• Title/Summary/Keyword: 재질분석

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The Preliminary Study on the Quantitative Analysis of Quarts by Fourier Transform Infrared Spectrophotometric Direct on Filter(FTIR-DOF) Method -Effects of filter materials, inhomogeneity of deposition, and humidity- (Fourier Transform Infrared Spectrophotometric Direct on Filter 방법을 이용한 석영 분석의 기초 연구 - 필터재질, 비균일 침착 및 습도의 영향 -)

  • Phee, Young Gyu;Kim, Hyunwook
    • Journal of Korean Society of Occupational and Environmental Hygiene
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    • v.15 no.1
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    • pp.1-7
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    • 2005
  • Although the Fourier Transform Infra-Red spectrophotometric Direct on Filter(FTIR-DOF) method is a useful analytical technique for quantifying quartz content in respirable dust samples, a number of analytical problems must be taken into consideration such as, to name only a few, inhomogeneous deposition of particles, level of environmental humidity, uneven surface of the filter, and interfering minerals in the sample. This study was designed to select the most suitable wavelength and proper filter material for the method, and to investigate effects of humidity and inhomogeneous deposition of particles on the filter. Samples of respirable dust, created in a dust chamber containing standard material of quartz, were collected using a cyclone equipped with a 25mm filter as a collection medium. The results were as follows; 1. Among seven (7) commercially available filters tested for the FTIR-DOF method, the DM 800 filter showed the best analytical performance having the lowest background absorbance bands and no overlapping peaks at 799, 779, and $695cm^{-1}$. 2. The variations of absorbance due to humidity ranged from 1.0% to 3.3% for $799cm^{-1}$, 1.0% to 3.3% for $779cm^{-1}$, and 8.9%~20.9% for $695cm^{-1}$ peaks, respectively. The $699cm^{-1}$ peak was proved to be most vulnerble to environmental humidity for quantitative analysis of quartz. 3. As for effects of inhomogeneous deposition of samples, the highest variation of absorbance of 10.9% ($13.5{\mu}g$) was observed when using the 695cm-1. The variations of absorbance from the other two peaks, 799 and $779cm^{-1}$, ranged from 1.2 to 3.2%, and 1.4 to 4.1%, respectively. Therefore, the $799cm^{-1}$ peak was considered to be most reliable for quantitative analysis of quartz. The results of this study suggest that, for quantitative analysis of quartz in the respirable dust samples, use of the $799cm^{-1}$ peak can minimize the influence of environmental humidity and inhomogeneous deposition of particles on the filter. The FTIR-DOF method, if adopted for routine analysis of quartz in the respirable dust samples, could save sample preparation time and efforts substantially and also could increase analytical throughputs. Since use of the $799cm^{-1}$ peak is prone to be affected by interferences in the sample, further research on minimizing the effects is needed.

Effects of anaerobic sealing agents on preload maintenance of screw-retained implant prosthesis with surface of screws (임플란트 보철물 나사의 전하중 유지에 나사 표면에 따른 혐기성 나사 고정제의 효과)

  • Ryu, Seung-Beom;Heo, Seong-Joo;Koak, Jai-Young;Kim, Seong-Kyun
    • The Journal of Korean Academy of Prosthodontics
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    • v.58 no.2
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    • pp.103-109
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    • 2020
  • Purpose: The purpose of this study was to evaluate the preload maintenance of the retaining screw when using anaerobic sealing agents in implant fixture and abutment components. Specifically, the study examines the effects of anaerobic sealing agents on different types of screws. Materials and methods: External hexagon implants made of titanium and anti-rotational abutments were used. Titanium abutment screws and ebony abutment screws from the same manufacturer were used. The experiment was divided into four groups (n = 10 in each group). In the control group, no sealing agent was used at the implant fixture and abutment screw interface. All abutment screws were tightened according to the manufacturer's recommended torque (30 N.cm). After 24 hours, the removal torque (detorque) of each screw was measured using a digital torque gauge device. The data were analyzed by two-way ANOVA test according to normality distribution satisfaction. Results: Looking at the results for each group, titanium screws and no treatment showed detorque values of 20.3 ± 1.6 N.cm. titanium screws and applied anaerobic sealing agent showed detorque values of 32.4 ± 6.7 N.cm. Ebony screws and no treatment showed detorque values of 20.2 ± 1.5 N.cm. ebony screws and applied anaerobic sealing agent showed detorque values of 30.4 ± 4.5 N.cm. Conclusion: The detorque value was higher in the case of using anaerobic sealing agents in both the titanium screw and ebony screw groups. But there was no difference between the two screws.

The Status of Contact Lens Wearing, Management and Eye Health Awareness Among Female University Students in Jeju Area (제주지역 여대생들의 콘택트렌즈 착용 및 관리 실태와 눈건강 인식)

  • Choi, Ji Young;Song, Yun Young;Byun, Jong Chul
    • Journal of Korean Ophthalmic Optics Society
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    • v.21 no.3
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    • pp.203-214
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    • 2016
  • Purpose: The purpose of this study is to analyze the status of contact lens wearing, management and awareness of eye health knowledge among female university students in Jeju area and to utilize the basic data for education and management of contact lens. Methods: Data for this study were collected from the 236 female university students in Jeju area who have a contact lens experience from May 1, 2016 to June 11, 2016. Results: We found the status of contact lens wearing and management of subjects and there were different correlations between discomfort and awareness of eye health knowledge among the subjects who have different characteristics. There were also correlations in discomfort, the average days of contact lens wear per week, initial wearing day and action when they have any discomfort in some contact lens wearers. Conclusions: We realized the status of contact lens wearing and management of female university students and it suggests appropriate contact care education and sustainable management system are need to be established for considering daily average wearing time, the type and material of contact lens wear and main discomfort and so on.

Detection of Thermal Ratcheting Deformation for Cylindrical Shells by Ultrasonic Guided Wave (유도초음파를 이용한 원통형 쉘의 열 라체팅 변형 탐지)

  • Joo, Young-Sang;Lee, Hyeong-Yeon;Kim, Jong-Bum;Park, Chang-Gyu;Lee, Jae-Han
    • Journal of the Korean Society for Nondestructive Testing
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    • v.26 no.5
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    • pp.297-305
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    • 2006
  • The thermal ratcheting deformation at the reactor baffle and upper internal structure of the liquid metal reactor (LMR) can occur due to movement of the hot sodium free surface. In in-service inspection of reactor internals of LMR, a new inspection technique should be developed for the detection of the thermal ratcheting damage. In this study, an inspection technique using ultrasonic guided wave is proposed for the detection of the thermal ratcheting damage of cylindrical vessels. A 316L stainless steel cylindrical shell specimen has been prepared. The thermal ratchet structural tests were cyclically performed by heat-up up to $550^{\circ}C$ with steep temperature gradients along the axial direction after cool-down by cooling water. Ultrasonic guided wave propagation has been characterized by analysis of dispersion curve of the stainless steel plate. The zero-order antisymmetric $A_0$ guided wave has been selected as the optimal mode for detection of the ratcheting deformation. It is confirmed that the thermal ratcheting deformation can be detected by the measurement of transit time difference of circumferentially propagated $A_0$ guided waves.

A Study on Electrical Characteristics for Coil Winding Number Changes of Eddy Current Bobbin Coil for Steam Generator Tubes in NPPs (원전 증기발생기 전열관 와전류검사용 보빈코일의 권선 수 변화에 대한 전기적 특성 연구)

  • Nam, Min-Woo;Kim, Cheol-Gi
    • Journal of the Korean Society for Nondestructive Testing
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    • v.32 no.1
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    • pp.64-70
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    • 2012
  • Two kinds of eddy current probes are mainly used to perform the steam generator tube integrity assesment in NPPs. The first one is the bobbin probe using for inspection of volumetric defect like a fretting wear. The second one is the rotating probe using for inspection of non-volumetric defect like a crack. The eddy current probe is one of the essential components which consist of the whole eddy current examination system, and provides a decisive data for the tube integrity in accordance with acceptance criteria described in specific procedures. The design of ECT probe is especially important to improve examination results because the quality of acquired ECT data is depended on the probe design characteristics, such as coil geometry, electrical properties, operation frequency. In this study, it is analyzed that the coil winding number of differential bobbin probe affects the electrical properties of the probe. Eddy current bobbin probes for the steam generator tubes in NPPs are designed and fabricated according to the results. Experiment shows that the change in coil winding number has much effects on the optimum inspection frequency determined by the tube geometry and material. Therefore, the coil winding number in bobbin probe is very important in the probe design. In this study, a basis of the coil winding number for the eddy current bobbin probe design for steam generator tubes in NPPs is established.

Fundamental Heat Analysis about the Thermoelectric Generation System Using the Waste Heat of Exhaust Gas from Ship (선박의 배기가스 폐열을 활용한 열전발전시스템에 관한 기초 열해석)

  • Kim, Myoung-Jun;Ga, Gwang-Jin;Chea, Gyu-Hoon;Kim, In-Seup
    • Journal of the Korean Society of Marine Environment & Safety
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    • v.22 no.5
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    • pp.583-592
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    • 2016
  • IMO (International Maritime Organization) in the UN (United Nations) set up that aim at reducing $CO_2$ emission from ship by up to 30 percent until 2030. The final purpose of this study is the development of marine thermoelectric generation system using waste heat from vessel of internal combustion engines. Before the development of marine thermoelectric generation system, this paper carried out the fundamental heat analysis of marine thermoelectric generation system. It was able to obtain the valuable results about the efficiency improvement of the thermoelectric generation system. The results is as follows : 1) It was confirmed that the efficiency of thermoelectric generation system improves to 8.917 % with increasing the temperature difference of peltier module by reducing the temperature difference between peltier module and heat source at the hot side. 2) System efficiency according to change in the external load resistance was confirmed that the change width of about 6 % which does not significantly occur. 3) System efficiency in the case stainless steel at the same condition is 8.707 %. System efficiency could be confirmed that the stainless steel is higher than duralumin (8.605 %), copper (8.607 %).

Numerical Fatigue Life Prediction of IGBT Module for Electronic Locomotive (수치해석을 이용한 전동차용 IGBT 모듈의 피로 수명 예측)

  • Kwon, Oh Young;Jang, Young Moon;Lee, Young-ho;Choa, Sung-Hoon
    • Journal of the Microelectronics and Packaging Society
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    • v.24 no.1
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    • pp.103-111
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    • 2017
  • In this study, the thermomechanical stress and fatigue analysis of a high voltage and high current (3,300 V/1200 A) insulated gate bipolar transistor (IGBT) module used for electric locomotive applications were performed under thermal cycling condition. Especially, the reliability of the copper wire and the ribbon wire were compared with that of the conventional aluminum wire. The copper wire showed three times higher stress than the aluminum wire. The ribbon type wire showed a higher stress than the circular type wire, and the copper ribbon wire showed the highest stress. The fatigue analysis results of the chip solder connecting the chip and the direct bond copper (DBC) indicated that the crack of the solder mainly occurred at the outer edge of the solder. In case of the circular wire, cracking of the solder occurred at 35,000 thermal cycles, and the crack area in the copper wire was larger than that of the aluminum wire. On the other hand, when the ribbon wire was used, the crack area was smaller than that of the circular wire. In case of the solder existing between DBC and base plate, the crack growth rate was similar regardless of the material and shape of the wire. However, cracking occurred earlier than chip solder, and more than half of the solder was failed at 40,000 cycles. Therefore, it is expected that the reliability of the solder between DBC and base plate would be worse than the chip solder.

The Research about Efficient Control of the Territorial Base Point (영해기준점의 효율적 유지관리 방안에 관한 연구)

  • Choi, Yun-Soo;Kim, Jae-Myeong;Yun, Chang-Beom
    • Spatial Information Research
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    • v.18 no.1
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    • pp.39-48
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    • 2010
  • Recently, many countries are promoting the rapid development of marine for securing territorial sea. The importance of territorial sea has being emphasized as territorial disputes among countries has been increasing. The South Korea should be encouraged to expand the territory due to territorial disputes with neighborhood countries. The purpose of this study is to derive a improvement plan for the efficient control of the territorial base point through analyzing the existing territorial base point and checking the territorial base point. Therefore, we proposed a variety of new plans for accurate positioning by sea level observation and MBES, reduced the surveying procedure through analyzing the existing territorial base points and provided a basis for the territorial base points which can be the 2nd grade national control points by improving a grade. We also suggested that the territorial base points and sub-territorial base points' database should be given standardized number for increasing the efficient management of other national control points and territorial base points. Finally, we suggested a improved work regulation about analysis and maintenance for territorial base points, the information activity of territorial base points and the new plan of community relations. This study will be a basis for the foundation of maritime territory which could be superior to other countries and the expansion of maritime territory.

Catch and cluster analysis according to net materials of gillnet for the Pacific herring in the coastal waters of Samcheok, Korea (삼척 연안 청어자망의 그물 재질에 따른 어획과 군집 분석)

  • AN, Heui-Chun;BAE, Jae-Hyun;PARK, Jong-Myung;HONG, Sung-Eic;KIM, Seong-Hun;PARK, Hae-Hoon
    • Journal of the Korean Society of Fisheries and Ocean Technology
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    • v.51 no.3
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    • pp.348-354
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    • 2015
  • Experiments for catch and cluster analysis on the catch by gillnet for the Pacific herring were conducted using traditional nylon net (PA) and developing biodegradable net (PBS) with different monofilaments of #2 (=0.23 mm) and #3 (=0.28 mm) in diameter between 2011 and 2012, and of #2, #2.5 and #3 in 2013 in the eastern coastal waters of Samcheok, Korea. The total catch during the experiments was 3,337kg in weight and 16,757 individuals in number. Though the catch ratio of the Pacific herring in 2011 and 2012 was 97.4% and 98.7%, respectively, that of the Pacific herring in 2013 was 73.6% as the biggest and followed by goldeye rockfish (8.6%), black edged sculpin (8.4%), atka mackerel (7.2%) and Alaska cod (1.0%). The ANOVA analysis on the total catch in relation to net material showed that there was not statistically significant difference at the 5% level between nylon net (PA) and biodegradable net (PBS) (p=0.91). With the cluster analysis on the catch in relation to net material (PA, PBS) and twine thick (#2, #3), it showed the influence of net material on the catch was greater than that of twine diameter in this experiment. From the test of homogeneity on the catch by the gillnet with PA and PBS in which several species were caught in 2013, there was not statistically significant homogeneity in relation to net material (p<0.005). That meant the traditional gillnet of nylon (PA) was more efficient than the biodegradable (PBS) gillnet to catch several kinds of fish, however the PBS gillnet was better than the PA gillnet to catch the target Pacific herring.

Physical Properties Analysis for Automated Process Design of Solar Salts (천일염 자동화 공정설계를 위한 물리적특성 분석)

  • Kim, Hoon;Kim, Woong;Lee, Hyo-Jae;Han, Jae-Woong
    • The Journal of Korea Institute of Information, Electronics, and Communication Technology
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    • v.11 no.4
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    • pp.408-413
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    • 2018
  • In this paper, the particle size, bulk density, friction coefficient and angle of repose were measured for the automatic processing of solar salt, which was classified with 5 levels of moisture content (16.5, 13.2, 8.2, 4.9, 3.7%). Average diameter was 1.98~1.60mm according to moisture content, and bulk density increased with increasing moisture content. As a result of measuring the coefficient of dynamic friction, the maximum value was shown in the stainless steel plate according to the material, and ABS plate and acrylic plate were lower in the order. Movement occurred at the moisture content of 8.2% or less, and the empty angle of repose was increased and the filling angle of repose was decreased as the moisture content increased.