• Applied Chemistry for Engineering
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• v.32 no.6
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• pp.621-626
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• 2021

A sequential design of experiments was used to optimize MOF-801 synthesis process. For the initial screening, a general 2^k factorial design was selected followed by the central composition design, one of the response surface methods. A 2³ factorial design based on the molar ratio of fumaric acid, dimethylformamide (DMF), and formic acid was performed to select the more suitable response variable for the design of experimental method among the crystallinity and BET specific surface area of MOF-801. After performing 8 synthesis experiments designed by MINITAB 19 software, the characteristic analysis was performed using XRD analysis and nitrogen adsorption method. The crystallinity with R² = 0.999 was found to be more suitable for the experimental method than that of BET specific surface area. Based on analysis of variance (ANOVA), it was confirmed that the molar ratio of fumaric acid and formic acid was a major factor in determining the crystallinity of MOF-801. Through the response optimization and contour plot of two factors, the optimal molar ratio of ZrOCl₂·8H₂O : fumaric acid : DMF : formic acid was 1 : 1 : 39 : 35. In order to optimize the synthesis process, the central composition design on synthesis time and temperature was performed under the identical molar ratio of precursors. The results derived through the designed 9 synthesis experiments were calculated using the quadratic model equation. Thus, the maximum crystallinity of MOF-801 predicted under the synthesis time and temperature of 7.8 h and 123 ℃, respectively.

• Journal of the Korean Data and Information Science Society
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• v.20 no.6
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• pp.1015-1027
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• 2009

Many problems of confounding and identifiability for polynomial models in an experimental design can be solved using methods of algebraic geometry. The theory of $Gr\ddot{o}bner$ basis is used to characterize the design. In addition, a fractional factorial design can be uniquely represented by a polynomial indicator function. $Gr\ddot{o}bner$ bases and indicator functions are powerful computational tools to deal with ideals of fractions based on each different theoretical aspects. The problem posed here is to give how to move from one representation to the other. For a given fractional factorial design, the indicator function can be computed from the generating equations in the $Gr\ddot{o}bner$ basis. The theory is tested using some fractional factorial designs aided by a modern computational algebra package CoCoA.

• Asia-Pacific Journal of Business Venturing and Entrepreneurship
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• v.11 no.3
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• pp.49-61
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• 2016

This study investigates the relationship between fear of failure of potential entrepreneur's psychological characteristics and entrepreneurial intentions using the mediation variables of planned behavior model. There are many existing prior research related to the entrepreneurial intentions, but they were mostly focused only entrepreneurial success factors. So in this study we focused on fear of failure of potential entrepreneur. To know the influence of the fear of failure related to entrepreneurial intention, we using the scale of PFAI (Performances Failure Appraisal Inventory). The purpose of this study is to examine an impact of fear of failure on entrepreneurial intention and add to mediating factors - attitude toward the acts, subjective norm, perceived behavior control - on the relationship between fear of failure and entrepreneurial intention. Also we examined entrepreneurial education as moderating effect in order to offset the fear of failure. In order to test research model, we collected data from 321 undergraduate students. To test the research questions and hypotheses, we employed SPSS 21.0 anf AMOS 18.0 for validity, reliability, confirmatory factor analysis, and structural model analysis. The results were as follows. First, the fear of failure negatively related to attitude toward the behavior and subjective norm. Second, attitude toward the behavior and subjective norm positively related to entrepreneurial intention in consistent with previous studies. Third, attitude toward the acts and subjective norm in TPB variables have full-mediation effects between fear of failure and intrepreneurial intention. Fourth, The moderating effects of entrepreneurial effect was not significant. The negative relationship between fear of failure and attitude toward the acts and subjective norm was even slightly stronger who have taken the entrepreneurial class group. We discuss the theoretical and managerial implications, and provide suggestions for future research.

• 한국신재생에너지학회:학술대회논문집
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• 2010.06a
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• pp.66.2-66.2
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• 2010

미니탭(Minitab) 프로그램에 있는 실험계획법(Design of experiment)를 이용하여 박막실리콘 I-layer의 주효과 및 교호작용에 대한 연구를 실시하였다. I-layer의 주요 특성은 증착속도 및 전도도에 대하여 분석을 하였으며, 최종적으로 선택된 증착조건을 사용하여 비정질 실리콘 태양전지를 제조하여 확인 하였다. 실험설계는 2수준 5인자 완전설계요인법을 사용하였다. 분석결과 단막의 증착속도에 영향을 주는 주효과로는 Power와 E/S거리고 나타났으며, Power와 E/S거리, Power와 Pressure에서 큰 교호작용이 일어남을 확인 할 수 있었다. 암전도의 영향을 주는 주효과는 Sub. Temp.를 제외하고는 모두 영향을 주고 있었으며, 상당히 복잡한 교호작용을 이루고 있어 정확한 분석을 할 수는 없었다. 광전도도의 경우도 주효과에서 SiH4 flow rate를 제외하고는 모두 영향을 주고 있었으며, 복잡한 교호작용으로 정확한 분석이 어려웠다. 따라서 P-value를 분석하여 최종 R-제곱값이 증착속도는 97%이상의 높은 값을 얻었으나 전도도의 경우 최대차수 3차항으로 70~80%정도의 낮은 값을 얻었을 수 있었다. 낮은 값을 얻은 이유로는 실험설계시 몇몇 조건이 불안정한 plasma 상태로 인하여 전도도의 측정 편차가 커 분석오차가 높았을 것으로 추정된다. 암전도를 망소특성, 광전도도를 망대특성으로 광민감도 $10^5$으로 최적화 하여 비정질 태양전지를 만들어 평가한 결과 약 9%대의 광변환 효율을 얻을 수 있었으나 만족도 40%대의 낮은 값으로 향후 이와 관련한 더 정밀한 측정 및 분석이 요구된다.

• The Journal of Korea Assosiation for Disability and Oral Health
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• v.14 no.2
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• pp.106-110
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• 2018

A 20-year-old male patient with Down syndrome presented with rampant caries and chronic periodontitis on full-mouth. Patient have many oral diseases despite of no abnormalities of medical history, no involuntary tremor, no excessive masticatory pressure, and no limitation of exercise. Also he had no experiences of oral health education of prostheses and oral health management. Therefore, A number of fixed prostheses and denture treatments were performed to caregiver and patient with education for oral hygiene and management. After delivery final prostheses, they had repeated follow-up for checking management.

• Proceedings of the Korean Society of Precision Engineering Conference
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• 2006.05a
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• pp.215-216
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• 2006

The effect of manufacturing parameters on friction characteristics of motorcycle break system was studied using a disk-on-pad type friction tester. Such parameters conditions have an effect on the frictional factor such as applied load, sliding speed, and number of ventilated disk hole. However, it is difficult to know the mutual relation of these factors. In this study, the friction characteristics using design of experiment containing 3 elements were investigated for an optimal condition for the best motorcycle break system employing Full factorial design. From this study, the result was shown that the applied load in frictional factors was the most important, next to sliding speed, number of ventilated disk hole.

• Applied Chemistry for Engineering
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• v.19 no.2
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• pp.179-184
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• 2008

The separation and purification of succinate are necessary for the succinic acid production by a fermentation process. Among the purification processes, desalination of succinate is inevitable. In this work, electrodialysis was selected as a desalination method and its operating parameters affecting the degree of desalination and energy consumption were examined. Commercialized electrodialysis apparatus was used in this work and its optimum operating parameters were determined by using design of experiment (DOE) method. Voltage, concentration of succinate, and pH were selected as main parameters. Among them, voltage seemed to be the most important one. The final conversion of succinate to succinic acid was calculated when the operating parameters were optimized. Finally, the effect of impurities, such as corn steep oil, yeast extract, and dextrose on the electrodialysis efficiency was also studied.

• Journal of the Microelectronics and Packaging Society
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• v.26 no.3
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• pp.51-57
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• 2019

To protect the Cu surface from oxidation in air, a two-step plasma process using Ar and $N_2$ gases was studied to form a copper nitride passivation as an anti-oxidant layer. The Ar plasma removes contaminants on the Cu surface and it activates the surface to facilitate the reaction of copper and nitrogen atoms in the next $N_2$ plasma process. This study investigated the effect of Ar plasma on the formation of copper nitride passivation on Cu surface during the two-step plasma process through the full factorial design of experiment (DOE) method. According to XPS analysis, when using low RF power and pressure in the Ar plasma process, the peak area of copper oxides decreased while the peak area of copper nitrides increased. The main effect of copper nitride formation in Ar plasma process was RF power, and there was little interaction between plasma process parameters.

• Physical Therapy Korea
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• v.10 no.4
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• pp.43-59
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• 2003

보행 종료(gait termination)는 인간의 보행개시(gait initiation)나 율동성 보행(rhythmical walking)에 비해 관심을 적게 받고 있다. 파킨슨 환자들이 보행종료와 방향전환 시 가지는 어려움은 이들 환자들이 보행 시 넘어지게 되는 노출 요인으로 보고되어져 왔다. 보행종료에 대한 기전의 이해는 효과적으로 걸음을 멈추지 못해 넘어지게 되는 위험요인을 가진 사람들에게 적용되어질 수 있다. 이 논문에서 우리는 보행종료에 대한 최근문헌을 고찰하고 우리 실험실에서 진행되어온 파킨슨환자의 보행종료에 관한 일련의 실험들의 결과를 요약하였다. 본 연구는 율동적인 보행상태에서 완전한 멈춤으로의 전환에서 일어나는 동역학의 변화를 검사하기위해 시행되었다. 보행속도가 증가함에 따라 따르는 다리(trailing limb; 보행종료시점에서 뒤에 위치하는 다리)의 유의한 가속력 감소가 나타나고 멈출 때 이끄는 다리(leading limb; 보행종료시점에서 앞에 위치한 다리)에서 유의한 감속력의 증가가 나타난다. 보행종료 시, 이끄는 다리의 뒤쪽에 질량중심(center of mass) 을 유지시키기 위해 하지 신전근의 활성도가 오래 지속되어져야 한다. 예측하지 못한 상황에서 보행종료 시, 보행 중이나 예측되어진 상황에서 멈출 때보다 이끄는 다리 아래에서 감속력이 빠르게 발생하는 경향을 보였다. 대상자들을 보행속도에 따라 두 군으로 나눌 때, 계획되지 않은 보행종료를 하는 동안 보행속도가 느린 군이 빠른 군보다 전방 가속력을 급속하게 증가시키는 것으로 나타났다. 이러한 결과들은 보행속도가 느린 대상자들이 따르는 다리로 힘을 생성하기 보다는 주로 이끄는 다리에 의존하여 보행종료를 하는 것을 보여준다. 따르는 다리에서 발생되는 힘과 근육활성도의 조절을 측정하기 위하여, 파킨슨 환자와 연령에 의해 짝짓기된 정상 환자군에게 표적 조건(target condition)을 추가하였다. 파킨슨 환자군은 표적에 다리를 정확히 놓기 위해 몇 발자국 전부터 보행 속도를 줄였다. 파킨슨 환자들은 보행종료를 촉진하기 위해 필요한 근육들의 활성도를 증가시키는데 큰 어려움을 가지고 있다고 생각되어진다.

• Journal of Nutrition and Health
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• v.50 no.3
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• pp.284-293
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• 2017

Purpose: This study was conducted to examine the behavioral intentions of breastfeeding in single women using the theory of planned behavior. Methods: The questionnaires were distributed to 350 single women in her 20~30s, and 316 respondents were analyzed by descriptive statistics, Spearman's correlation, and multiple regression analysis. Results: The subjects showed strong intentions and favorable attitudes toward breastfeeding. The subjects were more favorably influenced by their mothers, siblings, friends, and coworkers who previously experienced breastfeeding than ones with no breastfeeding experiences. There were significant correlations between breastfeeding intention and attitudes (r = 0.321, p < 0.0001), subjective norms (r = 0.434, p < 0.0001), and perceived control (r = 0.307, p < 0.0001). However, regression analysis with two different age groups revealed that subjective norms (p < 0.0001) and perceived control (p < 0.001) contributed to the model of explaining breastfeeding intentions in subjects who were 25 years old or younger, whereas attitudes did not. In addition, subjects who were more than 25 years old showed that attitudes (p < 0.003) and subjective norms (p = 0.002) contributed to the model of explaining breastfeeding intentions while perceived control (p < 0.070) showed less contribution. Conclusion: These results suggest that the theory of planned behavior can be a useful tool to increase the rate of breastfeeding intentions in single women when designing educational materials, which requires consideration of age differences.