• Title/Summary/Keyword: 재료시험

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Fabrication and characterization of boron free E-glass fiber compositions (붕소를 함유하지 않는 E-glass fiber의 제조 및 특성에 대한 연구)

  • Lee, Ji-Sun;Lim, Tae-Young;Lee, Yo-Sep;Lee, Mi-Jai;Hwang, Jonghee;Kim, Jin-Ho;Hyun, Soong-Keun
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.23 no.1
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    • pp.44-50
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    • 2013
  • E-glass fiber is the most widely used glass fiber for reinforced composite materials of aircrafts, automobiles and leisure equipments. But recently researches are being progressed to reduce boric oxide from 8 % to 0 (zero), as is called 'Boron free E-glass', because of increasing material cost, environmental problem, and improving chemical resistance and mechanical properties of E-glass fiber. In this study, we fabricated the bulk glass and fiber glass of 'Boron free E-glass (BF) compositions', and characterized thermal properties and optical properties. 'Boron free E-glass (BF)' was obtained by the melting of mixed batch materials at $1550^{\circ}C$ for 2 hrs with different $Al_2O_3$ compositions 5~10 %. We obtained transparent clear glass with high visible light transmittance value of 81~86 %, and low thermal expansion coefficient of $4.2{\sim}4.9{\times}10^{-6}/^{\circ}C$ and softening point of $907{\sim}928^{\circ}C$. For the chemical resistance test of 'BF' fiber samples, we identified that the higher alumina contents gives the better corrosion resistance of glass fiber.

Studies on Phosphorus-32 Labeling of the House Fly ( I ) (Phosphorus-32에 의한 집파리의 표식효과 (I))

  • Ryu J.;Chung K. H.;Kwon S. H.;Kim H. W.
    • Korean journal of applied entomology
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    • v.13 no.2 s.19
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    • pp.93-97
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    • 1974
  • This paper describes experiments made to develop a technique for marking insects and get the informations for ecological studies as a means of tagging flies with radioactive phosphorus, and also to learn the effect on the subsequent generation of flies. Tests were conducted with house flies, Musca domestica L. emerged front the larvae that had reared in a media containing various concentrations of P-32. Radioactivity of the flies was measured with end-window type $(2mg/cm^2)$ Geiger-Muller counter and proportional counter made by Aloka. In following the daily increases in counting rates by 6-day-old larvae it was apparent the larvae in the starting media containing the higher concentrations of P-32 were showing high counting rates. It was found that about 13.2 per cent of the radioactive material remained in the empty puparia after the flies emerged. Radioactivity of the emerged flies decreased gradually and the biological halflife of phosphorus-32 was approximately 6.14 days with considerable variation. A significant amount of P-32 were detected in the abdominal and thoracic sections as compared with other parts of adult. The activity of phosphorus·32 in eggs and larvae produced by adults reared in medium containing 0.2 microcurie or more of P-32 per gram were readily detected with Geiger-Mi·lier counter. On the other hand, the radioactivity of eggs and larvae produced by the treated males crossed with untreated normal females could be only detected in the medium containing more of 2.0 microcurie with G.M. counter. There was no apparent damage to the flies at dosages as high as 0.5 microcurie per gram of medium. For field studies a concentration of 0.5 microcurie of P-32 per gram of artificial medium appears to give adequate labeling for positive identification of flies and their egg masses.

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Measurement of Mechanical Properties of Thin Film Materials for Flexible Displays (플렉서블 디스플레이용 박막 소재 물성 평가)

  • Oh, Seung Jin;Ma, Boo Soo;Kim, Hyeong Jun;Yang, Chanhee;Kim, Taek-Soo
    • Journal of the Microelectronics and Packaging Society
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    • v.27 no.3
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    • pp.77-81
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    • 2020
  • Commercialization of flexible OLED displays, such as rollable and foldable displays, has attracted tremendous interest in next-generation display markets. However, during bending deformation, cracking and delamination of thin films in the flexible display panels are the critical bottleneck for the commercialization. Therefore, measuring mechanical properties of the fragile thin films in the flexible display panels is essential to prevent mechanical failures of the devices. In this study, tensile properties of the metal and ceramic nano-thin films were quantitatively measured by using a direct tensile testing method on the water surface. Elastic modulus, tensile strength, and elongation of the sputtered Mo, MoTi thin films, and PECVD deposited SiNx thin films were successfully measured. As a result, the tensile properties were varied depending on the deposition conditions and the film thickness. The measured tensile property values can be applied to stress analysis modeling for mechanically robust flexible displays.

The Forced Motion Analyses by Using Two Dimensional 6-Node and Three Dimensional 16-Node Isoparametric Elements with Modification of Gauss Sampling Point (6절점 2차원 및 16절점 3차원 등매개변수 요소의 가우스 적분점 수정을 이용한 강제진동 해석)

  • 김정운;권영두
    • Computational Structural Engineering
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    • v.8 no.4
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    • pp.87-97
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    • 1995
  • For the same configuration of two-dimensional finite element models, 6-node element exhibits stiffer bending stiffness than 8-node element. This is true in the relation between 16-node element and 20-node element for three-dimensional model. This stiffening phenomenon comes from the elimination of several mid nodes from full-node elements. Therefore, this may be called 'relative stiffness stiffening phenomenon'. It seems that there are a couple of ways to correct the stiffening effect, however, we could find only one effective method-the method of modification of Gauss sampling points-which passes the patch test and does not alter other kinds of stiffness, such as extensional stiffness. The quantity of modification is a function of Poisson's ratios of the constituent materials. We could obtain two modification equations, one for plane stress case and the other for plane strain case. This method can be extended to 3-dimensional solid elements. Except the exact plane strain cases, most 3-dimensional plates could be modeled successfully with 16-node element modified by the equation for the plane stress case. The effectiveness of the modification method is checked by applying it to several examples with excellent improvements. In numerical examples, beams with various boundary conditions are subjected to static and time-dependent loads. Free and forced motion analyses of beams and plates are also tested. The beam and plate may be composed of isotropic multilayers as well as a single layer.

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Neutron Shielding Performance of Mortar Containing Synthetic High Polymers and Boron Carbide (합성 고분자 화합물 및 탄화붕소 혼입에 따른 모르타르의 중성자 차폐성능 분석)

  • Min, Ji-Young;Lee, Bin-Na;Lee, Jong-Suk;Lee, Jang-Hwa
    • Journal of the Korea Concrete Institute
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    • v.28 no.2
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    • pp.197-204
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    • 2016
  • Concrete walls of neutron generating facilities such as fusion reactors and fission reactors become radioactive by neutron irradiation. Both low-activation and neutron shielding are a critical concern at the dismantling stage after the shutdown of facilities with a requirement of radioactive waste management. To tackle this, two types of additives were investigated in fabricating mortar specimens: synthetic high polymers and boron carbide. It is well known that a hydrogen atom is effective in neutron shielding by an elastic scattering because its mass is almost the same as that of the neutron. And boron is an effective neutron absorber with a big neutron absorption cross section. In this study, the effect of the type, shape, and size of polymers were investigated as well as that of boron carbide. Total 16 mix designs were prepared to reveal the effect of polymers on mechanical properties and neutron shielding performance. The neutron does equivalent of polymers-based mortar for fast neutrons decreased by 36 %, and the count rate of boron carbide-based mortar with regard to thermal neutrons decreased by 90 % compared to conventional mortar. These results showed that a combination of polymers and boron carbide compounds has potential to reduce the thickness of neutron shields as well as radioactive waste from reactors.

An Experimental Study on the Mechanical and Durability Properties of Ductile Cement Panel Used Vacuum Extrusion Molding (진공압출성형 고인성 시멘트 패널의 역학 및 내구특성에 관한 실험적 연구)

  • Rho, Hyoung-Nam;Lee, Jong-Suk;Han, Byung-Chan;Kwon, Young-Jin;Lee, Sang-Soo;Song, Ha-Young
    • Proceedings of the Korea Concrete Institute Conference
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    • 2008.11a
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    • pp.473-476
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    • 2008
  • Due to the pursuit of high function and international price increase in the field of construction, the application of the secondary product using cement is on the increase gradually in the construction industry in the pursuit of economic cost reduction by the shortening of the construction time like Expediting and the dry construction method at the same time. However, it is in very urgent situation of measures to improve the structural performance or durable performance because it is limited for use in terms of panel in interior exterior building or functional repair reinforce as yet. Accordingly, this study is to investigate applicability of permanent Formwork like mould with the structural performance or excellent durable performance in the field of construction, and to derive optimum mixture in the performance and quality of manufacture. As a result of analysis comparison with the dynamic and durable properties of vacuum extrusion molding high toughness cement panel according to the mixture of four conditions, this study has found that the test body of mixing ECC-DP3 using small filler and large granulated blast furnace slag and powder flame retardant had excellent relative hardness and bending stress strain. The durable performance has shown excellent tendency by the decrease of porosity and enhancement of water-tightness.

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Characterization of Ceramic Composite-Membranes Prepared by TEOS-PEG Coating Sol (TEOS-PEG계 Sol-Gel코팅에 의한 세라믹 분리 막의 제조 및 특성)

  • Kim, Tae-Bong;Choi, Se-Young;Kim, Goo-Dae
    • Journal of the Korean Ceramic Society
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    • v.42 no.3 s.274
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    • pp.165-170
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    • 2005
  • Sol-gel methods offer many advantages over conventional slip-casting, including the ability to produce ceramic membranes. They are purer, more homogeneous, more reactive and contain a wider variety of compositions. We produced ormosil sol using sol-gel process under various molecular weight of polymer species[polyethylene glycol(PEG)] in total system [Tetraethyl ortho silicate(TEOS)-polyethylene glycol(PEG)]. The properties of as-prepared ormosil sol such as viscosity and gelation time are characterized. Also, the ceramic membrane was prepared by dip-coating with synthetic sol and its microstructure was observed by scanning electron microscopy. The permeability and rejection efficiency of membrane for oil/water emulsion were evaluated as cross­flow apparatus. The ormosil sol coated membrane was easily formed by steric effect of polymer and it improved flux efficiency because infiltration into porous support decreased. Its flux efficiency was elevated about $200\;l/m^2h$ compared with colloidal sol coated membrane at point of five minutes from starting test.

Behavior Characteristics of Underground Flexible Pipe Backfilled with Lightweight Foamed Soil (경량기포혼합토로 뒷채움된 연성매설관의 거동특성)

  • Lee, Yong-Jae;Yea, Geu-Guwen;Park, Sang-Won;Kim, Hong-Yeon
    • Journal of the Korean Geosynthetics Society
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    • v.14 no.1
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    • pp.43-50
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    • 2015
  • Lightweight Foamed Soil (LWFS) is a useful material for underground pipe backfill because of reusability of excavated soil and no compaction effect. In this research, a pilot test is carried out and monitoring results are analyzed to investigate behaviors of a flexible pipe, when LWFS is applied as a backfill material. Simultaneously, they are compared with another test case which is backfilled with Saemangeum dredged soil. As a result, the vertical earth pressure of the case backfilled with LWFS slurry presents that decreases as much as 25.6% in comparison with dredged soil and it is only within 10% after solidification. In case backfilled with dredged soil, the horizontal earth pressure is more than 3.6 times of the case used by LWFS and the vertical and horizontal deformation is more than 3.2 and 2.6 times of the case, respectively. It presents excellent effects on earth pressure and deformation reduction of LWFS. The stresses measured at the upper side of the pipe generally present compressive aspects in case backfilled with dredged soil. However, they present tensile aspects in case of LWFS. It is because of negative moment occurred at the center of the pipe due to the buoyancy from LWFS slurry. Conclusively, LWFS using Saemangeum dredged soil is very excellent material to use near the area in comparison with the dredged soil. However, the countermeasure to prevent the buoyancy is required.

Fundamental Study on the Reinforcing Effect of Reinforced Clayey Soil with Nonwoven-geotextile (부직포 보강 점성토의 보강효과에 관한 기초적 연구)

  • 김유성;이재열
    • Geotechnical Engineering
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    • v.14 no.4
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    • pp.61-76
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    • 1998
  • Various kinds of reinforced soil methods have been developed by many researchers or companies for their economic merits mainly. These methods have generally used sandy soils which have high permeability as embanking or backfill material. That is because, if poor embanking materials, especially like a clayey soil which has very low permeability, are used in a reinforced soil embanking, and if excessive pore water pressure is produced by external factors, the friction resistance between reinforcing members and Boils decrease, as a result possible damage or collapse of the body of a reinforced embankment. In fact, clayey Boils can also be used as a embanking materials with reinforcement which has high permeable capacity, and are expected to be able to dissipate the excess pore water pressure effectively. In this study reinforcing effects have been examined through a serries of direct shear tests in which clayey soils are reinforced with nonwoven geotextiles of which permeability is very high and tensile strength is relatively weaker than geogrids which are usually used in reinforced soil wall. Even though such nonwoven geotextile are used as reinforcement of high saturated clayey soils. the test results show the possibility that nonwoven geoteztiles could be used as a reinforcement for reinforced soil walls effectively.

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유리반도체

  • 박창엽
    • 전기의세계
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    • v.24 no.4
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    • pp.6-10
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    • 1975
  • 반도체와 그의 응용소자는 지난 20여년간 눈부식 발전을 이룩하였다. 이는 주로 단결정의 제작기술 진보에 의한 것으로 본다. 그러나 최근 단결정과는 전연 다른 유리질반도체가 국제회의에서도 그 우수성을 의논하기에 이르렀다. 유리질 반도체가 주목을 끌게 된겻은 1968년 Ovshinsky가 "무질서 구조에 있어서 가역적 스위칭현상"이라는 논문이 발표되고 유리질 반도체를 사용한 Ovonic 스위칭 소자의 출현에 기인된다. 유리질 반도체가 전기스위칭 작용, 기억작용을 나타낸다고 하는 Ovshinsky의 발표는 전자제치로서의 응용에 대해 찬반되는 의견이 있었지만 물성적 연구의 교량적인 역할을했다고 할 수 있다. 이런 반도체에 속하는 재료는 호칭도 여러가지로 유리질반도체, 비정질반도체 무정형반도체등으로 불리어진다. 단결정체가 각 격자간에 장거리질서를 갖는 반면 유리질 반도체는 무질서한 구조로 각 격자간에 단거리 질서를 갖는 것이 단결정과는 본질적으로 다른 점이라 본다. 유리 반도체의 종류는 첫째, 원소성 유리반도체로서 Ge, Si, Se, Te 들과 같이 단일원소로 된 겻과, 둘째 IV, V, VI족 원소로 된 공유결합 합금인 As$_{2}$Se$_{3}$-As$_{2}$Te$_{3}$ 계 Ge Si As Te계등의 칼코게나이드 유리등으로 금지대는 어느 것이나 2eV이하이다. 셋째 이론결합인 SiO $Al_{2}$O$_{3}$ Ta$_{2}$O$_{3}$Si$_{3}$N$_{4}$등의 산화물 및 질화물로 대표되는 분자성 비정질 물질로서 금지대는 2eV보다 큰 세종류로 크게 분류할 수 있다. 분류할 수 있다. 한다. 단 개개의 문제에 관한 구체적인 해석 또는 검토에 관하여는 다음 기회에 미루기로하고, 우선 여기서는 당면문제로서 대처하지 않으면 안될 자동주파수제어문제및 계통의 경제운용문제만에 한정하여, 이것을 우리나라의 현상과 관련시켜 개설하고, 이들의 자동화에 관한 기본적인 문제를 간단히 적어 보겠다. 가능하다. 제작완료된 ASIC은 기능시험을 완료했으며 실제 line-of-sight(LOS) 시스템 구현에 적용중이다. 시대를 살아 갈 회원들이다. '컨텐츠의 시대'가 개막되는 것이며, 신세기통신과 SK텔레콤은 선의의 경쟁 과 협력을 통해 이동인터넷 서비스의 컨텐츠를 개발해 나가게 될 것이다. 3배가 높았다. 효소 활성에 필수적인 물의 양에 따른 DIAION WA30의 라세미화 효율에 관하여 실험한 결과, 물의 양이 증가할수록 그 효율은 감소하였다. DIAION WA30을 라세미화 촉매로 사용하여 아이소옥탄 내에서 라세믹 나프록센 2,2,2-트리플로로에틸 씨오에스터의 효소적 DKR 반응을 수행해 보았다. 그 결과 DIAION WA30을 사용하지 않은 경우에 비해 반응 전환율과 생성물의 광학 순도는 급격히 향상되었다. 전통적 광학분할 반응의 최대 50%라는 전환율의 제한이 본 연구에서 찾은 DIAION WA30을 첨가함으로써 성공적으로 극복되었다. 또한 고체 염기촉매인 DIAION WA30의 사용은 라세미화 촉매의 회수 및 재사용이 가능하게 해준다.해준다.다. TN5 세포주를 0.2 L 규모 (1 L spinner flask)oJl에서 세포간의 응집현상 없이 부유배양에 적응,배양시킨 후 세포성장 시기에 따른 발현을 조사한 결과 1 MOI의 감염조건 하에서는 $0.6\times10^6$cell/mL의 early exponential시기의 세포밀도에서 72시간 배양하였을 대 최대 발현양을

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