesses of Au, Ni(or pd), and Cr were $1000{\AA}$, $300{\AA}$, and $50{\AA}$, respectively. The substrate temperature during deposition and the post-deposition annealing temperature affected the sheet resistance of thin-films due to the inter-diffusion of each layer. As a result of Auger depth profile analysis, in the Au/Cr system Cr already diffused out to Au surface during deposition at the substrate temperature of $250^{\circ}C$ and Au distribution changed after heat treatment. In the Au/Ni/Cr and Au/Pd/Cr systems, diffusion phenomena of Ni and Pd were found and especially Ni (approximately 45 at.%) diffused out to Au surface and oxidized.

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Changes of Physicochemical and Sensory Characteristics in Vacuum-Packaged Beef Loin during Cold Storage Time (진공포장한 소등심육의 냉장저장중 이화학적, 관능적 특성의 변화)

  • 정인철;문윤희;홍대진;김미숙
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.27 no.2
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    • pp.214-219
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    • 1998
  • This study was carried out to investigate the changes of physicochemical and sensory characteristics according to cold storage period of the vacuum-time beef loin. The pH was decreased for 10 days, and then was increased gradually during storage time. The lactic acid content during the initial storage was 483mg/100g, after storage for 10 days it was increased significantly (p<0.05) to 625mg/100g, and then was decreased with storage time. Regarding of color difference, the L values were 41.0~42.5, but after storage for 40 days they were increased significantly(p<0.05) to 46.2, the a and b values wee 17.3~14.3 and 7.2~5.8, respectively, they were no significant differences depending n storage time. The shear force values showed 584 and 560g for 0 and 10 days, respectively but after storage for 20 days it was decreased significntly(p<0.05) to 299g. The myofibrillar protein extractability was no significant difference for 20 days, howener, it was increased remarkably at 30 days(p<0.05). The myofibrillar fragmentation index was increased significantly (p<0.05) on 20 and 40 days, and the Mg-ATPase activity of myofibrils was increasd to 30 days. The free amino acid was increased during storage periods. The composition of amino acid was composed of glutamic acid, alanine, valine and lysine, which were predominant amino acids as 45%. The total free amino acid was increased 182.18mg/100g to 40 days. The raw meat aroma showed no significant changes during storage time, but the tenderness was increased until 30 days(p<0.05). The color was superior from 20 to 30 days. The taste of cooked meat indicated significant changer to 30 days, but was significantly inferior(p<0.05) at 40 days, the aroma was superior until 30 days(p<0.05). The palatability was superior between 20 and 30 days.

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The fabrication and analysis of IR flat-band pass filter using chalcogenide thin films (칼코게나이드 박막을 이용한 IR flat-band pass filter 제작 및 특성 평가)

  • Kim, Jin-Hee;Yeo, Jong-Bin;Lee, Hyun-Yong
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2008.06a
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    • pp.231-231
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    • 2008
  • 최근 인터넷의 보급과 함께 고화질 및 양방향 TV, VOD 방송, 화상 전화 등의 멀티미디어 시대가 열리면서 초고속 통신 시스템에 대한 관심이 증가되고 있다. 특히 화상이나 동영상 같은 대량의 정보가 졸은 품질 및 빠른 속도로 전달될 수 있는 통신 시스템의 필요성이 대두됨에 따라 가장 효율적인 고속 전송 수단으로 광통신이 이용되고 있으며 그에 따른 광통신 능 수동 소자 개발에 관한 연구도 활발히 이루어지고 있다. 이러한 광통신 소자 중 원하는 빛을 선택적으로 투과하고 반사할 수 있는 flat-band pass(FP) filter의 역할이 중요한 부분을 차지하고 있다. 본 논문에서는 IR 영역에서 투과성이 우수한 칼코게나이드 물질을 이용해 l 차원 광자결정구조의 FP-filter를 설계, 제작하고 그에 대한 특성을 평가하였다. 시료는 5N의 순도를 갖는 As, Se, Te 물질을 준비하고 $As_xSe_yTe_z$를 조성비에 맞추어서 석영관에 진공 봉입한 후 용융 혼합하여 $As_{33}Se_{67}$$As_{40}Se_{25}Te_{35}$ 조성의 두 가지 비정질 벌크를 제작하였다. 제작된 시료의 굴절률은 ellipsometer을 사용하여 측정하였고, 본 연구진이 자체 개발한 계산툴에 따라 다중층막 구조를 설계하였다. 열 증착법을 이용하여 설계된 구조에 맞게 기판에 올리는 방법으로 1차원 광자결정 구조의 다중층막 샘플을 제작하였고 UV-Vis-IR Spectroscopy를 사용하여 반사도와 투과도를 측정하였다. 광통신용 L/C 밴드 주파수 범위에서 투과성이 우수한 칼코게나이드 박막의 1차원 광자결정 구조는 FP-filter등의 소자로써 유용하게 사용될 수 있다.

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