• Tribology and Lubricants
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• v.16 no.3
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• pp.173-181
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• 2000

Friction, wear and corrosion characteristics of various MoS$_2$ bonded film lubricants were investigated to apply them to automotive wheel joints. MoS$_2$ bonded film lubricants were formulated by combinations of several additives and binders, and they were coated onto the pre-treated surfaces of specimens. Friction and wear characteristics were evaluated with Falex pin & vee-block test and LFW-1 block-on-ring test. For the corrosion resistant characteristics of the films, salt solution spray corrosion tests were performed. Results showed that MoS$_2$ bonded films containing both inorganic and organic corrosion-resistant additives yielded a synergy effect on anti-corrosion resistance. Also, binders having the better water-proof and thermal stability showed the lower friction and higher corrosion resistance.

• Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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• 2001.06a
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• pp.42-48
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• 2001

Chromium carbides have the excellent wear properties as transition metal carbides. Their tribological applications were studied recently. The nano-sized ceramic could enhance the mechanical and electronical properties of materials. In this study, it was observed to test the wear of the coated surface of nano-sized chromium carbides. The nano-sized chromium carbides were produced by sol-gel processing. Coating surface of produced powders was obtained front plasma spraying. Wear test of coating surface was held increasing temperature. The friction coefficient and the wear loss were testified in dry environment. And the worn surfaces were analyzed by XRD and SEM.

• Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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• 1996.04b
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• pp.13-19
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• 1996

The tribological properties of the aluminum short fiber and glass fiber reinforced tin-bronze matrix composites manufactured by vacuum hot pressing was studied. The effect of the composition and the relative density on the wear properties was examined by a reciprocal type tribo-test machine. The results were discussed by the observation of the microstructure of sintered specimen and worn surface observation using SEM and EDS. Addition of the fibers led to the wear resistance since the metal matrix was reinforced by the fibers. The reinforcement of the fiber seemed to be stronger as the distribution of the fibers was more uniform. Graphite also reduce the wear loss. The pores in the sintered composites seemed to play an important role to improve the wear resistance since the pores provide the places where the solid lubricants locate.

• Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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• 2000.11a
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• pp.378-384
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• 2000

This paper presents the results of the repeated sliding tests to determine the wear-life of TiN coated AISI 52100 bearing balls deposited by PVD method and to show the wear mechanisms of those. The sliding tests were carried out using a ball-on-disk tribometer under ambient conditions. The coefficient of friction, wear volume and the cycles to failures of TiN coated bearing balls were measured with different normal loads and roughness of lower specimens. On the wear-life diagram, the normal loads and the cycles to failure showed the good linear relation on log-log coordinate. With a decreasing normal load, the diagram showed that the wear-limits, at which the coated bearing balls survived more than 4000cycles were under 0.1N of the normal load.

• Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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• 2000.11a
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• pp.59-66
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• 2000

An experimental study on the effect of silver particles on the sliding behavior of bearing steels was performed by using a ball-on-disk tribometer. Tests were carried out in ambient air, dry and vacuum. Disks of AISI 52100 were silver-coaled by a thermal evaporation method, and the effects of silver particle transfer on friction were firstly analyzed. In order to understand further the mechanism of silver particles transfer and its effect on friction and wear, pre-compressed silver particles were artificially introduced into the friction interface and the results were compared to those of silver-coated specimens. Results showed that the introduced silver particles produced transfer layers and resulted in low friction. It also showed that this low friction is closely related to the characteristic behavior of transfer layers. Shakedown and rachetting occurred at the friction interface and affected the friction and wear.

• Journal of the Korea Academia-Industrial cooperation Society
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• v.21 no.2
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• pp.634-643
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• 2020

In this study, the rheological and tribological properties of urea grease were studied according to the type and amount of polytetrafluoroethylene (PTFE) powders added to the urea grease, which is the most widely used among solid lubricants, to develop an optimal lubrication system. Urea grease was synthesized using 4,4'-methylenebis(phenyl isocyanate)(MDI), oleylamine, and cyclohexylamine, and PTFE powders prepared by dispersion or suspension polymerization process were then added. The basic rheological and tribological properties of the prepared greases were compared. The worked penetration numbers of urea grease decreased with increasing amount of PTFE powders, but both PTFE powders caused no significant changes in heat resistance and copper corrosion resistance. The shear viscosity increased with increasing PTFE powder content, and the dispersion-type PTFE powder was more effective in increasing the viscosity. In the value of the loss coefficient = 1, the shear stress was higher for the grease containing PTFE powders than the non-PTFE added grease, and the dispersion-type PTFE-added grease showed higher viscosity than the suspension-type PTFE-added grease. Finally, urea grease was found to have a low-performance improvement in terms of wear reduction effects by adding PTFE powders, but the load-bearing performance was up to 2.5 times higher for the dispersion-type PTFE and five times higher for the suspension-type PTFE.

• Applied Chemistry for Engineering
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• v.29 no.5
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• pp.533-540
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• 2018

Graphene has been reported to be an excellent lubricant additive that reduces friction and wear when coated on the surface of various materials or when dispersed in lubricants as an atomic thin material with the low surface energy. In this study, alkyl functionalized graphene oxide (FGO) nanosheets for oil-based lubricant additives were prepared by using three types of alkyl chloride chemicals (butyl chloride, octyl chloride, and tetradecyl chloride). The chemical and structural properties of the synthesized FGOs were analyzed by Fourier transform infrared (FT-IR), X-ray photoelectron spectroscopy (XPS), X-ray diffraction (XRD), Raman spectroscopy, scanning electron microscope (SEM), and transmission electron microscope (TEM). The synthesized FGOs were dispersed at 0.02 wt% in PAO-0W40 oil and its tribological characteristics were investigated using a high frequency friction/wear tester. The friction coefficient and the wear track width of poly alpha olefin (PAO) oil added with FGO-14 were tested by a ball-on-disk method, and the measured results were reduced by ~5.88 and ~3.8%, respectively compared with those of the conventional PAO oil. Thus, it was found that the wear resistance of PAO oil was improved. In this study, we demonstrated the successful functionalization of GO as well as the improvement of dispersion stability and tribological characteristics of FGOs based on various alkyl chain lengths.

• Journal of Energy Engineering
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• v.26 no.3
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• pp.131-136
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• 2017

Automobile engine oil is the most important lubricant for operating as the engine is started. Recently, manufacturers of the automotive industry and lubricants are considerably improving the quality of oil with additive to extend change cycle period. Most customers are recommended genuine oil among different types from shop expert. Through this report we suggest another reference point for consumer to pick highly efficient lubricant. This report is investigated oil compounds to compare with 6 different automotive considering actual running condition for 7 months. we conducted experiment from physical and chemical perspectives. In the field, through various experiments oil compounds between mineral oil and synthetic oil are largely distinguished in oxidation, viscosity, fluid and TBN. These are influenced by engine part wear as piston, bearing etc. Comparing various investigation with different oil the performance of synthetic oil is shown better condition in flash point, oxidation stability and also found less in change pollutant iron, Al compounds. Additives of oil show clear difference Ca level in detergent-dispersant both mineral oil and synthetic oil. And Zn in extreme pressure additives and P in Lubricity improver make no difference to both.

• Applied Chemistry for Engineering
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• v.27 no.6
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• pp.583-589
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• 2016

Lubricant additives including zinc dialkyldithiophosphate (ZDDP) containing metal have been widely used due to the advantage of very low cost, but they can generate impurities such as ash. In this work, ZDDP containing metals was partially replaced with bis[3-(dialkyloxyphosphorothionyl) thio-2-methylpropanyloxy] butane (BAP4s) which was synthesized conveniently and effectively from alkanediol without any metal components. Also, the wear resistance property of synthesized BAP4s were studied. Wear scar diameter (WSD) values of BAP4s with butyl, octyl, decyl, dodecyl or tetradecyl groups were also measured by four-ball test. As the length of the alkyl group increased from 4 to 8, the WSD value of BAP4s decreased rapidly from 0.59 to 0.45 mm, but from 8 to 14, the value increased very slowly from 0.45 to 0.50 mm. Thus, among all BAP4s, B8P4 having BAP4 with the octyl group, showed the lowest WSD value. Furthermore, the WSD values were measured in a lubricant base oil mixed with a 0.50 percent concentration (w/w) of either BAP4 or ZDDP. The former was 0.55 mm, and the latter was 0.45 mm. The thermal stability and tribofilm formation peroperty were also measured by thermogravimetric analyzer (TGA) and energy-dispersive X-rays spectroscopy (EDS), respectively.

• Tribology and Lubricants
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• v.31 no.3
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• pp.125-140
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• 2015

In this paper, we present the results of the wear analysis of journal bearings on a stripped-down single-cylinder engine during start-up and coast-down by motoring. We calculate journal bearing wear by using a modified specific wear rate considering the fractional film defect coefficient and load-sharing ratio for the asperity portion of a mixed elastohydrodynamic lubrication (EHL) regime coupled with previously presented graphical data of experimental lifetime linear wear in radial journal bearings. Based on the calculated wear depth, we obtain a new oil film thickness for every crank angle. By examination of the oil film thickness, we determine whether the oil film thickness at the wear scar region is in a mixed lubrication regime by comparing dimensionless oil film thickness, h/σ, to 3.0 at every crank angle. We present the lift-off speed and the crank angles involved with the wear calculation for bearings #1 and #2. The dimensionless oil film thickness, h/σ, illustrates whether the lubrication region between the two surfaces is still within the bounds of the mixed lubrication regime after scarring of the surface by wear. In addition, we present in tables the asperity contact pressure, the real minimum film thickness at the wear scar region, the modified specific wear rate, and the wear angle, α, for bearings #1 & #2. To show the real shape of the oil film at wear scar region, we depict the actual oil film thickness in graphs. We also tabulated the ranges of bearing angles related with wear scar. We present the wear volume for bearings #1 and #2 after one turn-on and turn-off of the engine ignition switch for five kinds of equivalent surface roughness. We show that the accumulated wear volume after a single turn-on and turn-off of an ignition switch normally increases with increasing surface roughness, with a few exceptions.