• Journal of Sericultural and Entomological Science
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• v.15 no.2
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• pp.45-53
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• 1973

1. The sericin solubility increased rapidly as the increase of water M-alkalinity. 2. The acidity of the treated water was nutralized at the over 25ppm of M-alkalinity. 3. The more M-alkalinity of the sample water is, the more M-alkalinity was found after cocoon treat. 4. The total hardness of sample water seemed to be droped as M-alkalinity increased. 5. The sericin solubility also seemed to be droped as the increase of water acidity. 6. In case of treat finish with cocoon, the acidity and total hardness seemed to increase as the acidity of the water increased, but M-alkalinity was nutralized at 20~40 ppm of water acidity or the M-alkalinity could not be found in case over 40ppm of acidity. 7. In case increase of iron component with sample water, sericin solubility seemed to drop down, and mangan component showed the same nature but dull drop. 8. After cocoon was treated with water, acidity, M-alkalinity and total hardness were increased by the extraction from cocoon shell because of pH and treating temperature but not because of iron componnent. Mangan component, however, affected as to increase of acidity and total hardness but to decrease for M-alkalinity. 9. In case change of M-alkalinity and total hardness, sericin solubility has increased also. 10. In case constant pH and total hardness, the more M-alkalinity is, the more sericin solubility was found. 11. In case constant pH, total hardness, and M-alkalinity, the more acidity is, the less sericin solubility was found. 12. In case constant pH(6.8) and M-alkalinity, the more total hardness is, the less sericin solubility was found. 13. Though the combination of water, high solubility water, medium solubility water and low solubility water were prepared. The high solubility water desolved sericin 2.2% more than low solubility water. And the medium solubility water desolved sericin as much as 2.4~2.9%. 14. It was found that the most important factors for filature water are pH, M-alkalinity, acidity and total hardness which may need more words for optimum filature water development. 15. In case of repeat use of water, the buffer action of water has increased so that the sericin solubility to be decreased.

• Journal of Sericultural and Entomological Science
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• v.30 no.1
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• pp.33-39
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• 1988

In the case of white cocoon, the fluorescence colors are classified as a yellowish fluorescence cocoon(Y.F.C.) and a violet fluorescence cocoon(V.F.C.) by exposing to ultra-violet ray. Accordingly, experiments were carried out to investigate the difference of sericin behaviors between Y.F.C. and V.F.C. by measuring the sericin solubility, surface tension and viscosity of the sericin solution. Also, the reelability of two different type of cocoons was investigated in the silk reeling process. The results were summarized as follows; 1. The sericin solubility of Y.F.C. shell is higher than that of V.F.C. shell with the dissolution temperature and time. It is shown that the sericin solubility curves of Y.F.c. and V.F.C. are similar in shape, but the difference of sericin solubility between Y.F.C. and V.F.C. is more significant at higher bath temperature. 2. The initial sericin dissolution curves of Y.F.C. and V.F.C. cocoon shell can be divided by four parts within the range of dissolving time from 5 minutes to 60 minutes. The initial dissolution velocity of Y.F.C. shell is faster than that of V.F.C. but the velocity difference is negligible after 30 minutes of dissolving time. 3. The gelation of V.F.C. sericin solution is faster than that of Y.F.C. at early stage(in the range of 15 minutes to 60 minutes). 4. In the silk reeling process, the reelability of Y.F.C. is better than that of V.F.C. with about 11%. This is mainly due to the higher sericin solubility in Y.F.C. followed by the fast dissolution velocity.

• Journal of the Korean Geotechnical Society
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• v.27 no.12
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• pp.17-25
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• 2011

A fabric of soil media may change due to certain factors such as dissolution of soluble particles, desiccation, and cementation. The fabric changes affect the mechanical behavior of soils. The purpose of this study is to investigate the effects of geo-material dissolution on shear strength. Experiments and numerical simulations are carried out by using a conventional direct shear and the discrete element method. The dissolution specimens are prepared with different volumetric salt fraction in sand soils. The dissolution of the specimens is implemented by saturating the salt-sand mixtures at different confining stresses in the experimental study or reducing the sizes of soluble particles in the numerical simulations. Experimental results show that the angle of shearing resistance decreases with the increase in the soluble particle content and the shearing behavior changes from dilative to contractive behavior. The numerical simulations exhibit that macro-behavior matches well with the experimental results. From the microscopic point of view, the particle dissolution produces a new fabric with the increase of local void, the reduction of contact number, the increase of shear contact forces, and the anisotropy of contact force chains compared with the initial fabric. The shearing behavior of the mixture after the particle dissolution is attributed to the above micro-behavior changes. This study demonstrates that the reduction of shearing resistance of geo-material dissolution should be considered during the design and construction of the foundation and earth-structures.

• Analytical Science and Technology
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• v.23 no.6
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• pp.511-517
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• 2010

Dissolution procedure of vanadium pentoxide, which is widely used as a catalyst for production of sulfuric acid or an oxide reaction of the numerous organic compounds, was investigated. Reagent of vanadium pentoxide was completely dissolved in aqua regia-$H_2O_2$-HF solution, but plate type of vanadium pentoxide sample was not clearly dissolved with mixed acids. Thus, in order to establish the dissolution procedure for plate type of vanadium pentoxide, the solubility of vanadium pentoxide was investigated through comparison of acid treatment-fusion and microwave digestion methods. The optimized acid for dissolution of vanadium compound was found to be mixing acids of aqua regia, $H_2O_2$ and HF. Acid-fusion and microwave digestion methods have a similar property in the solubility of vanadium compound, but the latter was more quick and convenient procedure. The content of vanadium pentoxide was found to be $97.9{\pm}0.9%$ using an inductively coupled plasma atomic emission spectrometer after dissolution of a sample with the microwave digestion system.

• Proceedings of the Korean Institute of IIIuminating and Electrical Installation Engineers Conference
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• 2005.05a
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• pp.402-405
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• 2005

부양용해 기술은 티타늄등 용해 및 주조에 어려움이 있는 기능성 금속의 용해 시 소재의 오염이나 고가의 도가니 없이 용해할 수 있는 기술로써 기계 부품 경량화 및 고강도를 위한 기술 및 신수요 창출을 위한 기반을 제공할 수 있다. 본 논문은 실기용 부양용해 cold crucible의 설계 및 제작에 앞서 실기 제작할 cold crucible에 대한 기초 자료를 바탕으로 컴퓨터 시뮬레이션을 위한 부양체를 포함한 3차원 전자기장 해석 model을 구축하여, 실제 cold crucible 설계 제작 시 다양한 형태로 활용될 수 있는 기본자료를 확보하는데 그 목적이 있다.

• Proceedings of the Korean Institute of Surface Engineering Conference
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• 2002.05a
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• pp.2-2
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• 2002

Quartz Crystal Microbalance(QCM)은 표면에 묻은 물질의 미량의 무게변화도 간단히 측정 할 수 있어 반웅기 내에서 일어나는 현상올 in-situ로 즉시 알 수 있는 장점을 가진 장치이 다. 이 장치를 이용하면 초엄계 이산화탄소 내에서 용해도를 알 수 있고, 대상물질이 녹아냐 가는 속도를 측정하면 확산계수를 구할 수 있다. 그리고, 초음파 혼을 반응용기 내에 설치하 고, 초음파 효과를 알아보았다. 먼저 static system에서 초음파 효과를 알아보았다. Cu(acac)2를 대상으로, 밀폐된 용기에서 수행한 실험에서, 액체와 초임계 이산화탄소 내에서 용해속도를 QCM으로 구할 수 있었다. 용해속도로부터 Cu(acac)2의 확산계수를 측정할 수 있었다. 액체 내에선 $10^{-4}{\;}cm2/sec$, 초임계상태에서 $10^{-2}{\;}cm2/sec$의 값을 갖는 것으로 나타 났다. 그리고, 초음파를 사용할 경우 이 확산계수값이 4-5배정도 증가하는 것으로 냐타났다. 이어서 dynamic system에서 반응을 알아보았다. Cyanex를 함유한 C02를 반응용기에 흘리 면서 QCM표면에 묻은 Co이온의 용해속도를 측정하였다. 초음파는 용해도에 아무 역활을 안하는 것으로 나타났다. 주어진 조건에서 13 microgram/gram-cyanex의 용해도를 갖는 것 으로 나타났다.

• Proceedings of the KAIS Fall Conference
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• 2008.11a
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• pp.397-399
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• 2008

흡착식 건조공정에서 가장 중요한 부분은 건조에 활용되는 용해제(Desiccant) 라고 할 수 있다. 그러나 국내에서 흡착식 건조기에 사용되는 대부분의 용해제는 수입에 의존하고 있는 실정이다. 그러므로 본 연구에서는 흡착식 제습 설비의 제작 능력을 기초로 하여 용해제의 자체 개발을 통하여 안정적인 기술력의 확보로 국내에서 친 환경적이며 무동력으로 사용할 수 있는 용해성 흡습제에 관한 연구를 진행하고자 한다. 이를 위해 알칼리성 흡수제를 합성하기 위하여 KCl, NaCl 그리고 $CaCl_2$ 등의 물질을 질량비로 일정비율이 되도록 수용액에 용해시켜 교반속도가 유지되는 회분식 반응기에서 일정시간 동안 반응 시킨 후 일정온도 범위에서 일정시간동안 건조시켜 시료를 제조 하여 흡습제의 조습특성을 분석하였다.

• Journal of the Korean Chemical Society
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• v.32 no.4
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• pp.311-317
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• 1988

The solubilities of naphthalene in ammonia could be measured at various temperatures and pressures above the critical point of ammonia to represent the relationship between the solubility and the density of ammonia at desired temperature and pressure by means of a simple equation. This equation allows a calculation of the solubilities at higher and lower pressures. Using the equation, the solution energies, the solution entropies, and the second cross virial coefficients between naphthalene and ammonia have been determined to be compared with those in the case of the dissolution of naphthalene in supercritical carbon dioxide.

• Proceedings of the KIEE Conference
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• 2003.07b
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• pp.885-887
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• 2003

부양용해 기술은 티타늄등 용해 및 주조에 어려움이 있는 기능성 금속의 용해 시 소재의 오염이나 고가의 도가니 없이 용해할 수 있는 기술로써 기계 부품 경량화 및 고강도를 위한 기술 및 신수요 창출을 위한 기반을 제공할 수 있다. 본 논문은 실기용 부양용해 cold crucible의 설계 및 제작에 앞서 모사 cold crucible에 대한 기초 자료를 바탕으로 컴퓨터 시뮬레이션을 위한 3차원 전자기장 해석 model을 구축하여, 모사 모델과의 측정값과 전자장 해석결과를 비교하여, 실제 cold crucible 설계 제작시 다양한 형태로 활용될 수 있는 기본자료를 확보하는데 그 목적이 있다.

• Journal of Energy Engineering
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• v.13 no.4
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• pp.301-310
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• 2004

Carbon dioxide ocean disposal is one of the promising options to reduce carbon dioxide concentration in the atmosphere. So, in the present study, calculations of the solubility, the surface concentration and the dissolution behavior of carbon dioxide when liquid carbon dioxide is released at 1,000m and 1,500m in depth are performed. The results show that liquid carbon dioxide changes to carbon dioxide bubbles around 500m in depth, and the hydrate acts as a resistant layer for the dissolution of liquid carbon dioxide. Also. the injection of liquid carbon dioxide from a moving ship is more effective than that from a fixed pipeline.