• Korean Journal of Materials Research
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• v.9 no.12
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• pp.1240-1244
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• 1999

In order to assess the effects on the magnetic properties due to the defect in the material irradiated by fast neutron ranging $10^0-10^{18}n/cm^2$, the magnetic properties such as maximum magnetic induction, coercivity, remanence, Barkhausen Noise Amplitude(BNA), Barkhausen Noise Energy(BNE) and hardness were measured. It is shown that the magnetic properties and hardness do not change by the fast neutron irradiation under $10^{17}n/cm^2$. Therefore, in this experiment, it is understood that the magnetic properties decrease by the increase of hardness. This measurement method can be used to evaluate the neutron irradiation embrittlement nondestructively since the magnetic properties and hardness do change by the neutron irradiation over $10^{17}n/cm^2$ consistently.

• Journal of the Korean Society for Nondestructive Testing
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• v.17 no.1
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• pp.31-40
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• 1997

원자로 압력용기 재료의 중성자 조사 취화 문제는 원자력발전소의 안전성 및 수명 관리에 가장 중대 한 영향을 미친다. 재료의 조사 취화를 평가하기 위하여 수행하고 있는 충격 및 인장시험 같은 파괴적 시험 결과는 석출물 크기나 분포, 전위 밀도 등, 재료 자체의 조직학적 특성에 좌우되므로 한정된 시편을 이용한 평가에는 많은 불확실성이 존재하게 된다. 따라서 이와 같은 문제점을 해결하기 위하여 비파괴기술을 이용한 조사 취화 평가에 대한 많은 연구가 진행되고 있다. 현재 원자로 압력용기 재료의 조사 취화에 따른 미세 조직 변화를 분석하기 위하여 응용되고 있는 비파괴기술로는 전기, 자기, 전자기, 초음파 및 경도측정법 등이 있으나 비파괴피험 결과와 미세조직의 변화, 기계적 성질 및 취화 정도 등과의 상관 관계를 정립해야만 기존 파괴적 시험의 대체가 가능하게 된다. 따라서 현재까지 수행되고 있는 여러 비파괴기술을 이용한 조사 취화 평가 연구결과를 비교 분석하여 보다 실현 가능성 있는 비파괴기술을 검토하였다.

• Journal of the Korean Crystal Growth and Crystal Technology
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• v.14 no.4
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• pp.129-134
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• 2004

In this study, we investigated the effect of a nitrogen atom on the amorphization of V-Fe alloy through solid-gas reaction during mechanical alloying (MA). MA by planetary ball mill of $V_{70}Fe_{30}$ elemental powders was carried out under the nitrogen gas atmosphere. Amorphization has been observed after 160 hours of ball milling in this case. The DSC spectrum for the mechanically alloyed ($V_{70}Fe$_{30}$)_{0.89}N_{0.11}$ powders exhibits a sharp exothermic peak due to crystallization at about $600^{\circ}C$. Structural transformation from the bcc crystalline to amorphous states was also observed through X-ray and neutron diffractions. We take a full advantage of a negligibly small scattering length of the V atom in the neutron diffraction measurement. During amorphization process the octahedral unit, which is typical of a polyhedron formed in any crystal structures, was preferentially destroyed and transformed into the tetrahedral unit. Futhermore, neutron diffraction measurements revealed that a nitrogen atom is selectively situated at a center of the polyhedron formed by V atoms.

• Nuclear Engineering and Technology
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• v.5 no.2
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• pp.137-149
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• 1973

A method of activation analysis, based on the irradiation and counting of an iron wire which contains manganese impurity as the single comparator. has been elaborated by critical evaluation of nuclear data involved in activation and activity measurement. The variation of effective cross section is investigated as a function of the spectral index and other parameters such as a measure of the proportion of epithermal neutrons in the reactor spectrum. The errors induced by shifts in the neutron spectrum in the irradiation positions are discussed. The known amount of each element is irradiated simultaneously together with the single comparator, and the obtained values are compared with the known amount of each element. The results show that en general the random errors are not greater than those obtained by using the conventional relative method, but the systematic errors were up to about 20%. This method is applied to the determinations of fourteen rare earth elements in monazite as well as other seven elements in the standard kale powder. The satisfactory reproducibility of the present method makes possible the determination of the elements with an accuracy attainable with the conventional relative method.

• Nuclear Engineering and Technology
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• v.13 no.4
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• pp.264-276
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• 1981

A simulation procedure which can represent time-dependent nuclear characteristics of TRIGA Mark-III reactor is developed. CITATION, a multi-group diffusion-depletion program, has been utilized as calculational tool. The group structure employed in this study consists of 7 groups: -3-fast and 4-thermal-which is conventionally utilized in TRIGA type reactor analysis. Three-dimensional nuclear characteristics are synthesized by combining results from two-dimensional plane calculation and two-dimensional cylinder calculation, since direct three-dimensional approach is not yet possible. An effort ia made to develope a method which can extract effective zone and group dependent bucklings by neutron diffusion theory rather than conventional zone and/or group independent Ducklings by neutron transport theory, since neutron leakage is quite high for small core such as research reactors. It is turned out that the method developed in this study gives satisfactory results. The calculation is performed under assumptions that all control rods are fully withdrawn, that no samples are inserted in the irradiation holes and that the core is located in the center of the reactor pool. Burnup-dependent variation of core excess reactivity, time dependent change of Xe-135 poisoning and reactivity worth of rotary specimen rack are calculated and compared with operation records. Neutron flux and power distribution as well as neutron spectrum in each irradiation .facility are presented.

• Analytical Science and Technology
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• v.18 no.4
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• pp.292-297
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• 2005

The effect of neutron irradiation on the chemical properties was measured in boric acid solution. The pH of the solution decreased in proportion to the irradiation time and the concentration of boric acid. The concentration of hydrogen peroxide, which is one of the radiolysis products of water, is in proportion to the concentration of boric acid, while in inverse proportion to the irradiation time. The oxygen and hydrogen gases had same chemically equivalent ratio in water radiolysis. The lithiun, which comes from $^{10}B(n,{\alpha})^7Li$, had poor relationship with neutron irradiation time at low concentration, $233{\sim}699{\mu}g/mL$, of boric acid, but the relationship was improved at higher concentration.

• Proceedings of the Korean Nuclear Society Conference
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• 1998.05b
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• pp.291-296
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• 1998

노내에서 지지격자 스프링의 잔류 탄성변위는 시간(연소도)에 따라 변하게 된다. 이는 격자판의 중성자 조사에 의한 길이방향의 성장으로 지지격자 셀 크기의 증가와 피복관의 크리프에 의한 직경의 감소 및 중성자 조사에 의한 지지격자 스프링력의 이완으로 인한 것이다. 만일 지지격자 스프링의 거동이 변하여 연료봉을 탄성적으로 지지하지 못할 경우 이것은 연료봉의 유체에 의한 진동을 가속시키게 되며, 연료봉과 지지격자 스프링이나 딤플간의 반복적인 고주기의 충격하중은 연료봉의 지지부와 봉간(grid-to-rod)의 프레팅 마모의 원인이 될 수 있다. 따라서 시간에 따라 변하는 변수들의 영향을 고려한 지지격자 스프링의 잔류 탄성변위를 예측할 수 있는 방법론을 정립하여 새로운 지지격자체의 개발시 건전한 연료봉의 지지거동을 평가할 수 있는 도구로 활용하고자 하였다.

• Transactions of the Korean Society of Pressure Vessels and Piping
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• v.15 no.2
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• pp.9-18
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• 2019

The objective of this study is to investigate the feasibility of simulating the mechanical properties of irradiatied austenitic stainless steels by cold-working. In this study, the tensile properties, cyclic hardening behaviors and fracture toughness of cold-worked TP316L stainless steel were compared with those of austenitic stainless steels irradiated by neutrons. It showed that cold-working can properly simulate the increase in strength and the decrease in ductility and fracture resistance of austenitic stainless steels by neutron irradiation, even though it could not perfectly simulate the microstructures of irradiated austenitic stainless steels. Also, cold-working can appropriately simulate the hardening behaviors of neutron irradiated austenitic stainless steels under monotonic and cyclic loading conditions.

• Korean Journal of Materials Research
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• v.11 no.8
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• pp.664-664
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• 2001

The mechanical alloying (MA) effect in $\sigma$-VFe intermetallic compound was studied by neutron and X-ray diffraction. The structure of MA $\sigma$-VFe powders were characterized by the X- ray diffraction with Cu- $K\alpha$ radiation and neutron diffraction with monochromatic neutrons of $1.835\AA$ using a high resolution powder diffractometer (HRPD). Mechanical alloying of $\sigma$-VFe compound gives rise to a dramatic structural change. After 60 hours of MA, the Fe-Fe distribution of the $\sigma$- phase VFe tetragonal structure with 30 atoms in a unit cell is found to change into that of the $\sigma$-(V,Fe) solid solution with bcc structure, which is a stable phase at elevated temperature above $1200^{\circ}C$. A comparison of X-ray diffraction data for the $\alpha$-phase has been also made with the corresponding neutron diffraction data. The (101) and (111) diffraction peaks of the $\sigma$-phase was clearly observed only in neutron diffraction pattern, which is believed to be a characteristic feature due to the chemical atomic ordering of $\sigma$- VFe phase.

• Korean Journal of Materials Research
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• v.8 no.11
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• pp.1020-1025
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• 1998

Irradiation-induced changes in mechanical properties and magnetic parameters were measured and compared to explore possible correlations for Mn-Mo-Ni low alloy steel surveillance specimens which were irradiated to a neutron fluence of $2.3\times10^{19}n/cm^2$(E>1.0MeV) in a typical pressurized water reactor environment at about $288^{\circ}C$. For mechanical property parameters, microvickers hardness, tensile and Charpy impact test were performed and Barkhausen noise amplitude, coercivity, remanence, maximum induction were measured for magnetic parameters. respectively. Results of mechanical property measurements showed an increase in yield and tensile strength, microvickers hardness. 41J indexed $RT_{NDT}$ and a decrease in upper shelf energy irrespective of base and weld metals. However, in the case of tensile properties, the changes in weld metal were negligible compared to the base metal. In the case of magnetic measurements, it is found that magnetic remanence, BN amplitude. BN energy have dropped significantly but coercivity(H,) has increased rapidly after irradiation. In this study. the measurements conducted on surveillance specimens of Mn-Mo-Ni low alloy steel showed that there were strong correlations between mechanical properties and magnetic properties.