• Elastomers and Composites
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• v.41 no.4
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• pp.223-230
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• 2006

Rubber compounds have a high viscoelastic property. One of the viscoelastic behaviors during profile extrusion is the swelling of extrudate, and the amount of swelling varies with operational conditions in extrusion. It is well recognized that the elastic portion in the viscoelastic property plays an important role in the extrudate swell. In this study computer simulation of the die swell at the capillary die for several rubber compounds has been performed using commercial CFD code, Polyflow. A non-linear differential viscoelastic model, Phan-Thien-Tanner (PTT) model, was used in the computer simulation. Non-isothermal behavior was considered in the calculation. Distribution of pressure, velocity and temperature in the reservoir and capillary die, and extrudate profiles were predicted through the simulation. The amount of the die swell fur the different rubber compounds was investigated for various flow rates and three types of length to diameter of the capillary die. It is concluded that the PTT model successfully represented viscoelastic behavior of rubber compounds.

• The Korean Journal of Rheology
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• v.2 no.2
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• pp.19-27
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• 1990

레이저와 타이머장치를 설치한 낙구식 점도계에서 구와 니들이 주어진 구간을 통과 하는 시간을 측정하여 종말속도를 정확히 결정하였고 점성이 작은유체와 낮은 전단률 점성 과 영전단률 점성은 속이 빈 알루미늄 구와 니들이 이용하여 측정하였다. 알루미늄 구와 니 들의 속에 철분을 삽입하여 밀도를 다양하게 변화시켰다. 낙구식 점도계에서 측정한 낮은 전단률 점성과 영 전단률 점성 그리고 모세관점도계에서 측정한 높은전단률 점성과 무한 전 단률 점성을 이용하여 점탄성 유체의 특성이완시간을 결정하였다. 실린더 속의 시험용 유체 를 교란시키지 않고 밑면에 떨어진 구를 회수하는 장치를 설치하였다. 이 장치는 하나의 구 로써 점탄성유체의 특성확산시간을 측정하는데 대단히 효과적이었다. Polyacrylamide Separan AP-273 용액(농도 500-200 wppm)의 특성이안시간과 특성화산시간을 낙구식 점도 계와 모세관 점도계의 실험결과를 이용하여 결정하고 폴리며 용액의 퇴화 현상을 실험적으 로 분석하였다.

• The Korean Journal of Rheology
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• v.7 no.1
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• pp.60-67
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• 1995

EPDM/BR 블렌드의 물성에 미치는 커플링결합체의 영향을 조사하였다. N,N＇ -(bis(2-methyl-2-nitroprpyl))-1,6-diamino hexane) (MNPDH)와 bis(3-triethoxysilyl propyl)-tetrasulfide (TESPT)의 두가지 종류의 커플링결합제를 사용하였다. EPDM/BR 블 렌드 및 EPDM/BR/MNPDH 또는 EPDM/BR/TESPT 블렌드의 용융점도, 탄성률 및 tan $\delta$ 를 모세관 점도계, 동적점탄성장치 및 동적응력 완화측정장치로 조사하였다. 동적점탄성 및 형태학적 연구 결과 MNPDH 또는 TESPT를 첨가할 경우 결합고무 함량이 증가하고 카본 블랙의 분산성이 좋아져 가황된 EPDM/BR 블렌드의 인열강도 및 내피로성등의 물성이 향 상되었다.

• The Korean Journal of Rheology
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• v.3 no.1
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• pp.13-21
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• 1991

본연구에서는 단단한 구형 입자가 적은 변형속도에서 2차 유체로 간주될 수 있는 점탄성 용액의 disc-plate (비틀림)흐름에 놓였을 때의 측면 이동속도에 관하여 분석하였다. 이론적 계산을 통해 비틀림 유체 흐름에서 입자는 항상 중심쪽으로 이동하고 안쪽으로의 이 동속도의 크기는 유체의 성질과 흐름의 형태의 함수라는 것을 발견하였으며 이것은 2차 유 체에서 입자는 높은 전단속도 영역에서 낮은 전단속도 영역으로 이동된다는 예측과 일치한 다는 것을 알 수 있었다. 그러나 2차 유체 모델로 부터의 이결과는 이전연구자들에 의해 관 찰된 비틀림 유체 흐름에서의 바깥방향으로의 입자의 이동은 설명하지 못하였다.

• Elastomers and Composites
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• v.46 no.1
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• pp.54-59
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• 2011

One of the viscoelastic flow behaviors during profile extrusion is the swelling of extrudate. In this study, die swell of rubber compound in the capillary die have been investigated through experiment and computer simulation. Simplified viscoelastic model and non-linear differential viscoelastic model such as PTT model have been used in the computer simulation. The simulation results have been compared with experimental data. Experiment and simulation have been performed using fluidity tester and commercial CFD code, Polyflow respectively. Die swells predicted by two models showed good agreement with experimental results. Pressure and velocity distribution, and circulation flow at the corner of reservoir have been well predicted by PTT model. Simplified viscoelastic model can not predict circulation flow at the corner of reservoir. However this model has an advantage in computation time compare with full viscoelastic model, PTT model.

• 유체기계공업학회:학술대회논문집
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• 2005.12a
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• pp.825-828
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• 2005

Experimental and numerical study was done to confirm the effect of the flexible tube in pipeline on transient flow oscillation. Experiment was made for a pipeline with and without deformable flexible tube using a single pumping system of main stainless pipe. The wave speeds of main pipe and flexible tube were calculated from the pipe material properties, structures, and boundary conditions. Time dependent pressure fluctuations were calculated for the pipeline using the simple and the Kelvin-Voigt viscoelastic models for the deformation of main pipe and flexible tube. Pressure calculated by the Kelvin-Voigt viscoelastic model showed better agreement with measured one than pressure by the simple model. Experimental and numerical results show that the maximum pressure as well as amplitude of pressure oscillation was decreased by inserting short flexible tube in pipeline. Hence, inserted short flexible tube to pipeline was found to be effective for the suppression of strong pressure oscillation. Moreover, the wave speed in pipe was discussed based on numerical and experimental results.

• Journal of the Korean Society of Visualization
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• v.19 no.1
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• pp.81-87
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• 2021

Extensional flow of viscoelastic fluids is widely utilized in various industrial processes such as electrospinning, 3D printing and plastic injection molding. Extensional rheological properties, such as apparent viscosity and relaxation time, play an important role in the design and evaluation of the viscoelastic fluid-involved processes. In this work, we propose a lab-built capillary breakup extensional rheometer (CaBER) based on flow image processing to investigate the capillary breakup of polyethylene oxide (PEO) solution and its extensional rheological properties. We found that the apparent extensional viscosity and extensional relaxation time of the PEO solution are independent of the strike time. The proposed CaBER is expected to be applied to characterization of the extensional rheological properties of viscoelastic fluids at low cost with high precision.

• Transactions of the Korean Society of Mechanical Engineers
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• v.14 no.1
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• pp.241-250
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• 1990

Characteristic relaxation time and characteristic diffusion time of viscoelastic fluids are determined experimentally by measuring the zero-shear-rate viscosity by falling ball viscometer and the infinite-shear-rate viscosity by capillary tube viscometer. Fluids used in experiments are aqueous solutions of polyacrylamide Separan AP-273 and the polymer concentrations range from 300 to 2000 wppm. A newly designed laser beam and timer system is employed to overcome the difficulty in measuring terminal velocities of the low concentration solutions. Ball removal device is prepared to remove the dropped ball from the bottom of cylinder without disturbing the testing fluid. In order to measure the zero-shear-rate viscosity, densities of hollow aluminium balls are adjusted very close to the densities of testing fluids. Characteristic diffusion time, which is ball viscometer. However, terminal velocity of a needle by falling ball viscometer is not affected by the time interval of dropping needles and characteristic diffusion time is not measured with a dropping needle. Powell-Eyring model predicts the highest values of the characteristic relaxation times among models used for heat transfer experimental works for a given polymer solution. As degradation of a polymer solution continues, the zero-shear-rate viscosity decreases more seriously than the infinite-shear-rate viscosity. Characteristic relaxation times of polymer solutions decreases as degradation continues.

• Proceedings of the Korean Society of Rheology Conference
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• 2002.11a
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• pp.47-50
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• 2002

No Abstract, See Full Text

• Journal of the Korean Geotechnical Society
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• v.18 no.5
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• pp.55-65
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• 2002

Model tests were performed to investigate the mechanism of lateral earth pressure on a buried pipe, which was installed in a plastic flowing soil mass undergoing lateral movement. On the basis of failure mode tests, the equation of lateral earth pressure to apply Maxwell's visco-elastic model was proposed to consider the soil deformation velocity. Through a series of model tests of differential soil deformation velocity, lateral earth pressure of theoretical equation was compared with experimental results. When lateral soil movement was raised, the lateral earth pressure acting on buried pipe increases linearly with the soil deformation velocity. It shows that the lateral earth pressure on buried pipe is largely affected by soil deformation velocity. When plastic soil movement was raised, lateral earth pressure predicted by theoretical equation showed good agreement with experimental results. Also, coefficient of viscosity by theoretical equation had a good agreement with direct shear test results.