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A Scientific Study on the Composition Analysis and Microstructure of the Yucheon-ri Goryeo Whiteware (유천리 고려백자의 조성 및 미세구조를 통한 과학적 연구)

  • Lee, Taejin;Koh, Minjeong;Lim, Sookyung;Yun, Eunyoung;Hwang, Hyunsung
    • Journal of Conservation Science
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    • v.30 no.1
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    • pp.67-80
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    • 2014
  • This study examined the chemical characteristics and the microstructure of Goryeo whiteware which was excavated in the kiln site Yucheon-ri, Gangwon-do, the southern part of South Korea. this area is considered to be used in the middle of the time of Goryeo Dynasty. We analyzed the chemical characteristics comparing Goryeo Whiteware from Seo-ri, Jungam-ri, Bangsan-dong and The temple site of Beopcheon. Based on the analysis, we confirmed the properties of raw material for making pottery. It is featured that body composition of Goryeo Whiteware from Yucheon-ri contains high silica and low solvent. However, the contents of the glaze are vice versa. Goryeo whiteware tends to contain larger part of oxide than that of titanium oxide, which applies to Goryeo Celadon. the whitewares during the early days of Goryeo Dynasty varies in components depending on kilns, whereas it does not mean that chronological changes happened in components. The whiteware shards from Yuchoen-ri have a similar aspect. The whiteware shard from the temple of Beopchen differ in composition, Thus they are estimated to have been produces and shipped from various sites. In conclusion, we judged that the component difference among Goryeo whitewares stems from production environment and origin of raw materials rather than chronological changers.

Compressive Strength Experiment of Lightweight Concrete Using Coarse Aggregate Produced by 3D Printing (3D 프린팅으로 제작한 굵은 골재를 사용한 경량콘크리트의 압축강도 실험)

  • Ahn, Byung-Ju
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.21 no.5
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    • pp.54-59
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    • 2020
  • Coarse aggregate is produced in various ways depending on the location and production method. Currently, the construction industry is in need of a stable supply of coarse aggregate and a way to secure standard quality. The purpose of this study is to examine whether the use of coarse aggregate in 3D printing can help solve this problem. ABS filament was selected for use in 3D printing. CATIA was used for the design of the coarse aggregate, and CUBICON Single Plus was used for the production. Six specimens were produced and cured in water for 28 days. Three of them were made with AE agent, and three were made without it. A compressive strength test confirmed that when the AE agent was used, the compressive strength was greater than the lightweight concrete design criterion specified in the concrete standard specification. This suggests that coarse aggregate produced by a 3D printer may be used for lightweight concrete. A mass production system using this method could help to solve the problems facing the construction industry, such as stable supply and demand for coarse aggregate and securing standard quality.

Joined in the government-owned handicraft industry during the Joseon Dynasty Job type and role (조선시대 관영수공업에서 입사장(入絲匠)의 직무 유형과 역할)

  • KIM, Serine
    • Korean Journal of Heritage: History & Science
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    • v.54 no.2
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    • pp.216-239
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    • 2021
  • Inlay (入絲), a poetic technique of digging grooves in the surface of crafts and decorating them with metal materials, was used throughout the royal daily routines, ceremonies and government officials of the Joseon Dynasty. The government-owned handicraft industry in the Joseon Dynasty was composed of craftsmen belonging to central and local government offices and was operated mainly by government-owned craftsmen. The inlay craftsman was transferred to the central government office and was in charge of inlay poetry for crafts. The current records of Korean inlay craftsmen are concentrated in the state-owned handicraft industry. In the state-owned handicraft industry, the government offices of inlay craftsmen can be divided into Kongjo (工造), Sangeuiwon (尙衣院), and the military. Here the election of a temporary government office for airspace is added. The government offices and military inlay craftsmen who use inlay crafts are assigned, and the inlay craftsmen are placed separately in the temporary office where the fine division of labor is developed. It can be made by utilizing craftsmen. The operation of these production systems was indispensable in pre-modern Korean society, where crafts had to be produced by hand. In this paper, we investigated the roles and job types of craftsmen in the state-owned handicraft industry during the Joseon Dynasty, focusing on inlay craftsmen. Although the details applied to the characteristics and materials of the field, labor supply and demand, etc. are different, Korea pursued crafts for various purposes through craftsmanship within the framework of the basic state-owned handicraft policy . The institutional equipment for implementation was almost common. We believe that adding and analyzing some literature records and relics will help us to study the crafts of the Joseon era in more detail.

Material Characteristics and Making Techniques of Pottery by Type from the Oryang-dong Kiln Site in Naju, Korea (나주 오량동 요지 출토 토기의 기종별 재료 특성과 제작기법 연구)

  • Jin, Hong Ju;Jang, Sungyoon;Kim, Su Kyoung;Lee, Myeong Seong
    • Journal of Conservation Science
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    • v.36 no.6
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    • pp.440-455
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    • 2020
  • This study aims to examine the material characteristics of bowls and compare the making techniques of flat cup with cover and jar coffin from the Oryang-dong kiln site, Naju. Bowls, the most frequently excavated small pottery have similar material characteristics, including gray surface, fine-grained texture, and small-sized tempers such as quartz and feldspar, regardless of the excavation slopes. However, the firing temperature of the bowls mostly ranges from 950 to 1,100 ℃. It is estimated that the bowls had formalized making techniques, owing to the similar material composition and firing technique regardless of the excavation slope. The flat cups with cover have similar texture and mineral phases, except their poorly sorted inclusions. However, the jar coffins contain not only fine-grained minerals but also medium-grained quartz, feldspar, and biotite, showing a relatively wide range of firing temperatures. According to the geochemical results of pottery by type, it is assumed that chemical compositions are classified into two groups: small pottery(bowl and falt cup with cover) and jar coffins. In conclusion, small potteries such as bowls and flat cups with cover were made by removing the heavy minerals from raw materials, whereas jar coffins were made by adding medium-grained minerals to raw materials to maintain and support their structures, despite the same source materials. In addition, it is presumed that pottery making proceeded by selecting the source materials, preparing according to their use and controlling the firing temperature and environment.

Characteristics of ZnO:Al thin films deposited with differentworking pressures (증착 압력에 따른 ZnO:Al 박막의 특성)

  • Kim, Seong-Yeon;Sin, Beom-Gi;Kim, Du-Su;Choe, Yun-Seong;Park, Gang-Il;An, Gyeong-Jun;Myeong, Jae-Min
    • Proceedings of the Materials Research Society of Korea Conference
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    • 2009.11a
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    • pp.49.2-49.2
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    • 2009
  • 투명전극은 디스플레이, 태양전지와 같은 광전자 소자에 필수적이며, 지금까지 개발된 재료 중에는 ITO가 가장 투명하면서 전기전도도가 높고 생산성도 좋기 때문에 투명전극의 재료로 사용하고 있다. ITO는 낮은 비저항(${\sim}10^{-4}{\Omega}cm$) 과 높은 투과율 (~85 %), 상대적으로 넓은 밴드갭 에너지 (3.5 eV) 의특성과 같이 뛰어난 전기적 광학적 특성에 반해서 높은 원자재 가격, 불안정한 공급량 등으로 인한 문제점이꾸준히 제기되고 있다. 따라서 $In_2O_3$:Sn, ZnO:Al, ZnO:Ga, ZnO:F, ZnO:B, TiN 등과 같은 물질들로대체하려는 연구가 활발하게 진행되고 있다. ZnO는 ITO보다원자재의 수급이 원활하기 때문에 원가가 낮으며, 상대적으로 낮은 온도에서도 제작이 가능하다. 또한 화학적으로 안정적이므로 ZnO에 Al, Ga 등의 3족 원소를 도핑함으로써 낮은 비저항의 박막 제작이 가능하고, ITO 박막과 비교하여 etching이 쉬우며 기판과의 접착성이 좋으며, sputtering 공정시 plasma 분위기에서의 안정성이 뛰어나고 박막증착율이 높기 때문에 투명전극으로 적합한 재료이다. 본 연구에서는 cylindrical type의 Aldoping된 ZnO single target을 사용하여 박막 증착 압력의 변화를 주어 유리기판 위에 DC sputtering을 하였다. Fieldemission scanning electron microscope (FESEM)을 통해 ZnO:Al 박막의 표면의 형상과 두께를 확인하였으며, X-ray diffraction (XRD) 분석을 통해 박막의 결정학적 특성을 관찰하였다. 투명전극용 물질로서 ZnO:Al 박막의 적합성 여부를 확인하기 위하여 Van der Pauw 방법을 이용하여 박막의 비저항, 전자 이동도, 캐리어 농도를 측정하였으며, 박막의 기계적 성질 및 표면 접착성을 확인하기 위하여 nano-indentaion 분석을 하였다. 또한 UV-vis spectrophotometer를 이용하여 ZnO:Al 박막의 투과율을 분석하여 투명전극으로의 응용 가능성을 확인하였다.

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Fluid-Structural Analysis of Circumference Pressurization type Butterfly Valve according to Pressurization Distance (원주가압형 극저온 버터플라이 밸브의 가압 길이에 따른 유동-구조 연성해석)

  • Kwak, Ki-Suk;Han, Dong-Seop;Han, Geun-Jo
    • Proceedings of the Korean Institute of Navigation and Port Research Conference
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    • 2010.04a
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    • pp.415-416
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    • 2010
  • Recently, development and using a range of natural gas is widening because anxiety of oil supply is increasing. Especially, around the world, development for Storage and transportation of natural gas is rapidly growing. On the other hand, in Korea because of technology loss for cryogenic part material, key component is rely on import. LNG and LPG are the future core of natural fuels. That are getting a lot of support and it have increased the frequency of use. So it should be associated with the development of technology. And key technology about design and manufacturing for cryogenic butterfly valve are secured. In this paper, we analyze the strength evaluation for circumference pressurization type cryogenic butterfly valve using the fluid-structure analysis.

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Development of Charging Container for Cutting Steel Plate and Evaluation of its Cutting Performance (강재 절단을 위한 장약용기의 개발과 절단 성능 평가)

  • Park, Hoon;Min, Gyeong-Jo;Cho, Sang-Ho;Suk, Chul-Gi
    • Explosives and Blasting
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    • v.36 no.2
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    • pp.10-18
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    • 2018
  • The shaped charge is used in explosive demolition of steel frame structure, but it was often not used because it was limited to use or impossible to supply at domestic and foreign. To solve this problem, we needed a device that could generate matal jets using industrial explosive. In this study, we made a charging container, which metal jets were generated when explosives were detonated. Cutting performance tests were carried out to evaluate the effect of cutting of a charging container on a steel plate of 25mm thickness. In addition, we compared the results between the numerical simulation of penetration process and cutting performance tests and then was evaluated a cutting performance for steel plates of 35mm and 70mm thickness.

An Evaluation of Cutting Performance for Cutting Structural Steel using Charging Container (장약용기를 이용한 강재 절단 성능 평가)

  • Park, Hoon;Noh, You-Song;Suk, Chul-Gi
    • Explosives and Blasting
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    • v.38 no.2
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    • pp.13-21
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    • 2020
  • The shaped charge was used in explosive demolition of a steel frame structure, but it was often not used because it was limited to use and impossible to supply at domestic and overseas. Existing linear shaped charge did not have sufficient cutting performance to cut steel frame structures with a huge scale and thick steel plate. To solve these problems, we produced a device that could generate metal jets using industrial explosives of high detonation velocity and pressure. In this study, we made a charging container of three types which applicable to explosive demolition of steel frame structures. The experiment of cutting performances was carried out to evaluate the effect of cutting of charging containers on the various thicknesses of the H-beam and steel plate. As a result of the experiment, sufficient cutting performance was confirmed.

휨 구조의 압전 마이크로-켄틸레버를 이용한 진동 에너지 수확 소자

  • Na, Ye-Eun;Park, Hyeon-Su;Park, Jong-Cheol
    • Proceedings of the Korean Vacuum Society Conference
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    • 2014.02a
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    • pp.476-476
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    • 2014
  • 서론: 저 전력 소모를 필요로 하는 무선 센서 네트워크 관련 기술의 급격한 발달과 함께 자체 전력 수급을 위한 진동 에너지 수확 기술에 대한 연구가 활발히 이루어지고 있다. 다양한 구조와 소재를 압전 외팔보에 적용하여 제안하고 있다. 그 중에서도 진동 기반의 에너지 수확 소자는 주변 환경에서 쉽게 진동을 얻을 수 있고, 높은 에너지 밀도와 제작 방법이 간단하다는 장점을 가지고 있어 많은 분야에 응용 및 적용 가능하다. 기존 연구에서는 2차원적으로 진동 에너지 수확을 위한 휜 구조의 압전 외팔보를 제안 하였다. 휜 구조를 갖는 압전 외팔보는 각각의 짧은 두 개의 평평한 외팔보가 일렬로 연결된 것으로 볼 수 있다. 하나의 짧고 평평한 외팔보는 진동이 가해지면 접선 방향으로 응력이 생겨 최대 휨 모멘텀을 갖게 된다. 그러므로 휜 구조를 갖는 외팔보는 진동이 인가됨에 따라 길이 방향과 수직 방향으로 진동한다. 하지만, 이 구조는 수평 방향으로 가해지는 진동에 대한 에너지를 수확하기에는 한계점을 가진다. 즉, 3축 방향에서 임의의 방향에서 진동 에너지를 수확하기는 어렵다. 본 연구에서는 3축 방향에서 에너지를 효율적으로 수확할 수 있도록 헤어-셀 구조의 압전 외팔보 에너지 수확소자를 제안한다. 제안된 소자는 길이 방향과 수직 방향뿐만 아니라 수평 방향으로도 진동하여 임의의 방향에서 진동 에너지를 수확할 수 있다. 구성 및 공정: 제안하는 소자는 3축 방향에서 임의의 진동을 수확하기 위해서 길이를 길게 늘이고 길이 방향을 따라 휘어지는 구조의 헤어-셀 구조로 제작하였다. 외팔보의 구조는 외팔보의 폭 대비 길이의 비가 충분히 클 때, 추가적인 자유도를 얻을 수 있다. 그러므로 헤어-셀 구조의 에너지 수확 소자는 기본적인 길이 방향, 수직방향 그리고 수평방향에 더불어 추가적으로 뒤틀리는 방향을 통해서 3차원적으로 임의의 주변 진동 에너지를 수확하여 전기적인 에너지로 생성시킬 수 있다. 제작된 소자는 높은 종횡비를 갖는 무게 추($500{\times}15{\times}22{\mu}m3$)와 길이 방향으로 길게 휜 압전 외팔보($1000{\times}15{\times}1.7{\mu}m3$)로 구성되어있다. 공정 과정은 다음과 같다. 먼저, 실리콘 웨이퍼 위에 탄성층을 형성하기 위해 LPCVD SiNx를 $0.8{\mu}m$와 LTO $0.2{\mu}m$를 증착 후, 각각 $0.03{\mu}m$$0.12{\mu}m$의 두께를 갖는 Ti와 Pt을 하부 전극으로 스퍼터링한다. 그리고 Pb(Zr0.52Ti0.48)O3 박막을 $0.35{\mu}m$ 두께로 졸겔법을 이용하여 증착하고 상부 Pt층을 두께 $0.1{\mu}m$로 순차적으로 스퍼터링하여 형성한다. 상/하부 전극은 ICP(Inductively Coupled Plasma)를 이용해 건식 식각으로 패턴을 형성한다. PZT 층과 무게 추 사이의 보호막을 씌우기 위해 $0.2{\mu}m$의 Si3N4 박막이 PECVD 공정법으로 증착되고, RIE로 패턴을 형성된다. Ti/Au ($0.03/0.35{\mu}m$)이 E-beam으로 증착되고 lift-off를 통해서 패턴을 형성함으로써 전극 본딩을 위한 패드를 만든다. 초반에 형성한 실리콘 웨이퍼 위의 SiNx/LTO 층은 RIE로 외팔보 구조를 형성한다. 이후에 진행될 도금 공정을 위해서 희생층으로는 감광액이 사용되고, 씨드층으로는 Ti/Cu ($0.03/0.15{\mu}m$) 박막이 스퍼터링 된다. 도금 형성층을 위해 감광액을 패턴화하고, Ni0.8Fe0.2 ($22{\mu}m$)층으로 도금함으로써 외팔보 끝에 무게 추를 만든다. 마지막으로, 압전 외팔보 소자는 XeF2 식각법을 통해 제작된다. 제작된 소자는 소자의 여러 층 사이의 고유한 응력 차에 의해 휨 변형이 생긴다. 실험 방법 및 측정 결과: 제작된 소자의 성능을 확인하기 위하여 일정한 가속도 50 m/s2로 3축 방향에 따라 입력 주파수를 변화시키면서 출력 전압을 측정하였다. 먼저, 소자의 기본적인 공진 주파수를 얻기 위하여 수직 방향으로 진동을 인가하여 주파수를 변화시켰다. 그 때에 공진 주파수는 116 Hz를 가지며, 최대 출력 전압은 15 mV로 측정되었다. 3축 방향에서 진동 에너지 수확이 가능하다는 것을 확인하기 위하여 제작된 소자를 길이 방향과 수평 방향으로 가진기에 장착한 후, 기본 공진 주파수에서의 출력 전압을 측정하였다. 진동이 길이방향으로 가해졌을 때에는 33 mV, 수평방향으로 진동이 인가되는 경우에는 10 mV의 최대 출력 전압을 갖는다. 제안하는 소자가 수 mV의 적은 전압은 출력해내더라도 소자는 진동이 인가되는 각도에 영향 받지 않고, 3축 방향에서 진동 에너지를 수확하여 전기에너지로 얻을 수 있다. 결론: 제안된 소자는 3축 방향에서 진동 에너지를 수확할 수 있는 에너지 수확 소자를 제안하였다. 외팔보의 구조를 헤어-셀 구조로 길고 휘어지게 제작함으로써 기본적인 길이 방향, 수직방향 그리고 수평방향에 더불어 추가적으로 뒤틀리는 방향에서 출력 전압을 얻을 수 있다. 미소 전력원으로 실용적인 사용을 위해서 무게추가 더 무거워지고, PZT 박막이 더 두꺼워진다면 소자의 성능이 향상되어 높은 출력 전압을 얻을 수 있을 것이라 기대한다.

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The development of conductive 10B thin film for neutron monitoring (중성자 모니터링을 위한 전도성 10B 박막 개발)

  • Lim, Chang Hwy;Kim, Jongyul;Lee, Suhyun;Jung, Yongju;Choi, Young-Hyun;Baek, Cheol-Ha;Moon, Myung-Kook
    • Journal of Radiation Protection and Research
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    • v.39 no.4
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    • pp.199-205
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    • 2014
  • In the field of neutron detections, $^3He$ gas, the so-called "the gold standard," is the most widely used material for neutron detections because of its high efficiency in neutron capturing. However, from variable causes since early 2009, $^3He$ is being depleted, which has maintained an upward pressure on its cost. For this reason, the demands for $^3He$ replacements are rising sharply. Research into neutron converting materials, which has not been used well due to a neutron detection efficiency lower than the efficiency of $^3He$, although it can be chosen for use in a neutron detector, has been highlighted again. $^{10}B$, which is one of the $^3He$ replacements, such as $BF_3$, $^6Li$, $^{10}B$, $Gd_2O_2S$, is being researched by various detector development groups owing to a number of advantages such as easy gamma-ray discrimination, non-toxicity, low cost, etc. One of the possible techniques for the detection is an indirect neutron detection method measuring secondary radiation generated by interactions between neutrons and $^{10}B$. Because of the mean free path of alpha particle from interactions that are very short in a solid material, the thickness of $^{10}B$ should be thin. Therefore, to increase the neutron detection efficiency, it is important to make a $^{10}B$ thin film. In this study, we fabricated a $^{10}B$ thin film that is about 60 um in thickness for neutron detection using well-known technology for the manufacturing of a thin electrode for use in lithium ion batteries. In addition, by performing simple physical tests on the conductivity, dispersion, adhesion, and flexibility, we confirmed that the physical characteristics of the fabricated $^{10}B$ thin film are good. Using the fabricated $^{10}B$ thin film, we made a proportional counter for neutron monitoring and measured the neutron pulse height spectrum at a neutron facility at KAERI. Furthermore, we calculated using the Monte Carlo simulation the change of neutron detection efficiency according to the number of thin film layers. In conclusion, we suggest a fabrication method of a $^{10}B$ thin film using the technology used in making a thin electrode of lithium ion batteries and made the $^{10}B$ thin film for neutron detection using suggested method.