• Title/Summary/Keyword: 적외선분광

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Lacquer Manufacturing Method for the Wooden Coffins of King Muryeong's Tomb based on the Scientific Analysis (과학적 분석방법을 이용한 무령왕릉 목관재의 옻칠 기법 연구)

  • Kim, Soo-Chul;Lee, Gwang-Hee;Kang, Hyung-Tae;Shin, Seong-Phil;Han, Min-Soo
    • Journal of Conservation Science
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    • v.26 no.3
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    • pp.247-258
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    • 2010
  • We conducted optical microscopy, infra-red spectroscopy and SEM-EDS analysis of the lacquer layers on the wooden coffins excavated from King Muryeong's Tomb. We found four varnishing methods according to the sub-materials of lacquer layers: The lacquer of wooden coffins with black paint layer on the surface were classified with two groups; single layer and three layers. The lacquer of wooden coffins without black paint layer on the surface were classified with two groups; single layer and two layers. IR spectra of the laquer were same as those of the oriental laquer. The SEM-EDS analysis showed that the lacquer layers were mixed with iron, copper and calcium.

Characteristic Analysis of Paint used in Defense Industries Equipments of Korean Conflict in The War Memorial of Korea (전쟁기념관 소장 6·25전쟁 방산장비의 도료 특성 분석)

  • Kang, Hyun Sam;Kim, Soo Chul;Park, Min Soo
    • Journal of Conservation Science
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    • v.32 no.2
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    • pp.215-221
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    • 2016
  • This study conducted analysis of paint samples from defense industries equipments of Korean Conflict in The War Memorial of Korea to identify the characteristics of the modern paint. The samples were analyzed by microscopic observation, infrared spectroscopy and SEM-EDS. Cross-section of paint samples are made up of several layers of about 9 to 20 times, and thickness of the layer is not uniform in the $10{\sim}100{\mu}m$. The putty was used for the surface treatment before painting. Inorganic analysis showed that one type of the putty consist of minium and kaolin, talc, titanium dioxide. According to the results of infrared spectroscopy, paint samples were identified as alkyd resin. Some bands such as C-H bending, C-O and C-C stretching, C-H rocking were found in spectra.

Introduction of Korea Oil Identification System(KOIS) (우리나라의 해상유출물질 감식.분석기법 연구)

  • Lee, Y.S.;Lee, S.J.;Kim, C.S.;Oh, H.J.;Kim, H.G.
    • Proceedings of KOSOMES biannual meeting
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    • 2006.05a
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    • pp.85-92
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    • 2006
  • Crude oil is complex mixture if thousands of different organic compound formed from a variety of organic materials that are chemically converted under differing geological conditions over long periods of time. Also oil composition varies according to crude source, refining, processing, handling and storage. The oil fingerprint method is application if specific knowledge of petrochemicals and use if sophisticated analytical equipment and techniques to identify the source(s) if oil pollution. KCG currently utilizes four primary analytical techniques: Gas Chromatography (GC), Fluorescence Spectroscopy(FL), Infrared Spectroscopy(IR) and Gas Chromatography mass spectrometer(GC/MS). Of all these techniques, GC technique are most widely used Gas Chromatography is used as a primary analytical method because high reliableness, high separating efficiency and repeatability.

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Effect of Combined Environmental Factors on Adhesive Shear Strengths and Chemical Structures of Adhesives (복합적 환경인자의 영향에 의한 접착제의 접착전단강도 및 화학구조 변화)

  • Hwang, Young-Eun;Yoon, Sung-Ho
    • Composites Research
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    • v.24 no.1
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    • pp.31-36
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    • 2011
  • Adhesive shear strengths of the established adhesives and the alternative adhesives were evaluated and their chemical structures were analyzed in order to investigate the possibility of replacing the established adhesives with the alternative adhesives applicable to the seeker for the guided missiles. Two types of the adhesives such as the structural adhesives and the sealant adhesives were considered. Those adhesives were exposed to the combined environmental factors consisting of temperature, moisture and ultraviolet over 1000 hours. Adhesive shear test was conducted to evaluate adhesive shear strengths and ATR FT-IR was utilized to investigate chemical structures. According to the results, the adhesive shear strengths of the alternative adhesives revealed higher than those of the established adhesives. Also the alternative adhesives were more stable to the combined environmental condition than the established adhesives. Therefore, it is found that the established adhesives were able to be replaced by the alternative adhesives.

Mineralogy and Genesis of Manganese Ores from the Eosangcheon Mine, Korea (어상주광산(魚上川鑛山)의 망간광석(鑛石)에 대(對)한 광물학적(鑛物學的) 및 성인적연구(成因的硏究))

  • Kim, Soo Jin;Kim, Seong Hoon
    • Economic and Environmental Geology
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    • v.15 no.4
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    • pp.205-219
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    • 1982
  • The Eosangcheon manganese ore deposits occur as supergene weathering deposits along quartz porphyry dikes developed in the Ordovician Heungweolri dolomite and Samtaesan limestone formations. The manganese ores are composed of manganese oxide minerals and associated other minerals. Rancieite and todorokite are abundantly found, and birnessite, nsutite, pyrolusite and chalcophanite are found in minor quantities. Associated other minerals are calcite, gypsum, goethite, lepidocrosite, quartz, and sericite. Microscopic, chemical, X-ray powder diffraction, infrared absorption spectroscopic and differential thermal analyses have been made for manganese oxide minerals and associated other minerals. The relationship of birnessite and rancieite was studied by means of X-ray powder diffraction and infrared absorption spectroscopic analyses. It is assumed that these minerals are closely related to each other in crystal structure, but separate species. The manganese oxide minerals were formed mainly by replacement, precipitation from solution, and recrystallization in the supergene weathering environment. The trend of formation of manganese oxide minerals is: (Rhodochrosite)-(todorokite)-(birnessite, rancieite)-(nsutite, pyrolusite, chalcophanite).

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Infrared Spectroscopy and Differential Scanning Calorimetry of Silk Fibroin/Hyaluronic Acid Blend Film (견피브로인/히아론산 브렌드 필름의 적외선 분광 분석 및 시차열분석)

  • Kweon HaeYong;Lee Kwang-Gill;Yeo Joo-Hong;Woo SoonOk;Han SangMi;Lee Yong Woo;Lee Jang Hern;Park Young Hwan
    • Journal of Sericultural and Entomological Science
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    • v.46 no.1
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    • pp.28-31
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    • 2004
  • Bombyx mori silk fibroin/hyaluronic acid blend films were prepared by mixing aqueous solution of B. mori silk fibroin and hyaluronic acid. According to the FTIR spectra, no interaction between silk fibroin and hyaluronic acid was found. The conformation of silk fibroin in blend films was changed from random coil to $\beta$-sheet structure by treatment of EDC ethanol solution. Thermal degradation peak of silk fibroin and hyaluronic acid was also not altered by blending each other. The average swelling ratio of silk fibroin/hyaluronic acid blend films was 70. Therefore, silk fibroin/hyaluronic acid blend films might be one of possible wound dressing materials.

과학기술위성3호 사용자를 위한 관측요청 및 관측데이터 인터페이스

  • Lee, Seung-Heon;Son, Jun-Won;Park, Jong-O;Chae, Tae-Byeong;An, Sang-Il;Lee, Seung-U;Lee, Cheol
    • The Bulletin of The Korean Astronomical Society
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    • v.37 no.2
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    • pp.190.1-190.1
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    • 2012
  • 과학기술위성3호는 170kg의 소형위성으로 2006년 사업을 착수하였으며, 올 2012년 12월에 러시아에서 발사할 예정이다. 주탑재체는 다목적 적외선 영상시스템 (MIRIS, Multi-Purpose IR Imaging System)으로 천문연에서 개발을 담당하였으며 우주관측과 지구관측을 수행한다. 우주관측은 $0.9-2{\mu}m$ 대역을 관측에서 은하면의 근적외선 방출광을 탐사하여 우리은하 고온가스의 기원 및 성간 난류의 물리적 특성을 연구한다. 또한 황도극지방을 추가로 관측하여 적외선 우주배경복사의 기원의 연구에 활용될 것이다. 지구관측은 $3-5{\mu}m$의 파장대역으로 한반도의 재해 및 환경변화의 연구에 활용될 예정이다. 부탑재체는 소형영상분광기 (COMIS, Compact Imaging Spectrometer)로 공주대에서 개발을 하였으며 $0.4-1.05{\mu}m$ 파장대역의 지표면 분광영상의 획득이 주요 임무이다. 소형영상분광기를 위하여 다양한 관측방법 (Strip, Stereo, Slow Skew)을 시도하며, 관측된 분광영상은 수질, 작황, 황사, 근해 환경변화 등 다양한 분야에 활용될 것으로 기대한다. 우주관측임무는 확정되어 주어진 임무기간동안 정해진 일정대로 우주관측을 수행되며, 지구관측임무는 사용자의 요구에 따라 관측지역 및 관측 횟수가 추후에 결정될 것이다. 과학기술위성3호는 기술적으로 기존 과학기술위성 시리즈 보다 향상된 위성체, 탑재체 시스템으로 주어진 우주 및 지구과학 임무를 성공적으로 수행할 것으로 예상되며, 또한 우주 및 지구과학의 연구를 위해 여러 분야에서 활동하는 국내 사용자의 적극적인 참여도 기대하고 있다. 본 발표에서는 다양한 사용자의 관측요청 접수를 위한 지상관제시스템의 설명과 임무관측을 통해 획득된 관측데이터의 전달 방법에 대해 논의한다.

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The Effects of Precursor on the Formation and Their Properties of Spin-on Dielectric Films Used for Sub-50 nm Technology and Beyond (50 nm 이상의 CMOS 기술에 이용되는 Spin-on Dielectric 박막 형성과 그 특성에 미치는 전구체의 영향)

  • Lee, Wan-Gyu
    • Journal of the Korean Vacuum Society
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    • v.20 no.3
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    • pp.182-188
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    • 2011
  • Polysilazane and polymethylsilazane based precursor films were deposited on Si-substrate by spin-coating, subsequently annealed at $150{\sim}850^{\circ}C$, and characterized. Structural analysis, shrink, compositional change, etch rate, and gap-filling were observed. Annealing the precursor films led to formation of spin-on dielectric films. C-containing precursor films showed that less loss of N, H, and C while less gain of O than that of C-free precursor films at $400^{\circ}C$, but more loss of N, H, and C while more gain of O at $850^{\circ}C$. Thus polysilazane based precursor films exhibited less reduction in thickness of 14.5% than silazane based one of 15.6% at $400^{\circ}C$ but more 37.4% than 19.4% at $850^{\circ}C$. FTIR indicated that C induced smaller amount of Si-O bond, non-uniform property, and lower resistance to chemical etching.

Research about Multi-spectral Photographing System (PKNU No.2) Development (다중영상촬영을 위한 PKNU 2호 개발에 관한 연구)

  • 최철웅;김호용;전성우
    • Korean Journal of Remote Sensing
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    • v.19 no.4
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    • pp.291-305
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    • 2003
  • The cost of deploying Geological and Environmental information gathering systems, especially when such systems obtain remote sensing and photographic data through the use of commercial satellites and aircraft. Besides the high cost equipment required, adverse weather conditions can further restrict a researcher's ability to collect data anywhere and anytime. To mitigate this problem, we have developed a compact, multi-spectral automatic Aerial photographic system. This system's Multi-spectral camera is capable of the visible (RGB) and infrared (NIR) bands (3032*2008 pixel). It consists of a thermal infrared camera and automatic balance control, and can be managed by a palm-top computer. Other features includes a camera gimbal system, GPS receiver, weather sensor among others. We have evaluated the efficiency of this system in several field tests at the following locations: Kyongsang-bukdo beach, Nakdong river (at each site of mulkeum-namji and koryung-gumi), and Kyungahn River. Its tested ability in aerial photography, weather data, as well as GPS data acquisition demonstrates its flexibility as a tool for environmental data monitoring.

Effect of ethanol concentration on the infrared spectroscopic characteristics of silk beads (알코올의 농도에 따른 실크 비드의 적외선 분광 특성)

  • Kim, Sung-Kuk;Jo, You-Young;Lee, Kwang-Gill;Kim, Kee-Young;Kim, Hyun-bok;Kweon, HaeYong
    • Journal of Sericultural and Entomological Science
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    • v.53 no.2
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    • pp.118-123
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    • 2015
  • The structural transition of silk protein has been induced by various method including alcohol treatment. To know the effect of alcohol concentration on silk beads conformation, silk beads were prepared in different alcohol concentration (100%, 70%, and 50%) and then examined the infrared spectra of silk beads. Silk beads prepared in 100% alcohol showed at $1265cm^{-1}$ attributed ${\beta}-sheet$ conformation and did not showed a characteristic absorption peak from model drug. However, silk beads in 70% and 50% alcohol showed some peaks originated from model drug including $2933cm^{-1}$, $1069cm^{-1}$, and $973cm^{-1}$. These results means that the micro-environment of silk beads was affected by alcohol concentration.