• 제목/요약/키워드: 온도회복

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Effects of Heat-treatments on Discharge Characteristics of TiFe1-xNix Alloy Electrodes for Ni/MH Secondary Battery (Ni/MH 2차전지용 TiFe1-xNix 합금전극의 방전특성에 대한 열처리의 영향)

  • Joung, Soon-dol;Joung, Sang-sik;Ahn, Hyo-jun;Kim, Ki-won
    • Journal of Hydrogen and New Energy
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    • v.9 no.4
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    • pp.135-141
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    • 1998
  • The effects of heat-treatment on discharge characteristics of $TiFe_{1-x}Ni_x$ alloy were investigated. The content of Ni in alloy was varied from x = 0.1 to 0.6 by each 0.1 increment. Discharge capacity change of each alloy with C/D cycles was measured. With increasing Ni-content initial discharge capacity was increased. but at x = 0.6 it was deceased again. With increasing C/D cycles discharge capacity was rapidly decreased in the alloy of high Ni-content. In order to investigate the effects of heat-treatment on cycle life, $TiFe_{0.5}Ni_{0.5}$ alloy having maximum initial discharge capacity was heat-treated at various temperatures in the range of $700{\sim}900^{\circ}C$ and tested. The loss of initial discharge capacity was appeared at all temperatures. but cycle characteristics of the alloy was improved. The electrodes heat-treated for 1 hour in the range of $700{\sim}850^{\circ}C$ showed good recovery of discharge capacities through repeated cycles, and from SEM observation results these were considered as 1 hour in the range of $700{\sim}850^{\circ}C$ showed good recovery of discharge capacities through repeated cycles, and from SEM observation results these were considered asbeing due to increased electrode strength and small loss of porosity during heat-treatment. The electrode heat-treated for 1 hour at $900^{\circ}C$ showed poor discharge characteristics because of low porosity.

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Effect of Saccharides and Incubation Temperature on pH and Total Acidity of Fermented Black Tea with Tea Fungus (배양액 제조에 사용된 당의 종류와 농도 및 배양 온도가 Tea Fungus발효 홍차의 pH 변화와 Total Acids생성에 미치는 영향)

  • Choi, Mi-Ae;Kim, Jeong-Ok;Choi, Kyung-Ho
    • Korean Journal of Food Science and Technology
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    • v.28 no.3
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    • pp.405-410
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    • 1996
  • The fermented black tea with tea fungus (FBTF) known to cure various diseases was prepared by culturing tea fungus biomass in black tae with different kinds (sucrose, glucose, fructose and corn syrup) and concentrations (10-60% m/v) of saccharides. pH changes and total acid production of FBTF were investigated during 14 dats incubation at $5-45^{\circ}C$ The patterns of acid production in sucrose and fructose black tea solution were similar each other, and those in glucose and corn syrup black tea solution were similar each other showing that tea fungus biomass utilizes fructose than glucose more efficiently. The optimum incubation temperature for the formation and growth of tea fungus Biomass, and the acid production was $30^{\circ}C$ Low contents of total aids (0.1%-0.2%) were produced in 20% of higher concentrations of sucrose and fructose black tea solution, while 1.8% and 0.68% were produced in the 10% of sucrose and fructose black tea solutions, respectively, pH of FBTF dropped to 2.74-3.56 after 2 days of incubation of all the culture solution and Kept this level to 14 days incubation.

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Fe-doped beta-tricalcium phosphate; crystal structure and biodegradable behavior with various heating temperature (Fe 이온 치환 beta-tricalcium phosphate의 하소 온도에 따른 미세구조 및 분해 특성)

  • Yoo, Kyung-Hyeon;Kim, Hyeonjin;Sun, Woo Gyeong;Yoon, Seog-Young
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.30 no.6
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    • pp.244-250
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    • 2020
  • β-Tricalcium phosphate (β-TCP, Ca3(PO4)2) is a kind of biodegradable calcium phosphate ceramics with chemical and mineral compositions similar to those of bone. It is a potential candidate for bone repair surgery. To improve the bioactivity and osteoinductivity of β-TCP, various ions doped calcium phosphate have been studied. Among them, Iron is a trace element and its deficiency in the human body causes various problems. In this study, we investigated the effect of Fe ions on the structural variation, degradation behavior of β-TCP. Fe-doped β-TCP powders were synthesized by the coprecipitation method, and the heat treatment temperature was set at 925 and 1100℃. The structural analysis was carried out by Rietveld refinement using the X-ray diffraction results. Fe ions existed in a different state (Fe2+ or Fe3+) with different heat treatment temperatures, and the substitution sites (Ca-(4) and Ca-(5)) also changed with temperature. The degradation rate was fastest at Fe-doped β-TCP with heated at 1100℃. The cell viability behavior was also enhanced with the substitution of Fe ions. Therefore, the substitution of Fe ion has accelerated the degradation of β-TCP and improved the biocompatibility. It could be more utilized in biomedical devices.

An Evaluation of Epoxy Asphalt Mixtures for Long-Span Steel Bridge Deck (장경간 강바닥판 교량용 에폭시 아스팔트 혼합물의 적용성 평가)

  • Baek, Yu Jin;Park, Chang Woo;Kim, Nakseok
    • KSCE Journal of Civil and Environmental Engineering Research
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    • v.32 no.6D
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    • pp.579-586
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    • 2012
  • The main objective of the research is to evaluate the laboratory performances of epoxy asphalt mixtures for long-span steel bridge decks. The aggregate gradations were recommended for field applications. The laboratory performance test results showed that the durability of epoxy asphalt mixtures was more noticeable than that of conventional ones. The structural analysis was conducted using resilient modulus and bond-shear test results. The analysis results revealed that just 9% out of total bond-shear stress was enough for the entire required bond-shear stress in the pavement system. The tensile stresses in the bridge decks were within limits compared to the laboratory test results from the Nanjing Grand Bridge in China. As a result, the laboratory performances of the epoxy asphalt mixtures for long-span steel bridge decks were better than those of conventional asphalt mixtures. However, the laboratory performance tests of epoxy asphalt mixtures for long-span steel bridge decks should be conducted precisely since the strengths of the mixtures are sensitive to the temperatures and curing times.

Thermal Annealing and Fading Characteristics of LiF:Mg,Cu,P TLD (LiF:Mg,Cu,P TLD의 잠상퇴행과 열처리 특성)

  • Doh, Sih-Hong;Lee, Woo-Gyo;Yoo, Myung-Jin;Kang, Hee-Dong;Kim, Do-Sung
    • Journal of Sensor Science and Technology
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    • v.7 no.5
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    • pp.313-318
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    • 1998
  • The thermal annealing, reusability and fading characteristics of the highly sensitive LiF:Mg,Cu,P TLDs are investigated. Thermoluminescent sensitivity of the fabricated LiF:Mg,Cu,P TLD is 25.3 times higher than the commercial dosimeter TLD-700(Harshaw Chemical Co.). The main dosimetric peak shows no fading for 1 month at room temperature and 50% for 7 days at $100^{\circ}C$. The thermal annealing characteristics is examined in the temperature range from $260^{\circ}C$ to $320^{\circ}C$. For annealing the TLD at $280^{\circ}C$ for 10 minutes, TLDs can be reusable by recovering the initial sensitivity.

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[ $NO_2$ ] Gas Sensing Characteristics of Carbon Nanotubes (탄소 나노튜브를 이용한 이산화질소 감지 센서의 특성)

  • Lee R. Y.
    • Journal of the Microelectronics and Packaging Society
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    • v.12 no.3 s.36
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    • pp.227-233
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    • 2005
  • Carbon nanotubes (CNT) which were grown, on the alumina substrate with a pair of comb-type Au electrodes, by plasma enhanced chemical vapor deposition have been investigated for $NO_2$ gas sensor. The electrical resistance of CNT film decreased with temperature, indicating a semiconductor type of CNT, and also the resistance of CNT sensor decreased with increasing $NO_2$ concentration. Upon exposure to $NO_2$ gas, the electrical resistance of CNT film sensor rapidly decreased within 3 minutes, and then showed a constant value after $20\~30$ minutes. It is found that the sensitivity of CNT sensor has been improved by air oxidation. The CNT sensor oxidized at $450^{\circ}C$ for 30 minutes showed higher sensitivity value than that without oxidation by $27\%$, even for a low 250 ppb $NO_2$ concentration at operating temperature of $200^{\circ}C$. But it needs a recovery time more than 20 minutes for reuse after detection of $NO_2$ gas.

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The Experimental Study on the Quinaldine(2-Methylquinoline) Toxicity for a Long Anaeathetization Period (장기 마취시 어류에 미치는 quinaldine 독성에 대한 기초 연구)

  • Yoon, Jong-Man;Lee, Jae-Hyun;Park, Hong-Yang
    • Journal of fish pathology
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    • v.2 no.1
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    • pp.37-44
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    • 1989
  • This study was taken to induce either anaesthesia or sedation for the purpose of applying to transport of live fish safely. 7 species of fish in addition to Tilapia mossambica were exposed to 250 ppm concentration of the anaesthetic quinaldine to determine the safe level for handling and transportation of these species. The results obtained are as follows ; 1. The time taken to lose balance increased with a decrease on the concentration of the anaesthetic. 2. Anaesthetization must be carried out under temperature lower or higher rather than optimum temperature. 3. The longer the length of the fish, the longer the anaesthetization time and recovery time of fish. 4. Coefficient of recovery period and body length is 0.78. 5. At 10-15 min. after anaesthetization, the serum levels of glucose, ALP and SGOT were at peat. 6. LDH of the anaesthetized fish is much more increased than that of the unanaesthetized. 7. In the more 250 ppm treatment, the pyknosis of the brain and spleen tissue appeared.

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Change of Dimensional Stability of Thermally Compressed Korean Pine (Pinus koraiensis Sieb. et Zucc.) Wood by Heat Treatment (잣나무 열압밀화재의 열처리에 의한 치수안정성 변화)

  • Cho, Beom-Geun;Hwang, Sung-Wook;Kang, Ho-Yang;Lee, Won-Hee
    • Journal of the Korean Wood Science and Technology
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    • v.43 no.4
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    • pp.470-477
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    • 2015
  • This study was carried out to investigate the change of dimensional stability of thermally compressed Korean pine (Pinus koraiensis Sieb. et Zucc.) wood by post heat treatment. Specific gravity of compressed wood was notably increased with thermal compression. In the compression set 50%, compressed Korean pine showed a specific gravity of 0.84. The amount of water absorption and swelling of thermally compressed Korean pine decreased with increasing temperature and time of the heat treatment. Set recovery also decreased with increasing temperature and time of heat treatment. Thermally compressed Korean pine that heat-treated in $120^{\circ}C$ for 24 hours showed a set recovery of 3.8%, whereas non-treated group showed 11.5%. Therefore, it was confirmed that the thermal treatment was a very effective method for the dimensional stability of the heat compressed wood.

A Study on the Recrystallization Behavior of Zr-xSn Binary Alloys (Zr-xSn 이원계 합금의 재결정에 관한 연구)

  • Lee, Myeong-Ho;Gu, Jae-Song;Jeong, Yong-Hwan;Jeong, Yeon-Ho
    • Korean Journal of Materials Research
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    • v.9 no.11
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    • pp.1123-1128
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    • 1999
  • To investigate the effect of Sn on the recrystallization of Zr-based alloys. Zr-xSn (x=0.5, 0.8, 1.5, 2.0wt.%) alloys were manufactured to be the sheets through the defined manufacturing procedure. The specimens were annealed at $300^{\circ}C$ to $800^{\circ}C$ for 1 hour. The hardness, microstructure and precipitate of the alloys with the annealing temperature were investigated by using micro- knoop hardness tester, optical microscope(O/M) and transmission electron microscope(TEM), respectively. The cold-worked Zr-xSn alloys showed the typical behavior of the recovery. recrystallization, and grain growth. The recrystallization of Zr-xSn alloys occurred between $500^{\circ}C$ and $700^{\circ}C$. As the Sn content increased. the recrystallization temperature of the cold-worked alloys increased but their grain sizes after recrystallization decreased. It is suggested that the recrystallization of the cold- worked Zr alloys be occurred by the subgrain coalescence and growth mechanism.

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Photosynthetic Capacity and Water Use Efficiency under Different Temperature Regimes on Healthy and Declining Korean Fir in Mt. Halla (한라산 구상나무 건전개체와 쇠약개체의 온도변화에 따른 광합성능력과 수분이용효율)

  • Lim, Jong-Hwan;Woo, Su-Young;Kwon, Mi Jeong;Chun, Jung Hwa;Shin, Joon Hwan
    • Journal of Korean Society of Forest Science
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    • v.95 no.6
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    • pp.705-710
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    • 2006
  • We investigated seasonal photosynthetic capacity and water use efficiency changes of Korean fir (Abies koreana Wils.) trees located at three sites around the peak of Mt. Halla, Witseorum, Youngsil and Jindallebat. At each sites, we chose healthy and declining individuals to examine the differences of physiological characteristics between them. Net photosynthetic capacity in $15^{\circ}C$ were lower than those of $20^{\circ}C$ and $25^{\circ}C$. The difference of net photosynthetic capacity between healthy and damaged trees was clear in June and August but damaged trees recovered with passing of the time. There was no difference between healthy and damaged trees in September on photosynthetic rate. Generally, water use efficiency (WUE) of damaged trees was higher than healthy trees.