• Title/Summary/Keyword: 잔류분

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Elimination of BHC Residues in the Polishing and Cooking Processes of Brown Rice (현미(玄米)의 도정(搗精) 및 취반(炊飯) 과정중 BHC 잔류분(殘留分)의 제거(除去))

  • Kim, Yong-Hwa;Kim, Hye-Nam;Kim, Sang-Soon;Lee, Su-Rae
    • Korean Journal of Food Science and Technology
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    • v.11 no.1
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    • pp.18-25
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    • 1979
  • In order to investigate the effect of polishing washing and cooking processes on the residue level of BHC in rice grain, brown rice samples having a 0.3 ppm total BHC content were subjected to various treatments and residue analysis. The results are summarized as follows: 1) The conventional polishing process of brown rice decreased the residue level down to 8 and 20% for 100 and 70% polished rice, respectively. 2) The washing procedure decreased the level to 34 and 31% for 100 and 70% polished rice, respectively. 3) The cooking processes with a conventional kettle and an automatic electric cooker decreased the residue level to 86 and 77% in 100% polished rice, and 69 and 41% in 70% polished rice, respectively. 4) By summation of the above results in sequence. it was concluded that the residue levels of BHC in cooked rice were 2.3 and 4.3% of original residue in the brown rice for 100 and 70% polished rice, respectively.

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Studies on the Residues of Chlorinated Organic Insecticides -3. Heptachlor residues in soil 15 years after yearly treatment of the soil insecticide in a tobacco field- (유기염소계 살충제의 잔류분에 관한 연구 -3. 담배연작토양의 Heptachlor 잔류분에 관하여-)

  • Park, Chang-Kyu
    • Applied Biological Chemistry
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    • v.18 no.2
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    • pp.61-64
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    • 1975
  • Soil residues in a tobacco field yearly treated with a soil insecticide, Heptachlor, was analyzed by GLC equipped with electron capture detector(ECD). In addition, translocation of the heptachlor residues into two staple vegetables, radish and chinese cabbage was also studied under field conditions. The results were summarized as follows; 1. The Heptachlor residues in the soil of tobacco plots were less than 0.010 ppm. 2. The Heptachlor residues in radish and chinese cabbages cultivated in the tobacco plot were also below 0.010 ppm. 3. Amount of Heptachlor residues translocated into the vegetables were not related to the concentrations of the residues in the soil.

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Studies on the Residues of Chlorinated Organic Insecticides - I. Heptachlor Residues in or on Commercial Vegetables - (유기염소계(有機鹽素系) 살충제(殺蟲劑)의 잔류분(殘留分)에 관(關)한 연구(硏究) - 1. 시판채소중(市販菜蔬中) Heptachlor 잔류분(殘留分)에 관(關)하여 -)

  • Park, Chang-Kyu;Yoo, Jai-Yoon
    • Applied Biological Chemistry
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    • v.15 no.1
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    • pp.7-17
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    • 1972
  • Samples of 13 vegetables were collected, between 14 July and 6 August, 1971, from 15 markets located in 12 different cities and analyzed for Heptachlor residues by gas liquid chromatograph. The residue concentrations of Heptachlor and its epoxide were estimated separately, at a sensitivity level of 0.001 p.p.m., to produce Heptachlor residues on the fresh weight basis. The Heptachlor residues in or on the crops analyzed, including three staple vegetables, potatoe, radish and chinese cabbage, were found fairly low and are far lower than the residue tolerences for respective vegetables recommended jointly by FAO and WHO of the United Nations.

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Operating Principle of Residual Gas Analyzer (잔류가스분석기 (RGA)의 작동원리)

  • Park, C.J.
    • Journal of the Korean Vacuum Society
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    • v.17 no.4
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    • pp.262-269
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    • 2008
  • The residual gas analyzer (RGA) is employed for the process control of a vacuum system by measuring residual gases in it. This review paper introduces operating principles of the RGA and problems that can be encountered during use, together with their possible solutions.

Development of a New Resilience Index Considering the Residual flow of Urban Drainage System (도시 배수 시스템의 잔류 유량을 고려한 새로운 복원력 지수 개발)

  • Kim, Young Nam;Lee, Eui Hoon
    • Proceedings of the Korea Water Resources Association Conference
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    • 2021.06a
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    • pp.57-57
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    • 2021
  • 최근 급격한 도시화와 기후변화로 인해 도시의 홍수피해가 증가하고 있으며, 복합적인 재난으로 악화되는 경우가 많아졌다. 복합재난으로 인한 피해를 줄이기 위해 재해발생 전·후 대응이 중요하며, 이를 위해 복원력 개념을 도입할 필요가 있다. 도시 배수 시스템의 복원력은 대상유역의 면적과 절대적인 침수량에 따라 좌우된다. 따라서 지역의 도시 배수 시스템의 복원력을 정확하게 평가하기 위해 대상유역의 정보를 반영한 지역 맞춤형 복원력 지수의 개발이 필요하다. 대상유역의 정보를 반영하기 위해 도시 배수 시스템의 배수능력을 복원력 지수에 적용하였다. 도시 배수 시스템의 배수능력을 나타내기 위해 시스템 잔류유량을 분모로, 침수량을 분자로 하여 복원력 지수를 계산하였다. 본 연구에서는 제안된 새로운 복원력 지수를 대구 비산 빗물펌프장에 적용하였다. 강우자료는 재현기간이 100년, 200년 그리고 300년 빈도의 확률강우량을 사용하였으며, 지속시간은 30분, 60분 그리고 90분으로 설정하였다. 침수량과 시스템 잔류 유량은 1분 단위로 EPA SWMM을 통해 값을 구하였다. 시스템 잔류 유량을 기반으로 하는 복원력 지수는 최소 0.995029에서 최대 0.998662로 나타났다. 본 연구에서 제안한 도시 배수 시스템 잔류 유량 기반 복원력 지수는 배수 시스템의 처리 능력을 반영한 지수라고 할 수 있으며 배수 시설의 설치, 교체 및 재건 등 수해 방재 계획 평가에 활용될 수 있다.

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잔류가스분석기를 활용한 베이크아웃 시험 종료조건 수립 검토 결과

  • Park, Seong-Uk;Seo, Hui-Jun;Jo, Hyeok-Jin;Im, Seong-Jin;Son, Eun-Hye;Mun, Gwi-Won
    • Proceedings of the Korean Vacuum Society Conference
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    • 2015.08a
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    • pp.103.1-103.1
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    • 2015
  • 위성체 개발에 있어서 지상에서 위성체의 부품에 대한 고온($85^{\circ}C$ 이상)과 고진공($5.0{\times}10-3Pa$ 이하)의 상태를 모사하여 오염물질을 제거하는 베이크아웃 시험이 필수적이다. 일반적으로 베이크아웃 시험의 종료여부는 TQCM (Thermoelectric Quartz Crystal Microbalance)을 이용한 탈기체(outgassing)의 흡착률을 측정하여 결정한다. 측정된 흡착률을 통해 시험 대상 표면에서 발생하는 탈기체량을 추정할 수 있으며, 결국 시험 대상의 우주 부품으로써의 적합성을 판단할 수 있다. TQCM을 적용하지 못하는 경우, 베이크아웃 시험 종료여부를 판단하기 위해 잔류가스분석기(Residual Gas Analyzer: RGA)를 활용하는 것을 고려하였다. 베이크아웃 시험 중 잔류가스분석기를 활용하여 시편에서 방출되는 오염물질을 측정하였으며, 그 중 측정량이 가장 많은 40-45 amu 범위의 측정값 추이를 관찰하여, 베이크아웃 시험 종료조건 수립 가능성을 검토하였다.

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Determination and confirmation of the carbendazim residue in soybean sprout (콩나물중 살균제 carbendazim 잔류분의 정량 및 확인)

  • Kim, Young-Gook;Park, Jong-Tae;Hong, Suk-Soon
    • The Korean Journal of Pesticide Science
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    • v.2 no.3
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    • pp.79-84
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    • 1998
  • Tandem HPLC and atmospheric pressure chemical ionization(APcI) LC/MS method was used for the determination and confirmation of carbendazim residues in soybean sprout. Fluorescence(FL) detector was connected in tandem with the ultraviolet(UV) detector for dual detection of the carbendazim residue at the excitation and emission wavelength of 280 nm and 310 nm, respectively. The limit of detection for carbendazim was $0.1{\mu}g/kg$ sample. Recoveries of carbendazim from fortified soybean sprout at 0.5, 1.0 and 2.0 ppm were averaged 89.1%. Mass spectrometry using a APcI source confirmed the carbendazim residue in the soybean sprout sample. Fragmentation pattern on the APcI LC/MS spectrum of carbendazim was simpler than that from electron impact(EI) mass spectrum. Carbendazim produced 3 major ions including m/z 133, m/z 159 and m/z 191($M^{+}$). This method was sensitive enough to provide reliable and reproducible results for practical applications.

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Degradation of [$^{14}C$]Carbofuran in Soils and Characterization of its Nonextractable Residues (토양중 [$^{14}C$Carbofuran의 분해 및 비추출성 잔류분의 특성)

  • Park, Chang-Kyu;Lee, Young-Deuk
    • Applied Biological Chemistry
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    • v.38 no.3
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    • pp.263-268
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    • 1995
  • A study was undertaken to compare degradation patterns of carbofuran in soils between submerged and upland moisture conditions [$3-^{14}C$]Carbofuran was treated in each soils at the rate of 1.0 mg/kg (87.8 kBq $^{14}C/50g$ soil) and the time-course analysis for distribution of radioactivity and degradation products were conducted. Differences in the pathway and rate of carbofuran degradation in soils were observed between submerged and upland moisture conditiona major degradation being hydrolysis at 7-C position and oxidation at 3-C position, respectively. Carbofuran showed less persistence in soils of higher moisture contents A significant portion, $24{\sim}39%$ of the total radioactivity, resided in soils as nonextractable residues at 60 days after treatment The nonextractable radioactivity was mainly located in soil organic matter, fulvic acid, humic acid and humin factions Gel filtration chromatography confirmed the incorporation of carbofuran and its degradation products into the organic matter.

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A Study on the Neoasozine Residues in Rice Grain by Neutron Activation Method (방사화(放射化) 분석법(分析法)에 의한 미곡(米穀)중 네오아소진 잔류분(殘留分)에 관한 연구(硏究))

  • Kim, Yong-Hwa;Lee, Koon-Ja;Lee, Su-Rae
    • Korean Journal of Food Science and Technology
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    • v.13 no.1
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    • pp.20-24
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    • 1981
  • Residues of neoasozine in rice grain were determined by neutron activation and colorimetric techniques. Twice application of the chemical before flowering did not lead to any increased residue level while 4-times application resulted in significant increase in the residue level up to 0.54-0.75 mg $As_2O_3/kg$. The partition ratio of arsenic residues into polished rice grain and bran was 73 : 27 in 100% polishing while most of the residues in the bran was transferred to oil cake fraction during solvent extraction, reaching up to 2.9 mg $As_2O_3/kg$. The neutron activation technique was advantageous because of its high sensitivity and the smaller sample amounts required for analysis.

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