• Proceedings of the Costume Culture Conference
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• 2004.04a
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• pp.44-46
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• 2004

심하게 퇴색된 출토 복식유물의 경우 유물의 고유색을 알지 못함은 물론 사용된 염료의 종류를 알지 못함으로 인하여 유물의 보존처리 및 장기간 보관과 전시에 큰 어려움을 지닌다. 이화학 분야에서는 미지시료의 기초 성분분석 방법으로서 thin layer chromatography(TLC)법이 오래 전부터 사용되었는데, 퇴색된 복식유물의 염료분석을 다룬 일부 선행연구에서는 이를 활용하여 유물의 염료를 판정하였다(Kharbade ＆ Agrawal, 1985; Schweppe, 1989). (중략)

• Journal of Conservation Science
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• v.12 no.1 s.15
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• pp.71-82
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• 2003

The paper relics excavated from the 4th excavation of the historical spot No.259 Seonwon temple area were analyzed and conserved. Because these works remained folded, the most important conservation treatment was a separation. This process depended on the state of the works: dry state works were separated using Gore-Tex chamber and the filtrated water, wet state works were separated through vacuum freeze drying method. Analyses of the paper relics performed were examination on the paper to find its distinction, binocular microscope and SEM on fiber, and XRF on character ingredient. This study presumed the times though $C^{14}$ dating of these works. The works were able to be classified through analysis and conservation treatment. This separation made lost part of the works conserve an archetype. This study presented the application of conservation methods on the paper relics which are in the bad condition and obtained information through carbon dating of it.

• Korean Journal of Human Ecology
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• v.2 no.2
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• pp.39-48
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• 1999

본 연구의 목적은 두 종류의 다른 연구자료- 유물과 문헌자료를 이용하여 1950년대 초기에 유행하였던 미국여성복식 가운데 쉬스 드레스(sheath dress)의 디자인 특징을 고찰하는 데에 있다. 본 연구의 일차자료로는 하와이대학교(University of Hawaii)의 The Western Costume Collection에 소장된 1950년대 초기의 복식으로 추측되는 유물과 1950년부터 1955년 사이에 출판된 Vogue, Harper's Bazaar, New York Times Magazine을 문헌자료로 이용하였다. 연구결과, 1950년대 초기의 미국 여성복 디자인의 특징은 여성의 신체적 특징을 강조하며 여성스러움의 미를 극단적으로 추구하는 쉬스 드레스(sheath dress)의 ‘the straight and slender look’으로 요약될 수 있었다. 나아가 문헌분석을 통하여 본 연구의 유물자료가 50년대 초기(1950-1954)의 미국여성복식 디자인의 특징을 보여주는 대표적인 이 시기의 복식유물로 그 사용연대가 확증되었다. 본 연구는 지금까지 주로 문헌자료의 분석만으로 한정되어 왔던 한국의 전형적인 서양복식연구에서 한 걸음 나아가 과거에 실제로 입혀졌던 복식에 대한 이해를 확장하기 위한 또 하나의 연구방법으로 문헌분석과 유물분석(object study)을 병행하여 시도해 보았다는 데에 그 의의가 있다.

• Korean Journal of Heritage: History & Science
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• v.48 no.4
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• pp.4-23
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• 2015

Buried bronze objects are naturally corroded by their surrounding environment, which results in producing corrosion layers containing a number of constituents. Corrosion layers in stable condition protect the objects from the environment and also could provide information in terms of the objects. Characteristic and mechanism of the corrosion layers is likely to be valuable information for the conservation treatment. Many research have been conducted to figure out the formation and characteristic of the corrosion layers, but the more research should be conducted with various approach and analytical methods. Raman spectroscopy is one of the analytical methods to identify microcrystal as a compound while other analytical methods are used to identify element. Therefore, the aim of this research is to identify the characteristic of corrosion layers of both excavated bronze objects through the raman spectroscopy. Two analytical methods, which are raman spectroscopy and SEM~EDS, were used to analyse four excavated bronze bowls. In the case of bronze bowls, malachite was found from the exterior corrosion layer and albite, quartz, and microcline, which are minerals, were also found. Cuprite was detected from the interior corrosion layers illustrating slightly different spectrum due to the combined compound. Lead segregation shows the form of PbO, $PbSO_4$ and $PbCO_3$ or it replaced as cuprite. In this study, small number of samples were analysed. This research is likely to be useful information to figure out not only the characteristic of the corrosion layers but also the authenticity of the artifacts if relevant research will be conducted. Therefore, further comprehensive researches on the various archaeological objects and corrosion environment condition are required in the future.

• Journal of Conservation Science
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• v.29 no.4
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• pp.297-309
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• 2013

Iron objects become corroded at fast speed from the moment when they are excavated, so it is needed to control corrosion through processes of conservation treatment. However, re-corrosion mostly takes place in excavate iron objects, although they have already gone through the process of conservation treatment, and it is more difficult to carry out the second conservation treatment of re-corroded excavated iron objects than the first conservation treatment, and it requires a longer period of time to treat them as well. In this study, aims to discover factors of re-corrosion by scientifically analyzing corrosion products generated during the process of storage after the process of conservation treatment. The finished on conservation treatment of the iron artifacts, which were unearthed from three ancient site in Gyeongju by using the same conservation method between 2002 and 2009, re-corrosion condition observed on the packaging-iron artifacts. Focused on 9 target forged iron artifacts among them, this study analyzed the physical changes by mass measurement, naked-eye and microscopic observations and the chemical changes by SEM-EDS, XRD, IC and ICP analysis. The results show that the yellowish brown corrosion products formed on the facing surface of part dropped from the artifacts had different associated forms but acicular shape. In addition, the acicular shape became clearer as the color changed from red to yellowish brown. According to the process when the conservation treatment was completed, the mass of the artifacts increased in proportion to the corrosion products and the chloride ion ($Cl^-$) concentration had a tendency to increase relatively. ${\beta}$-FeOOH (akaganeite) was confirmed in the XRD analysis for the corrosion products of all the collected samples. As a result of ICP analysis, $Na^+$ and $Ca^{2+}$ components were confirmed.

• 한국문화재보존과학회:학술대회논문집
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• 2002.02a
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• pp.45-52
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• 2002

본 연구에서는 KaOH, $K_2CO_3$, Sodium, 그리고 1차 이온수 용액의 $Cl^-$ 이온 추출량과 부식생성물의 생성순위, 부식물 생성, 그리고 부식물 제거에 관하여 관찰하였으며 이 연구로 아래와 같은 결과를 얻었다. $Cl^-$ 이온 추출량에 대한 실험 결과 NaOH은 탈염 초기에는 Cl- 이온을 잘 추출시켰으나 탈염 횟수가 증가하면서 $Cl^-$ 이온의 추출량이 급감하였다. 또한 유물 중량 변화에도 감소폭이 가장 심하였다. $K_2CO_3$은 NaOH나 1차이온수 용액과 비교해 보면 이 방법은 탈염처리동안 $Cl^-$ 이온을 꾸준히 추출시켜 주었으며 다른 탈염용액에 비해 유물 중량변화가 거의 관찰되지 않았다. Sodium 용액은 $K_2CO_3$ 용액과 마찬가지로 탈염처리 동안 $Cl^-$ 이온을 꾸준히 추출시켰으며 다른 탈염 용액에 비해 $Cl^-$ 이온 추출량이 가장 많았다. 하지만 이 용액은 약품 내에 불순물인 $Cl^-$ 이온을 $3\~5\;ppm$을 기지고 있어 보존처리자가 탈염처리를 할 때 좀 더 신중하게 생각해야 할 것 같다. 1차 이온수 용액은 부식인자가 $Cl^-$이온을 완전하게 제거해주지는 못하였지만, pH가 $7.5\~7.9$로 다른 탈염 용액에 비해서 전위차가 낮으며, 별도로 탈알칼리 처리를 하지 않아도 되기 때문에 유물손상은 극소화할 수가 있다. 따라서 이 용액은 부식이 매우 심한 철제 유물이나 균열이 많은 주조 철편과 같은 유물을 처리할 때 적절한 용액이다. 부식생성물 관찰에서는 출토 철기 유물에 생성된 부식물은 주로 인철광$(\gamma-FeOOH)$, 침철광$(\alpha-FeOOH)$, 적금광$(\beta-FeOOH)$, 그리고 자철광$(Fe_3O_4)$이다. 인위적 부식에서는 전부 인철광의 부식물이 생성되었고 자연적 부식에서는 모두 침철광의 부식물이 생성되었다. 특히 철제 표면에 자연적으로 생성된 공식 녹을 XRD 분석한 결과 적금광으로 동정되었다. 이런 모든 시편들을 각 탈염방법에 따라 탈염처리한 후 XRD와 SEM-EDS으로 분석한 결과 인철광과 침철광은 어떠한 변화도 보이지 않았고, 다만 적금광으로 동정된 시편만이 잔존하지 않았다. 철기 제작별 $Cl^-$ 이온 추출량과 탈염효과에 대한 비교 실험은 이온 크로마토그래피 분석 결과와 마찬가지로 단조 철제유물이 주조 철제보다 $Cl^-$ 이온을 많이 가지고 있었으며, 탈염 처리 후에는 $Cl^-$ 이온은 전혀 발견되지 않았다. 이상의 결과 $K_2CO_3$와 Sodium 용액은 탈염처리에서 가장 적합한 탈염처리 용액으로 알수가 있었으며 특히 어떠한 탈염 용액으로 유물을 처리한다 해도 철제유물에 생성된 부식물은 제거되지 않는다는 것을 알게 되었다. 따라서 보존처리자는 유물 표면의 부식 상태만을 보고 처리하기 보다는 철기제작물로 고려하여 처리하는 것이 필요하다. 또한 금속에 부식을 야기시키는 $Cl^-$ 이온과 부식물을 완전하게 제거하여 탈염처리를 하는 것이 유물 부식을 최대한 지연시킬 수 있는 것이라 생각된다.

• The Journal of the Acoustical Society of Korea
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• v.28 no.3
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• pp.222-228
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• 2009

This study compared the sound spectrums of pyeonjong remains and pyeonjong replica to investigate tuning ways of bells. pyeonjong remains, exhibited at King Sejong Memorial Museum and pyeonjong replica, played at the National Center for Korean Traditional Performance Arts were analyzed. To get mode frequencies and mode shapes, pyeonjong replicas' sound spectrums were analyzed and modal analyses by TV holography were performed. Also pyeonjong remains' sound spectrum were analyzed. Nominal frequencies on the pyeonjong replica and remains showed differences in a range between 9.8 cent and 203 cent. Two facts were inferred as causes of the differences, the tuning conditions of pyeonjong remains were not good and C4 in western tempered scale was preferred as the sound standard of Kukak, whangjong. Relative ratio of higher mode frequencies to the nominal frequencies were calculated to figure out tonal differences between two pyeonjongs. The differences in relative ratio of higher mode frequencies except (3,0)a and (3,0)b modes were significants as well as beyond the just noticeable difference. These results implied that the tonal differences between two pyeonjongs could exist. More pyeonjong remains are needed to be investigated to confirm this result in addition to the analyses of alloy components and bell structure of pyeonjong remains and replica.

• Conservation Science in Museum
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• v.27
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• pp.57-66
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• 2022

This study conducted conservation treatment of a briefcase used by a soldier who fought in the Korean War as a member of the United Nations Forces. The zooid characteristics of its main material, leather, were analyzed in collaboration with the researchers at the National Palace Museum of Korea who have conducted relevant research. A plan for conservation treatment was established based on the results of this analysis. The briefcase was made of leather with a wooden frame. The many densely arranged tiny pores in different patterns on the leather's surface suggests calf leather. The wooden frame and leather had suffered deformation over long years of deterioration and thus required conservation treatment to enhance their structural stability. The conservation treatment began with the removal of contaminants from the exterior and interior of the briefcase. The stiffened leather was softened through humidification, and torn or separated areas were restored using cowhide glue. It is expected that the results of this conservation treatment and analysis of the leather material will serve as useful sources for basic research on leather items as well as wartime and military items.

• Journal of the Korean Wood Science and Technology
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• v.46 no.3
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• pp.260-269
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• 2018

The purpose of this study is to interpretate the tools and the method of making wooden artifacts by analyzing the trace of tools on the surface of wooden artifacts estimated to be from the 2nd to the 4th century. As a result of analyzing the trace of tools on the surface of 97 items of wood artifacts, it was confirmed that various tools such as rhizome, chisel, claw, hand knife and ax were used to make these artifacts. Particularly, the marks of the turning knife and the turning lathe were confirmed, and it was found that the method of turning operation was used at this time. In addition, it was confirmed that both the Nunjil (tangential process) and the Seonjil (longitudinal process) were used to produce the wooden container artifacts by turning operation. It observes that proper processing method operation was applied to manufacture wooden container artifact depending on its form and intended use.

• Journal of Conservation Science
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• v.28 no.1
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• pp.75-86
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• 2012

Iksan Mireuksaji Stone pagoda was built A.D. 639 when King Moo was governing Baekje, in which Sarira has been enshrined in a hole dug in the stereobate for 1,370 years. In South Korea, about 150 cases of Sarira have been found so far. In this connection, many studies have been conducted on how to manage it and on its genesis, but there have been no data on environments to which it has been exposed. In this study, accordingly, researches were made into environments to which Sarira has been exposed as well as into how much it has been damaged under the environments. Sarira in wooden pagodas was influenced greatly by water, but that in stone pagodas by saturated relative humidity. Thus, Sarira in the containers was significantly influenced by the outside temperature for 1 to 2 days, but had no any reaction to humidity. The time it took for the humidity in a Sarira container to reach its maximum, varied depending upon the humidity of the day when Sarira was enshrined. In the case of this pagoda, the humidity reached its maximum 30 days later.