• Title/Summary/Keyword: 유리미세 구조물

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An Experimental Study on the Degradations of Material Properties of Vinylester/FRP Reinforcing Bars under Accelerated Alkaline Condition (급속 알칼리 환경하에서의 비닐에스터/FRP 보강근의 재료성능 저하 특성에 관한 실험적 연구)

  • Oh, Hongseob;Kim, Younghwan;Jang, Naksup
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.23 no.2
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    • pp.51-59
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    • 2019
  • There is increasingly more research focusing on the application of FRP reinforcing bars as an alternative material for steel reinforcing bars, but most such research look at short term behavior of FRP reinforced structures. In this study, the microscopic analysis and tensile behavior of Basalt and Glass FRP bars under freezing-thawing and alkaline conditions were experimentally evaluated. After 100 cycles of the freezing and thawing, the tensile strength and elastic modulus of FRP bars decreased by about 5%. In the case of microstructure of FRP bars during the initial 20 days, no significant damages of FRP bar sections were found under $20^{\circ}C$ alkaline solution; however, the specimens immersed in $60^{\circ}C$ alkaline solution were found to experience resin dissolution, fiber damage and the separation of the resin-fiber interface. In the alkaline environment, the strength decrease of about 10% occurred in the environment at $20^{\circ}C$ for 100 days, but the tensile strength of FRPs exposed for 500 days decreased by 50%. At temperature of $40^{\circ}C$ and $60^{\circ}C$, an abrupt decrease in the strength was observed at 50 and 100 days. Especially, the tensile strength decrease of Basalt fiber Reinforced Polymer bars showed more severe degradation due to the damage caused by dissolution of resin matrix and fiber swelling in alkaline solution. Therefore, in order to improve the long-term performance of the surface braided FRPr reinforcing bars, surface treatment is required to ensure alkali resistance.

Dechlorination/Solidification of LiCl Waste by Using a Synthetic Inorganic Composite with Different Compositions (합성무기복합체 조성변화에 따른 모의 LiCl 염폐기물의 탈염소화/고형화)

  • Kim, Na-Young;Cho, In Hak;Park, Hwan-Seo;Ahn, Do-Hee
    • Journal of Nuclear Fuel Cycle and Waste Technology(JNFCWT)
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    • v.14 no.3
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    • pp.211-221
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    • 2016
  • Waste salt generated from a pyro-processing for the recovery of uranium and transuranic elements has high volatility at vitrification temperature and low compatibility in conventional waste glasses. For this reason, KAERI (Korea Atomic Energy Research Institute) suggested a new method to de-chlorinate waste salt by using an inorganic composite named SAP ($SiO_2-Al_2O_3-P_2O_5$). In this study, the de-chlorination behavior of waste salt and the microstructure of consolidated form were examined by adding $B_2O_3$ and $Fe_2O_3$ to the original SAP composition. De-chlorination behavior of metal chloride waste was slightly changed with given compositions, compared with that of original SAP. In the consolidated forms, the phase separation between Si-rich phase and P-rich phase decreases with the amount of $Al_2O_3$ or $B_2O_3$ as a connecting agent between Si and P-rich phase. The results of PCT (Product Consistency Test) indicated that the leach-resistance of consolidated forms out of reference composition was lowered, even though the leach-resistance was higher than that of EA (Environmental Assessment) glass. From these results, it could be inferred that the change in the content of Al or B in U-SAP affected the microstructure and leach-resistance of consolidated form. Further studies related with correlation between composition and characteristics of wasteform are required for a better understanding.

Ultrastructure of the Integument of Adult Paragonimus westermani (폐흡충 표피의 미세구조)

  • 최원영;유재을
    • Parasites, Hosts and Diseases
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    • v.23 no.1
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    • pp.111-122
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    • 1985
  • The present study was performed to observe the ultrastructure of the integument of adult Paragonimus westermani. Dogs experimentally infected with 60 metacercariae of F. westermani were autopsied 4 months after the infection. Adult p. westermani were extracted from the dogs and the fine structure was studied by means of scanning and transmission electron microscope. The findings are as follows: 1. Scanning electron microscopic findings showed that the spines and the papillae are distributed at whole body surface but the well developed spines or papaillae are shown around the oral sucker and ventral sucker. 2. At the end of the body, excretory pore was found, the shape was irregular. 3. Transmission electron microscopic findings showed that plasma membrane, tegument, basal lamina, connective tissue, circular muscle layer, longitudinal muscle layer. nerve axon and tegumental cell were observed. 4. In higher magnification, plasma membrance and bar-shaped granules were found at the outer surface of the tegument.

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77-GHz Slot Array Antenna Using PCB and ACF (PCB와 ACF를 이용한 77 GHz 슬롯 배열 안테나)

  • Yoon, Pyoung-Hwa;Kwon, Oh-Yun;Song, Reem;Kim, Byung-Sung
    • The Journal of Korean Institute of Electromagnetic Engineering and Science
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    • v.29 no.10
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    • pp.752-757
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    • 2018
  • This study presents the performance evaluation results of a 77-GHz waveguide slot array antenna that was fabricated by attaching a patterned printed circuit board(PCB) on a metal block. The 77-GHz waveguide was divided into a top plate and a bottom structure. The top plate was fabricated using a patterned PCB that can implement a fine slot at low cost. The top cover was then bonded to the bottom metal structure with a waveguide trough using anisotropic conductive film. For evaluating the antenna performance, a $1{\times}16$ slot array antenna was fabricated using our proposed method and the gain and pattern were measured and compared with the simulation results. Though the measurement results demonstrate a reduction in gain of around 2.3~3.5 dB compared to the simulation results assuming ideal bonding conditions, the pattern hardly changed and the slot antenna with a gain of approximately 17 dBi at 77 GHz can be easily manufactured at a low cost using the proposed method.

IGZO 박막트렌지스터의 열처리 조건에 따른 Ti/Au 전극 연구

  • Lee, Min-Jeong;Choe, Ji-Hyeok;Gang, Ji-Yeon;Myeong, Jae-Min
    • Proceedings of the Materials Research Society of Korea Conference
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    • 2010.05a
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    • pp.54.1-54.1
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    • 2010
  • 산화물 기반의 TFT는 유리, 금속, 플라스틱 등 기판 종류에 상관없이 균일한 제작이 가능하며, 상온 및 저온에서 대면적으로 제작이 가능하고, 저렴한 비용으로 제작 가능하다는 장점 때문에 최근 많은 연구가 이루어지고 있다. 현재 TFT 물질로 많이 연구되고 있는 산화물은 ZnO (3.4 eV)나 InOx (3.6 eV), GaOx (4.9 eV), SnOx(3.7 eV)등의 물질과 각각의 조합으로 구성된 재료들이 주로 사용되고 있으며, 가장 많은 연구가 이루어진 ZnO 기반의 TFT는 mobility와 switching 속도에서 우수한 특성을 보이나, 트렌지스터의 안정성이 떨어지는 것으로 보고 되고 있다. 그러나 IGZO 물질의 경우 결정학적으로 비정질이며 상온 및 저온에서 대면적으로 제작이 가능하고, 높은 전자 이동도의 특성을 가지고 있는 장점 때문에 최근 차세대 산화물 트렌지스터로 각광받고 있다. IGZO TFT 소자의 경우 Ag, Au, In, Pt, Ti, ITO 등 다양한 전극 물질이 사용되고 있는데, 이들 중 active channel과 ohmic contact을 이루는 Al, Ti, Ag의 적용을 통해 향상된 성능을 얻을 수 있다. 하지만 이들 전극 재료는 TFT 소자 제작시 필수적인 열처리 공정에 노출되면서 active channel 과 전극 사이 계면에 문제점을 야기할 수 있다. 특히, Ti의 경우 산화가 잘되기 때문에 전극계면에 TiO2를 형성하여 contact resistance의 큰 영향을 미치는 것으로 보고 되고 있다. 본 연구에서는 ohmic 전극재료인 Ti 또는 Ti/Au를 적용하여 TFT 소자 제작 및 특성에 대한 평가를 진행했으며, 열처리에 따른 전극과 IGZO 계면 사이의 미세구조와 전기적인 특성간의 상관관계를 연구하였다. 이를 통해, 소자 제작 공정을 최적화하고 신뢰성 있는 소자 특성을 얻을 수 있었다.

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Engineering Geological Implications of Fault Zone in Deep Drill Cores: Microtextural Characterization of Pseudotachylite and Seismic Activity (시추코어 단층대에서의 지질공학적 의미: 슈도타킬라이트의 미세조직의 특징과 지진활동)

  • Choo, Chang-Oh;Jeong, Gyo-Cheol
    • The Journal of Engineering Geology
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    • v.27 no.4
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    • pp.489-500
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    • 2017
  • It is not rare that pseudotachylite, dark colored rock with glassy texture, is recognizable in deep core samples drilled up to 900 m from the surface. Pseudotachylite with widths varying few to 20 cm is sharply contacted or interlayered with the host rocks composed of Jurassic granite and Precambrian amphibolite gneiss, showing moderately ductile deformation or slight folding. Pseudotachylite occurring at varying depths in the deep drill core are slightly different in texture and thickness. There is evidence of fault gouge at shallower depths, although brittle deformation is pervasive in most drill cores and pseudotachylite is identified at random depth intervals. Under scanning electron microscope (SEM), it is evident that the surface of pseudotachylite is characterized by a smooth, glassy matrix even at micrometer scale and there is little residual fragments in the glass matrix except microcrystals of quartz with embayed shape. Such textural evidence strongly supports the idea that the pseudotachylite was generated through the friction melting related to strong seismic events. Based on X-ray diffraction (XRD) quantitative analysis, it consists of primary minerals such as quartz, feldspars, biotite, amphibole and secondary minerals including clay minerals, calcite and glassy materials. Such mineralogical features of fractured materials including pseudotachylite indicate that the fractured zone might form at low temperatures possibly below $300^{\circ}C$, which implies that the seismic activity related to the formation of pseudotachylite took place at shallow depths, possibly at most 10 km. Identification and characterization of pseudotachylite provide insight into a better understanding of the paleoseismic activity of deep grounds and fundamental information on the stability of candidate disposal sites for high-level radioactive waste.

Contact fatigue and strength degradation in dental ceramics (치아용 세라믹스에서의 접촉피로 및 강도저하)

  • 정연길;이수영;최성철
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.9 no.5
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    • pp.527-533
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    • 1999
  • Hertzian indentation tests with spherical indenters in water were conducted to examine the contact fatigue in three dental ceramics, such as feldspathic porcelain, micaceous glass-ceramic (MGC) and glass-infiltrated alumina, which was used as dental restorations, and evaluated the effect of contact damage on strength. Initial damage was dependent of microstructure, showing cone cracks of brittle behavior in the feldspathic porcelain and deformation of quasi-plastic behavior in the MGC, with an intermediate case in the glass-infiltrated alumina. However, as increasing the number of cyclic loading (n=1~n =$10^6$)all materials showed an abrupt strength degradation, at which fracture was originated from damage in the contact fatigue. There were two strength degradation with increasing the number of cyclic loading in specific loads (200N, 500N, 1000N):first was from the cone cracks, and second was from the radial cracks created by cyclic loading. The radial cracks, once formed, led to rapid degradation in strength properties, Finally the material was failed at the high number of cyclic loading. Strength degradation with indentation load at fixed number of cyclic loading indicated that the feldspathic porcelain should be highly damage tolerant to the contact fatigue.

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Environmental Mineralogical Study on Weathering of the Western Stone Pagoda in Gameun Temple by Sea Salts Spray (해염(Sea Salts) 분무에 의한 감은사지 삼층석탑(서탑)의 풍화현상에 관한 환경광물학적 연구)

  • Sung, So Young;Kim, Soo Jin;Park, Chan Soo
    • 한국문화재보존과학회:학술대회논문집
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    • 2004.03a
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    • pp.78-91
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    • 2004
  • 염(Salts)은 일반적으로 가장 강력한 풍화요인 물질 중 하나이다. 염의 결정화(crystallization) 및 수화(hydration)작용은 석재의 화학적 풍화 뿐만이 아니라 물리적 풍화를 가속화 시킨다. 감은사지 석탑은 오랜 세월 대기 중에 노출되어 대기환경오염으로 인한 화학적 풍화 뿐만이 아니라 지리적으로 바다에 인접해 있어 바다에서 기원한 염화나트륨(NaCl)의 영향으로 다른 석조물에 비해 심한 물리적 풍화현상을 보이고 있다. 편광 현미경 및 SEM, XRD, XRF를 이용하여 석탑의 구성석재 및 염(salts)에 대한분석을 실시하였으며, 용출실험을 통해 얻은 용액에 대해서는 IC와 ICP-AES를 이용하여 분석하였고, 염류와 석재의 반응산물로 만들어진 염에 대해서는 정방위시료와 부정방위시료를 제작하여 분석하였다. 감은사지 석탑을 이루는 암석은 결정응회암으로 주 구성 광물은 사장석 및 정장석이며 소량의 석영 및 흑운모 등이 함유되어 있고 소량의 유리질 석기로 구성되어 있다. 석재의 표면에는 주 구성 광물들의 화학적 풍화로 인해서 생성된 2차 광물로 팽창성 점토광물인 스멕타이트가 존재하며, 대기오염물질과의 결합에 의해 생성된 대표적인 황산염인 석고$(gypsum,\;CaSO_4{\cdot}2H_2O)$, 소금(halite, NaCl), 해양기원 염류인 소금성분과 대기오염물질이 만들어낸 테나다이트$(thenardite,\;Na_2SO_4)$가 존재한다. 이들 염류는 일차적으로 암석의 표면에 백화현상을 초래하기도 하고, 대기 중의 오염물질과 결합하여 일부는 흑화현상을 보이기도 한다. 또한 암석 내 수분이 증가할 경우 이들 염들이 암석의 공극이나 열극을 따라 내부로 이동하여 subflorescence를 발생시켜 박락 및 박탈의 원인이 되었으며, 온도와 수분의 변화에 따른 이들 염(salts)의 수화 및 결정 작용 그리고 새로운 염(salts)의 침전작용을 반복하면서 석재 내부와 외부의 암석 및 결정에 균열과 미세열극 등이 생성되어 석재 자체의 구조적 안정성에 영향을 주고 있다. 따라서 감은사지 석탑은 지리적 환경 차이로 인해 일반적인 환경의 석조물들과는 다른 형태의 풍화양상을 보이고 있어서 풍화양상 및 풍화형태에 대한 정확한 연구와 이해를 바탕으로 보존대책이 마련되어야 한다.

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Study on the Property of Sintered Silver Clay for Rapid Modeling (신속 조형용 은점토 소결체의 물성 연구)

  • Kim, Jun-Hwan;Kim, Keum-Jong;Kim, Myung-Ro;Song, Oh-Sung
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.9 no.6
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    • pp.1548-1554
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    • 2008
  • The market of silver precious metal clay (PMC) is promising as its application for agile metal craft. The property of suitable hardness and shrinkage as well as environment-safe is strictly required as people make the final product with bare hands. We propose a silver PMC with new organic binder made of palm oil, glycolic acid and water. Then we prepared disk specimen of our proposed PMC and well-known commercial PMC. We investigated the hardness, weight change, linear shrinkage, density and micro structure evolution with sintering temperature of $700{\sim}900^{\circ}C$ ($50^{\circ}C$ gap) for 15minutes. We confirm our proposed PMC has suitable property for craft product comparable for commercial PMC, and the optimum sintering condition is $850^{\circ}C$-15minutes for metal craft application.

Effect of In2O3 Doping on the Properties of ZnO Films as a Transparent Conducting Oxide (투명전도성 ZnO 박막의 특성에 미치는 In2O3 첨가에 따른 영향)

  • Lee, Choon-Ho;Kim, Sun-Il
    • Journal of the Korean Ceramic Society
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    • v.41 no.1
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    • pp.57-61
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    • 2004
  • Zinc Oxide (ZnO) have the crystal structure of wurtzite which is semiconducting oxide with band gap energy of 3.3eV. $In_2O_3$-doped ZnO films were fabricated by electron beam evaporation at $400^{\circ}C$ and their characteristics were investigated. The content of $In_2O_3$ in ZnO films had a marked effect on the electrical properties of the films. As $In_2O_3$ content decreased. $In_2O_3$-doped ZnO films was converted amorphous into crystallized films and showed a better characteristics generally as a transparent conducting oxide. As $In_2O_3$-doped ZnO films were prepared by $In_2O_3$-doped ZnO pellet with 0.2at% of $In_2O_3$ content, the value of resistivity was about $6.0 {\times} 10^{-3} {\Omega}cm$. The transmittance was higher than 85% throughout the visible range.