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금속중간층을 이용한 나노결정질 다이아몬드 박막 코팅

  • Na, Bong-Gwon;Myeong, Jae-U;Gang, Chan-Hyeong
    • Proceedings of the Korean Vacuum Society Conference
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    • 2013.02a
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    • pp.99-99
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    • 2013
  • 나노결정질 다이아몬드(Nanocrystalline Diamond: NCD) 박막은 고경도와 낮은 마찰계수를 가지고 있어 초경합금이나 고속도강과 같은 절삭공구 위에 코팅하여 공구의 성능 향상을 도모하려는 노력이 있어 왔다. 그러나 NCD 박막의 잔류응력이 크고, 초경합금과 철계 금속에 NCD가 증착되지 않는다는 문제점이 있다. 따라서 잔류응력 완화와 다이아몬드 핵생성을 위하여 제3의 중간층 재료가 필요하다. 본 연구에서는 W과 Ti을 중간층으로 하여 초경합금(WC-Co)과 고속도강(SKH51)에 NCD 박막을 코팅하고 기계적 특성을 비교하였다. 초경합금 또는 고속도강기판 위에 W 또는 Ti 중간층을 DC magnetron sputter를 이용해 각 1 ${\mu}m$의 두께로 증착하고 그 위에 MPCVD (Microwave Plasma Chemical Vapor Deposition)를 이용해 NCD 박막을 2${\mu}m$의 두께로 코팅하였다. FESEM을 이용하여 표면과 단면의 형상을 관찰하였고, XRD와 Raman spectroscopy를 통해 NCD 박막의 결정성을 확인하였다. 그리고 tribology test를 실시하여 코팅된 박막의 내마모성을 비교하였으며, Rockwell C indentation test를 이용하여 밀착력을 비교하였다. 초경합금에 적용 시, W이 Ti보다 중간층으로서 더 우수한 것으로 나타났으며 이는 열팽창계수 차이에 의한 잔류응력의 차이에 의한 것으로 여겨진다. 중간층 두께에 따른 박막의 기계적 특성 변화를 알아보기 위해 W 중간층의 두께를 1, 2, 4 ${\mu}m$로 변화를 주었다. 중간층 두께가 2 ${\mu}m$ 이상일 때 박막의 밀착력이 증가되는 것으로 나타났다. 고속도강 위에 같은 방법으로 1 ${\mu}m$의 W 또는 Ti 중간층 위에 2 ${\mu}m$의 NCD 박막을 코팅한 시편들은 초경합금에 코팅한 것과 달리 두 시편 모두 낮은 밀착력을 나타내었다. 열팽창계수 차이에 의한 잔류응력을 완화하기 위해 고속도강에 W/Ti 복합박막을 중간층으로 Ti, W순으로 각각 1 ${\mu}m$ 두께로 증착 후 그 위에 NCD 박막을 2 ${\mu}m$ 두께로 코팅 한 후 특성을 비교하였다. Ti/W 복합 중간층 위에 코팅된 NCD 박막의 밀착력이 W 혹은 Ti 단일 중간층에 코팅된 박막에 비해 우수한 것으로 나타났다. 그러나 실제 공구에 적용하기에는 박막의 밀착력 개선이 요구되며 이를 위해서 더 연구가 필요하다.

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Micropatterning on Biodegradable Nanofiber Scaffolds by Femtosecond Laser Ablation Process (펨토초 레이저 절삭 공정을 이용한 생분해성 나노섬유 표면 미세 패터닝 공정)

  • Chung, Yongwoo;Jun, Indong;Kim, Yu-Chan;Seok, Hyun-Kwang;Chung, Seok;Jeon, Hojeong
    • Journal of the Korean institute of surface engineering
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    • v.49 no.6
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    • pp.555-559
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    • 2016
  • A biodegradable nanofiber scaffolds using electrospining provide fibrous guidance cues for controlling cell fate that mimic the native extracellular matrix (ECM). It can create a pattern using conventional electrospining method, but has a difficulty to generate one or more pattern structures. Femtosecond(fs) laser ablation has much interested in patterning on biomaterials in order to distinguish the fundamental or systemic interaction between cell and material surface. The ablated materials with a short pulse duration using femtosecond laser that allows for precise removal of materials without transition of the inherent material properties. In this study, linear grooves and circular craters were fabricated on electrospun nanofiber scaffolds (poly-L-lactide(PLLA)) by femtosecond laser patterning processes. As parametric studies, pulse energy and beam spot size were varied to determine the effects of the laser pulse on groove size. We confirmed controlling pulse energy to $5{\mu}J-20{\mu}J$ and variation of lens maginfication of 2X, 5X, 10X, 20X created grooves of width to approximately $5{\mu}m-50{\mu}m$. Our results demonstrate that femtosecond laser processing is an effective means for flexibly structuring the surface of electrospun PLLA nanofibers.

Mathematical Theorem of Mode Acceleration Method (모우드 가속도법의 수학적 정리(定理))

  • 김태남
    • Journal of the Earthquake Engineering Society of Korea
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    • v.7 no.2
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    • pp.1-7
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    • 2003
  • Mode superposition method(MSM) is the most commonly used for solving linear response problems of structural dynamics. The major advantage of MSM is that usually a small number of lower mode is sufficient to analysis the response. However, the convergence is slow and many modes would be needed to give an accurate MSM in large structure with many degrees of freedom. The inaccuracies of MSM are caused by mode truncation in the solution. These demerits can be overcome by use of the mode acceleration method(MAM). Example analyses are carried out in simple beam subjected to harmonic loadings and compared the convergence of the joint displacements by the two methods. For relatively low frequency loadings, a good results was obtained by the lowest one mode in MAM, so the method is more economic in numerical analysis on an accurate solution.

Satellite Communication Microstrip Antenna for Tx/Rx Dual Operation at X-Band (X 대역 위성통신 송/수신 겸용 마이크로스트립 안테나)

  • Kim, Kun-Woo;Lee, Sung-Jae
    • The Journal of Korean Institute of Electromagnetic Engineering and Science
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    • v.25 no.2
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    • pp.164-171
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    • 2014
  • Transmit(Tx)/Receive(Rx) dual band operation microstrip array for X-band satellite communications are designed, fabricated, and measured in this paper. The microstrip array antenna has Right Handed Circular Polarization(RHCP) for Tx band and Left Hand Circular Polarization(LHCP) for Rx band. Two stacked patches are used for wideband characteristics and corner-truncated square patches are adopted for a circular polarization. To enhance bandwidth characteristics of a circular polarization, $2{\times}2$ sequential rotation array are applied. From the measured result, $8{\times}12$ microstrip array antennas have a good agreement with those of the simulation. Therefore the array antennas are applicable to military satellite communication antennas.

A Study on Seepage Cutoff Effect of the Environmentally Friendly SCM (SCM 친환경주입공법에 의한 차수 효과에 관한 연구)

  • Chun, Byung-Sik;Roh, Jong-Ryun;Jooi, Tae-Seong;Do, Jong-Nam
    • Journal of the Korean GEO-environmental Society
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    • v.6 no.4
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    • pp.65-71
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    • 2005
  • Recently, difficulties in soft ground improvement that caused by effectiveness of the ground improvement, the durability and environmentally friendliness of the injection material come to the fore. This paper studies the field applicability of the SCM in reinforcement and seepage cutoff of the back of an existing continuous wall. SCM uses double rod which imposes heavy pressure($10-100kgf/cm^2$) to disturbed, cut, discharge, and mix the ground. It is observed that a bulb is formed by using cement paste and environmentally friendly injection materials with minimal alkali leaching. Unconfined compression test and fish poison tests are performed. Test results indicate that the method results in higher durability, less leaching through use of the environmentally friendly injection material, and faster mobilization of the strength. In addition, field tests confirm the formation of the bulb and the seepage cutoff wall.

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The Infection Control of Dental Impressions (치과용 인상체의 감염 관리)

  • Lee, Jin-Han
    • Journal of Dental Rehabilitation and Applied Science
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    • v.29 no.2
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    • pp.183-193
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    • 2013
  • The characteristics of dental treatment makes the dental staff frequently contact with patient directly. Also the daily use of high-handpieces, sharp instruments, and needles often causes bleeding on oral cavity. Therefore, the risk of cross transmission grows up. The pathogen from dental practice could spread on not only the practice itself but also the dental laboratory with contaminated impressions and prosthesis. Dental clinic staffs (dentists, dental hygienists and dental technicians) should recognize all the patients have a possibility of cross contamination, and try to prevent the transmission of infection by proper infection control. In this study, we review the articles about disinfection methods and chemical infection agents used for dental impressions, and try to figure out the suitable and effective infection control system of dental impressions.

Fixed prostheses fabricated by direct metal laser sintering system: case report (Direct metal laser sintering 방식을 이용하여 제작한 다양한 고정성 보철물 수복 증례)

  • Baek, Ju-Won;Shin, Soo-Yeon
    • Journal of Dental Rehabilitation and Applied Science
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    • v.32 no.3
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    • pp.246-254
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    • 2016
  • Nowadays, 3 dimentional (3D) printing, especially Direct Metal Laser Sintering (DMLS) system is used in dentistry. DMLS system has recently been introduced for fabrication metal framework for metal ceramic crowns to overcome the disadvantages of the casting method and computer aided design/computer aided manufacturing (CAD/CAM) milling system. DMLS system uses a high-temperature laser beam to selectively heat a substructure metal powder based on the CAD data with the framework design. A thin layer of the beamed area becomes fused, and the metal framework is completed by laminating these thin layers. Utilizing DMLS system to fabricate fixed prostheses is expected to achieve free-from shaping without mold and limitations from cutting tools, fabricate prostheses with complex geometry, prevent distortion and fabrication defects that inherent to conventional fabrication methods. The purpose of this case report is to demonstrate various fixed prostheses such as long span fixed prostheses, post to achieve satisfactory results in functional and esthetic aspects.

Performance Comparisons of Wavelet Based T2-Test and Neural Network in Monitoring Process Profiles (공정프로파일 모니터링에서 웨이블릿기 반 T2-검정과 신경회로망의 성능비교)

  • Kim, Seong-Jun;Choi, Deok-Ki
    • Journal of the Korean Institute of Intelligent Systems
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    • v.18 no.6
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    • pp.737-745
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    • 2008
  • Recent developments of process and measurement technology bring much interest to the online monitoring of process operations such as milling, grinding, broaching, etc. The objective of online monitoring systems is to detect process changes as early as possible. This is helpful in protecting facilities against unexpected failures and then preventing unnecessary loss. This paper investigates, when the process monitoring data are obtained as a profile, the monitoring performances of a statistical $T^2$-statistic and a feedforward neural network by using a wavelet transform. Numerical experiments using cutting force data presented by Axinte show that the proposed wavelet based $T^2$-test has an acceptable power in detecting profile changes. However, its operating characteristic is very sensitive to autocorrelation. On the contrary, compared with $T^2$-test, the neural network has more stable performance in the presence of autocorrelation. This indicates that an adaptive feature to analyze noises should be incorporated into the wavelet based $T^2$-test.

Probabilistic Behavior of In-plane Structure due to Multiple Correlated Uncertain Material Constants (상호 상관관계가 있는 다중 재료상수의 불확실성에 의한 평면구조의 확률론적 거동)

  • Noh Hyuk-Chun
    • Journal of the Computational Structural Engineering Institute of Korea
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    • v.18 no.3
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    • pp.291-302
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    • 2005
  • Due to the importance of the parameter in structural response, the uncertain elastic modulus was located at the center of stochastic analysis, where the response variability caused by the uncertain system parameters is pursued. However when we analyze the so-called stochastic systems, as many parameters as possible must be included in the analysis if we want to obtain the response variability that can reach a true one, even in an approximate sense. In this paper, a formulation to determine the statistical behavior of in-plane structures due to multiple uncertain material parameters, i.e., elastic modulus and Poisson's ratio, is suggested. To this end, the polynomial expansion on the coefficients of constitutive matrix is employed. In constructing the modified auto-and cross-correlation functions, use is made of the general equation for n-th moment. For the computational purpose, the infinite series of stochastic sub-stiffness matrices is truncated preserving required accuracy. To demons4rate the validity of the proposed formulation, an exemplary example is analyzed and the results are compared with those obtained by means of classical Monte Carlo simulation, which is based on the local averaging scheme.

Influencing factors for abrasive flow rate and abrasive flow quality of abrasive injection waterjet systems for tunnel excavation (터널굴착용 투입형 연마재 워터젯 시스템의 연마재 투입량과 유동성에 미치는 영향 인자)

  • Joo, Gun-Wook;Oh, Tae-Min;Cho, Gye-Chun
    • Journal of Korean Tunnelling and Underground Space Association
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    • v.16 no.4
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    • pp.417-430
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    • 2014
  • A new rock excavation method using an abrasive waterjet system is under development for efficiently creating tunnels and underground spaces in urban areas. In addition, an appropriate abrasive flow rate and abrasive flow quality are important for the new rock excavation (cutting) method using an abrasive waterjet system. This study evaluated the factors influencing the abrasive flow rate and abrasive flow quality, specifically the abrasive pipe height, length, tortuosity and inner diameter, through experimental tests. Based on the experimental test results, this study suggested optimal conditions for the abrasive flow rate and abrasive flow quality. The experimental results can be effectively utilized as baseline data for rock excavation methods using an abrasive waterjet system in various construction locations such as tunnels near urban surroundings, utility tunnels, and shafts.