• Proceedings of the Korean Fiber Society Conference
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• 2007.11a
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• pp.427-428
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• 2007

$Ca(OH))2$ 양에 관계없이 1일(日) 추출시에는 추출 pH 6에서 인디고 함량이 높았으며, 2일(日) 추출시에는 추출 pH에 의한 인디고 함량의 차가 매우 작았다. 추출 pH에 상관없이 쪽 추출액의 저장시간이 길어질수록 인디고 함량이 낮은 분말이 얻어졌다.

• KOREAN JOURNAL OF CROP SCIENCE
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• v.51 no.spc1
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• pp.247-250
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• 2006

We herein studied the effect of polyamines (putrescine, spermidine and spermine) on growth and indigo biosynthesis in hairy root cultures of Polygonum tinctorium Lour. Our results revealed that polyamine treatment increased hairy root growth and indigo biosynthesisat all tested concentrations, with the highest growth rate (4.4 g/ flask) and indigo yield (216 ug/g) induced by 70 mg/L putrescine. These results show far the first time that the growth rates and indigo biosynthesis of Polygonum tinctorium hairy roots may be improved by addition of polyamines to the liquid culture medium.

• Proceedings of the Korean Society of Dyers and Finishers Conference
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• 2012.03a
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• pp.101-101
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• 2012

천연가죽에 색상을 부여하기 위한 염색공정에서 종전의 합성염료가 아닌 자연에서 추출한 천연염료를 이용하여 블루색상을 가지는 피혁 제조 공정을 확립하였다. 피혁에 적용 가능한 블루색상을 가지는 천연염료 중에 쪽 염료가 유일한 상황이다. 가죽 무게 대비 5%의 쪽염료를 가죽 제조 드럼에 투입하여 100분간 충분히 회전시킨 후에 가죽의 유연성을 부여하는 가지제를 12% 추가로 투입하여 블루 색상을 가지는 가죽을 제조하였다. 그 결과 마찰견뢰도, 일광견뢰도, K/S가 우수한 피혁 염색공정을 확립하였다.

• Proceedings of the Korean Fiber Society Conference
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• 2007.11a
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• pp.363-364
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• 2007

• KOREAN JOURNAL OF CROP SCIENCE
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• v.40 no.2
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• pp.203-211
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• 1995

This study was conducted to know how low temperature response of rice varieties is available for breeding lines adapted to cold weather. Some agronomic characters related to cold tolerance were evaluated for 188 varieties including three varietal types of Japonica, Tongil, and Indica. Cold tolerance of Japonica and Indica type varieties varied in leaf discoloration, heading delay, reduction of culm length, panicle number, spikelet number, panicle exsertion, spikelet fertility, and phenotypic acceptability at maturity, while Tongil type varieties were susceptible in most agronomic characters. In leaf discoloration, most Japonica type varieties were highly tolerant, while Indica type varieties showed various responses from tolerant to susceptibility. Not significant difference among three varietal types was observed on reduction of panicle number and spikelet number due to low temperature.

• Journal of Sericultural and Entomological Science
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• v.47 no.1
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• pp.31-35
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• 2005

This study had done to find an easily-dyeing method for novices because the dyeing method of traditional indigo has not been general to the public so that only an expert could dye the fibers. The results are as the following. When the powders after burning the shell of cockle (tegillarca granosa) were added. pH of the solution was 12.35 The k/s value of 2.49 was the highest in the dye after dipping in the solution of indigo for 1-2 days and the k/s value was 3.10 when adding 20 g/l of the starch (55% corn-starchy products in Korean market) into the solution of indigo. In addtion, the k/s value was the highest when fermenting temperature was $30^{\circ}C$ and when the powders after burning the cockle shell were 4 g/l. There were no differences between water and lye of rice straw which had used for the ferment of indigo. The components of two dye which has traditionally made of the cockle shell and which has made of calcium hydroxide were all the same.

• Journal of the Korean Society of Clothing and Textiles
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• v.25 no.10
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• pp.1763-1769
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• 2001

본 논문에서는 쪽의 발효염색이 잿물과 같이 강 알칼리 매체 하에서 사용해야 하고 또한 자연 발효의 경우 온도조절이 제한되어 있어 단백질 섬유 특히 양모에는 적합하지가 않은 점 등을 해결하기 위해 우리나라에서 주로 현재 재배되고 있는 polygonum tinctorium을 사용하여 Saxon blue 법으로 단백질 섬유를 염색하여 염색성을 살펴보았다. 그 결과 Saxon blue로 염색할 때의 등온흡착곡선은 Langmiur형임을 보였으며 색상은 주로 B 영역에서 나타났다. Saxon Blue로 염색한 견 직물과 양모 직물 모두 우수한 항균성을 나타내었으며 드라이 크리닝과 마찰에 대해서는 좋은 견뢰도를 보여 주었다.

• Korean Journal of Medicinal Crop Science
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• v.21 no.3
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• pp.213-219
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• 2013

This study was carried out to find out the optimum method of preparation of indigo standard solution and its stability, and to investigate the indigo contents in Niram, blue dye extract, from a total of 7 indigo plants and 34 breeding lines of Persicaria tinctoria H. Gross. Proper solvent for indigo standard was dimethyl sulfoxide (DMSO), and appropriate concentration was 1 mg of indigo in 10 mL of DMSO. Absorbance value of UV/Vis Spectrophotometer at 620 nm of standard solution was changed decreasingly 12 hours after the preparation of standard solution irrespective of the storage conditions such as temperature and light. Average value of absorbance of 8-fold diluted standard solutions prepared daily during 16 days was $0.210{\pm}0.005$, indicating the powder of indigo compound was stable chemically. Calibration curve was made for quantitative analysis of indigo of 7 Niram samples, and indigo contents ranged from 0.69% to 18.76% showing relatively larger variation. Across all 34 breeding lines, the range of indigo content was from 7.9 mg to 56.4 mg per 100 g of fresh leaves, averaging 25.2 mg of indigo content and showing a 47.7% coefficient of variation.

• Conservation Science in Museum
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• v.13
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• pp.13-22
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• 2012

The patterns for Jeogui and Pyeseul (patterns of the queen's ceremonial robe worn and a belt ornament covering knees in the front) as owned by National Museum of Korea were made in the early 20th century and both of them were colored on paper. Through a non-destructive analysis on pigments and dyes used on both the patterns, it was attempted to identify the coloring materials. As for the analysis of the coloring pigments, the XRF was used. As a result of the pigment analysis on the pattern for Jeogui, it is presumed that lead white was used for obtaining the white color, ink stick for black color, orpiment for yellow color, cinnabar and red lead for red color, copper and arsenical or a mixture of copper carbonate and orpiment for green color whereas brass seems to have been used for obtaining other colors. The pigments used for obtaining the colors of white, black, yellow and green on the pattern for Pyeseul are the same as those used on the pattern for Jeogui whereas the red pigments used on each of the two patterns are seen to be different. Although it may be difficult to identify the kinds of blue pigments that were used on the patterns for Jeogui and Pyeseul, a mixture containing lead white is presumed to be used as blue pigment. Also, as a result of the UV-Vis spectroscopic analysis performed on the blue hanji (traditional Korean paper) of the pattern for Jeogui, it was presumed to have been dyed with indigo.

• Journal of Sericultural and Entomological Science
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• v.49 no.1
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• pp.8-13
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• 2007

Natural indigo colorants were prepared by extraction of Polygonum tinctorium which was harvested just in the blooming season(in the late of July). The components were analyzed by TLC and HPLC, and its structures were analyzed by FT-IR, EI-mass. The results obtained are summarized as follows; The natural indigo powder was dissolved in DMSO and developed in eluent, $CHCI_3/CH_3CN$(8.5:1.5 v/v) by means of TLC for its quality analysis. It was segregated into indirubin as a red colour and indigo as a blue colour. In case of HPLC analysis,. FT-IR spectrum of indirubin showed a peak for NH residue between 3200 and $3300cm^{-1}$. $^1H-NMR$ spectrum for indigo displayed AA'BB' spin system caused by indole structure between 6.5 and 7.7ppm of H4, 5, 6 and 7, and -NH proton for indirubin showed an singlet between 10.88 and 11.0ppm. EI-mass spectrum of indigo and indirubin both disclosed their molecular size as 262 and it implies that these two substances are isomer.