• 전기의세계
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• v.37 no.10
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• pp.18-24
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• 1988

이 글에서는 토양 열특성의 종류와 각각의 특성이 내포하고 있는 의미와 전력 케이블의 설계 및 운용에 수반되어야 할 열저항율, 열확산율 및 열안정도의 측정필요성을 기술하고자 한다.

• Proceedings of the Korean Society of Propulsion Engineers Conference
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• 2009.05a
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• pp.159-162
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• 2009

In temperature controlled batch reactor, the effect of temperature and contact metals on the thermal stability of Exo-tricyclo[$5.2.1.0^{2,6}$]decane (tricyclodecane, exo-THDCP) were investigated by use of GC/MS. And the characteristic of metal in contact with tricyclodecane were analyzed by SEM-EDX. In fuel temperature variation test, thermal decomposition of exo-THDCP was occurred at $350^{\circ}C$. In case of fuel contact metals, Titanium was less effective to decomposition of exo-THDCP than stainless steel 304, 316.

• Journal of the Korean Society of Propulsion Engineers
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• v.15 no.5
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• pp.48-53
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• 2011

We investigated thermal stability improvement of exo-tetrahydrodicyclopentadiene (exo-THDCP) with thermal stabilizers (additives). The reaction products were sample during the reactions. The compositions of products were determined by gas chromatography-mass spectrometry (GC-MS) to measure thermal decomposition products of exo-THDCP and to specify mechanism for thermal stabilizers. Hydrogen donors (thermal stabilizers) such as 1,2,3,4-tetrahydroquinoline (THQ), benzyl alcohol (BnOH) increased thermal stability of exo-THDCP. These materials donated hydrogen to radical of exo-THDCP produced after initiation of exo-THDCP. We found that stabilization of exo-THDCP radicals decreased activity of primary products of exo-THDCP and lowered formation of secondary products (above-$C_{11}$ products).

• Proceedings of the Korean Society of Propulsion Engineers Conference
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• 2010.11a
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• pp.294-299
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• 2010

Thermal stability of exo-tetrahydrodicyclopentadiene (exo-THDCP) were investigated in a batch-type reactor perfectly coated with quartz. The 1 ml liquid product, which was a sufficiently small amount so as not to affect the reaction pressure, was sampled at 90 min intervals during the reaction and determined by gas chromatography-mass spectrometry (GC-MS) to measure thermal decomposition products of exo-THDCP and specify mechanism for additives (thermal stabilizer). Hydrogen donors (thermal stabilizer) such as 1,2,3,4-tetrahydroquinoline (THQ), benzyl alcohol (BnOH) increased thermal stability of exo-THDCP. These materials donated hydrogen to radical of exo-THDCP produced after initiation of exo-THDCP to decrease activity of primary products of exo-THDCP.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 2004.11a
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• pp.45-48
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• 2004

본 논문은 니켈실리사이드 (Ni-Silicide)의 열안정성을 개선하기 위해서 Ti와 TiN capping 층을 이용한 새로운 구조 Ni/Ti/Ni/Tin 구조를 제안하였다. 계면특성과 열안정성을 향상시키기 위해 타이타늄(Ti)을 니켈(Nickel) 사이에 적용하고, 니켈 실리사이드 형성 시 산소와의 반응을 억제하여 실리사이드의 응집현상을 개선시키고자 TiN capping을 적용 하였다. 니켈 실리사이드의 형성온도에 따른 $NiSi_2$로의 상변이를 억제할 수 있었고, 열안정성 평가를 위한 $700^{\circ}C$, 30분간 고온 열처리에서도 제안한 구조로 니켈실리사이드의 단면특성과 19 % 정도 면저항 특성을 개선하였다.

• Proceedings of the Korean Fiber Society Conference
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• 2001.10a
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• pp.279-282
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• 2001

Oxi-PAN(Oxidized PAN, Oxi-PAN)섬유는 PAN 섬유를 1-2$^{\circ}C$/min정도의 승온 속도로 180-30$0^{\circ}C$ 정도의 저온, 산화 분위기에서 인장력을 가한 상태로 열처리하여 얻는 섬유이며, 이 열처리 과정 중에 PAN 섬유의 분자쇄에서는 Cyclization, Dehydrogenation 및 산화 반응이 일어나게 된다. 이렇게 제조된 Oxi-PAN 섬유는 탄소섬유의 프리컷(Precursor)로 사용되기도 하고 또한 열안정성이 뛰어나 내염화섬유용으로 사용되기도 한다. (중략)

• Electrical & Electronic Materials
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• v.3 no.4
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• pp.287-294
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• 1990

이 논문은 메모리 재료의 기록, 소거의 반복시험에 의한 재료의 열화정도, 기록시의 열안정성, 신뢰성 등을 조사한 결과 다음과 같은 것을 알았다. 1)Ex/Ec가 0.69의 경우 $10^{7}$ 회 이상의 기록, 소거의 반복시험에도 분극의 변화는 없었으며 또한 1.78배에 있어서도 $10^{3}$회 까지는 문제가 없음을 알았다. 2)항전계의 1/2을 초과하는 역펄스 전게에서도 분극에는 전혀 변화가 없었다. 3)열처리 시험에 있어서 열에 의한 분극의 감쇠는 15분 이내에 일정치에 달했으며 또한 불화 비닐덴의 조성비가 클수록 열안정성이 증가했다.

• Microbiology and Biotechnology Letters
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• v.18 no.1
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• pp.44-48
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• 1990

Alkalophilic sp. YC-335 isolated from soil was capable of producing large amount of cyclodextrin glycosyltransferase (CGTase) in culture broth. This enzyme was successively purified 52.9 folds with 17.8 yield by ethanol precipitation, DEAE-Toyopearl column chromatography and Sephadex G-100 column chromatography. The purified enzyme have a molecular weight of approximately 75,000 estimated by SDS polyaerylamide gel electrophoresis. The optimum pH and temperature for the enzyme activity were 6.0 and 5$0^{\circ}C$, respectively. The enzyme stable between pH 6 and 10, and up to 5$0^{\circ}C$. The thermostability of the enzyme was increased up to 6$0^{\circ}C$ by the addition of 15mM CaCl$_2$.

• Applied Chemistry for Engineering
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• v.3 no.2
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• pp.280-287
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• 1992

Aromatic liquid crystalline polyesters were synthesized from terephthalic acid(TPA), biphenyl dicarboxylic acid(BPA) and hydroquinone(HQ) by solution polymerization. Effects of TPA/BPA ratio(by mole %) on the thermal properties, thermal stability and textures of mesophases were investigated with DSC, TGA, cross-polarized microscopy and X-ray diffractometer. The synthesized polymers in this study were thermotropic and showed nematic textures. Melting temperature($T_m$) and isotropization temperature($T_i$) of polymer increased and thermal stabilities of polymer were improved with the content of BPA. Most of the polymers in this study had crystallinity more than 30%.

• Journal of Life Science
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• v.8 no.6
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• pp.627-637
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• 1998

In order to utilize tuna pyloric caeca among fish intestines wasted when treated raw fish in fish processing manufactory, a crude enzyme with high proteolytic activity was extracted and its optimum condition were investigated. An immobilized enzymes also were prepared by adsorption method to enhance thermostability of the crude proteinase. The yield of the crude proteinase was approximately 2.7% on dry basis. The proteolytic activity for casein was 0.54 U/mg protein, for BTEE 1.10 U/mg protein, and for BAEE 2.69 U/mg protein. It was almost similar to that of the commercial trypsin purified. Optimum hydrolysis activity of the crude proteinase was about 80%, as the degree of hydrolysis for casein, at pH 10.0 and 45$^{\circ}C$ for 12 hrs. Also, when the crude proteinase was immobilized on DEAE-Cellulose and chitin, the residual activities remained after 7 days of pre-incubation time were maintained about 90% or more and their thermostabilities were enhanced by about 50%, compared with the native enzyme.