• Title/Summary/Keyword: 접착공정

Search Result 247, Processing Time 0.023 seconds

A study on the manufacturing of motor case assembly for K-PSAM propulsion system by Trans. power molding(TPM) process (유동가압성형(TPM)을 이용한 휴대용 유도무기용 연소관 조립체 제작공정연구)

  • 정상기;윤남균
    • Journal of the Korean Society of Propulsion Engineers
    • /
    • v.2 no.3
    • /
    • pp.107-115
    • /
    • 1998
  • This paper deals with the study on injection with EPDM(Ethylene propylene dien ter polymer) the gap which narrow, long, and tubular between an ablative composite tube and a steel motor case. Small size motor assembly was designed and manufactured for man-portable air defense propulsion system. Motor assembly is consisted with steel tube, ablative composite tube and insulation rubber. Ablative composite tube was made of carbon/phenolic prepreg by rolling process and insulation rubber was made of EPDM by TPM(Trans-power molding) process. To select the insulation rubber material, we tested ablative insulation property and degradation property at first and we tested fluidity, adhesive property and hardness of EPDM rubber. Finally we designed TPM process to manufacture motor case assembly and the motor case assembly was examined by non-destructive test(X-ray).

  • PDF

Study for Synthesis and Properties of Polyurethane Based on Polyester Polyol with Varying Hydroxyl Values for Automotive Pre-painted Metal Sheet Applications (자동차 선도장 강판용 폴리에스테르 폴리올 기반 폴리우레탄의 합성과 물성에 대한 연구)

  • Kang, Choong Yeol;Lee, Jae Young;Noh, Seung Man;Nam, Joon Hyun;Park, Jong Myung;Jung, Hyun Wook;Yu, Sang Soo
    • Journal of Adhesion and Interface
    • /
    • v.12 no.1
    • /
    • pp.34-42
    • /
    • 2011
  • The roll coating process is well-known for completely replacement coating system with an existing wet paint process for automotive which has low productivity and is not environment-friendly process. It is very important to evaluate the curing behavior, corrosion resistance and processing property as well as rheological behavior in order to realize a film flexibility and hardness simultaneously. In this study, we have synthesized the polyester resin modified with hydroxyl values and molecular weight to apply the pre-painted system, and then evaluated the curing behavior, deep drawing, tensile strength and rheological properties. It was observed that N-0375-40 of 40 (mg KOH/mol) hydroxyl values showed the most suitable for flexibility, film hardness, and curing behavior.

Fabrication of Natural Fiber Composites through Hot Press and Analysis of Interfacial Adhesion (고온 프레스를 이용한 자연섬유 복합재료 제조와 계면 결합 분석)

  • Yi, Jin W.;Hwang, Byung S.;Lee, Jung H.;Nah, Chang W.
    • Journal of Adhesion and Interface
    • /
    • v.7 no.2
    • /
    • pp.26-31
    • /
    • 2006
  • In order to effectively improve interfacial adhesion strength between polypropylene (PP) and jute fiber, we particularly incorporated maleic anhydride grafted PP (MAPP) into the matrix through the environment-friendly process without an additional method of process and had better mechanical performances by providing the alignment into the natural fiber than those of the conventional fabrication technology such as an extrusion or injection molding. We also proposed hot pressing method which applied relatively low shear to the composites and confirmed the chemical bonds among the functional groups of MAPP and jute using FT-IR approach. The concentration of MAPP for maximum tensile strength and modulus was optimized at 3 wt%. Flexural properties had no noticeable tendency to increase with MAPP contents compared to tensile strength, which could probably be explained by the degree in wetting of PP/MAPP matrix.

  • PDF

Characterization of Core/Shell PMMA/CdS Nanoparticles Synthesized by Surfactant-free Emulsion Polymerization (무유화 유화중합에 의해 합성된 Core/shell 형태 PMMA/CdS 나노입자의 특성분석)

  • Yoon, Hyojung;Rhym, Young-Mok;Shim, Sang Eun
    • Journal of Adhesion and Interface
    • /
    • v.13 no.4
    • /
    • pp.188-192
    • /
    • 2012
  • Herein, CdS-coated PMMA nanoparticles were prepared by in-situ surfactant-free emulsion copolymerization and subsequent CdS coating process. As-prepared CdS/PMMA hybrid particles had 201.7 nm in diameter. The amount of CdS nanocrystals in the hybrid particles was 10.37 wt% determined by TGA and elemental analysis. The size of CdS crystals was 3.55 nm preferentially grown in (111) plane. UV-vis spectrum of PMMA/CdS nanoparticles showed the significant blue-shift in optical illumination. The reason was found because the synthesized CdS nanocrystals on PMMA particles had a different band gap energy of 2.70 eV which was significantly higher than that of known-value of bulk CdS (2.41 eV) due to a quantum confinement effect.

Synthesis of Hollow Mesoporous Carbon Nitride Spheres Using Polystyrene Spheres as Template (폴리스티렌 구형입자를 주형으로 이용한 할로우 메조포러스 질화탄소 구형입자의 합성)

  • Park, Sung Soo;Ha, Chang-Sik
    • Journal of Adhesion and Interface
    • /
    • v.15 no.2
    • /
    • pp.63-68
    • /
    • 2014
  • Hollow mesoporous carbon nitride material with sphere shape was synthesized using polystyrene sphere as template and cyanamide as nitrogen and carbon atom sources via thermal treatment process. The process of the silica removal is not necessary because silica as template is not in use for the synthesis of hollow mesoporous carbon nitride material and any solvents are also not in use. The size of polystyrene spheres was about 170 nm. Hollow diameter and wall thickness were 82 nm and 13 nm, respectively, in hollow mesoporous carbon nitride sphere. Surface area, mesopore size and pore volume of hollow mesoporous carbon nitride material was $188m^2g^{-1}$, 3.8 nm and $0.35cm^3g^{-1}$, respectively. The wall in hollow sphere has graphitic structure. Hollow mesoporous carbon nitride material has potential applications in the area of fuel cell, catalysis, photocatalysis, electroemmision device, etc.

Understanding Interfacial Charge Transfer Nonlinearly Boosted by Localized States Coupling in Organic Transistors (유기트랜지스터 내부 편재화 준위간 커플링에 의한 계면 전하이동의 비선형적 가속화 현상의 이해)

  • Han, Songyeon;Kim, Soojin;Choi, Hyun Ho
    • Journal of Adhesion and Interface
    • /
    • v.22 no.4
    • /
    • pp.144-152
    • /
    • 2021
  • Understanding charge transfer across the interface between organic semiconductor and gate insulator gives insight into the development of high-performance organic memory as well as highly stable organic field-effect transistors (OFETs). In this work, we firstly unveil a novel interfacial charge transfer mechanism, in which hole transfer from organic semiconductor to polymer insulator was nonlinearly boosted by localized states coupling. For this, OFETs based on rubrene single crystal semiconductor and Mylar gate insulator were fabricated via vacuum lamination, which allows stable repetition of lamination and delamination between semiconductor and gate insulator. The surfaces of rubrene single crystal and Mylar film were selectively degraded by photo-induced oxygen diffusion and UV-ozone treatment, respectively. Consequently, we found that the interfacial charge transfer and resultant bias-stress effect were nonlinearly boosted by coupling between localized states in rubrene and Mylar. In particular, the small number of localized states in rubrene single crystal provided fluent pathway for interfacial charge transport.

A Study on the Manufacturing and Properties of High Density Polyethylene Composites Filled with Waste Gypsum (부산 석고를 충전한 고밀도폴리에틸렌 복합재료 제조 및 물성 연구)

  • Jin, Woo Seok;Moon, Junho;Kong, Tae Woong;Kim, Hyang Tae;Choi, Sang Hwan;Oh, Jeong Seok
    • Journal of Adhesion and Interface
    • /
    • v.22 no.3
    • /
    • pp.106-110
    • /
    • 2021
  • Recently, research using waste among eco-friendly materials has been attracting attention. In this study, we investigated the physical properties of blends in which high density polyethylene (HDPE) was filled with waste gypsum (CaSO4) generated during fertilizer manufacturing. Composites were prepared by adding the gypsum content 0~20 wt% using a twin screw extruder. The mechanical, rheological, and thermal properties of the composites were evaluated. It was found that the tensile strength of the composites was less than 4.1% compared to that of unfilled HDPE, so there is no significant deterioration in physical properties. The thermal stability of the composites was improved as the gypsum content increased and the gypsum content had little effect on the viscosities of the composites.

PVP Hydrogel Coatings on Polypropylene Fibers using E-beam Irradiation (전자 빔을 이용한 폴리프로필렌 섬유의 PVP 하이드로젤 코팅)

  • Lee, Ji Eun;kwak, Hyo-Bin;Lee, Yong-Hyo;Kim, Kyung-Min;Lim, Jung-Hyurk
    • Journal of Adhesion and Interface
    • /
    • v.20 no.2
    • /
    • pp.66-70
    • /
    • 2019
  • The surface of hydrophobic polypropylene (PP) fibers (spun-bonded fabric) was treated by an atmospheric plasma treatment method. These pre-treated hydrophilic PP fabrics were dip-coated in the aqueous poly(N-vinyl pyrrolidone) (PVP) solution. PVP layers on the surface of PP fiber were crosslinked by an irradiation of electron beam. The thickness of PVP hydrogels coated on the surface was easily controlled by changing the concentration of PVP in coating solution. The stepwise surface treatment, PVP coating, and hydrogel formation via electron beam irradiation were analyzed by the measurement of contact angle, scanning electron microscopy, and optical microscopy.

A Study on Glass/Mo/ZnO/Glass Thin-film-heaters for Water Heating (수중 발열을 위한 Glass/Mo/ZnO/Glass 구조의 박막형 발열체 연구)

  • Kim, Jiwoo;Choi, Dooho
    • Journal of the Microelectronics and Packaging Society
    • /
    • v.29 no.1
    • /
    • pp.43-47
    • /
    • 2022
  • In this study, we demonstrated an eco-friendly thin-metallic-film-based heater which can be operated in water. Based on the materials stability, Mo was selected as the heating element to secure long-term stability. Using a magnetron sputtering, 40 nm-thick Mo layers were deposited onto a glass substrate, followed by the deposition of 60-nm-thick ZnO layer to prevent oxidation during the heater fabrication process. Then, PVB (Polyvinyl Butyral) was applied on top of ZnO layer and an additional glass substrate was placed, which were heated at 150℃ for 2 hr. The PVB was cured with strong adhesion by the processing condition. We operated the Glass/Mo/ZnO/Glass heater in water, and it was shown that the water temperature reached 50℃ within 2 minutes, with a minimal resistance change of the heater. Finally, the heaters exhibit a semi-transparency, and this aesthetic advantage is expected to contribute to the added value of the heater.

Chemical Vapor Deposition of High-Quality MoSe2 Monolayer and Its Application to van der Waals Heterostructure-Based High-Performance Field-Effect Transistors (화학기상증착법을 통한 고품질 단층 MoSe2합성 및 반데르발스 수직이종 접합 구조 기반 고성능 트랜지스터 제작)

  • Si Heon Lim;Sun Woo Kim;Seon Yeon Choi;Hyun Ho Kim
    • Journal of Adhesion and Interface
    • /
    • v.24 no.1
    • /
    • pp.36-40
    • /
    • 2023
  • A van der Waals material refers to a material having a two-dimensional layered structure composed of van der Waals bonds with weak interlayer bonding. The research based on heterojunction structures using such van der Waals two-dimensional materials has been steadily studied since the discovery of graphene. Herein, this paper reports a van der Waals heterojunction -based field-effect transistor device based on monolayer single crystalline MoSe2 grown by atmospheric pressure chemical vapor deposition. We found that MoSe2 grown under optimized process conditions did not have atomic-level defects and the transistor devices incorporating MoSe2 also showed excellent characteristics.