• Title/Summary/Keyword: 열분석적 특성

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Synthesis of CO2 Adsorbent with Various Aminosilanes and its CO2 Adsorption Behavior (다양한 아미노실란을 이용한 이산화탄소 흡착제 합성 및 흡착 특성)

  • Jeon, Jae Wan;Ko, Young Soo
    • Applied Chemistry for Engineering
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    • v.27 no.1
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    • pp.80-85
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    • 2016
  • The carbon dioxide adsorption behavior of silica with a large specific surface area and pore volume functionalized with aminosilane compounds via in-situ polymerization and functionalization method were investigated. The organosilanes include amino functional group capable of adsorbing carbon dioxide. Elemental analyzer, in situ FT-IR and thermogravimetric analyzer were used to characterize the sorbents and to determine their $CO_2$ adsorption behavior. Comparison of different aminosilane loading in the support revealed that polyaminosilane functionalization of 70% of the pore volume in the support was better in terms of the adsorption capacity and amine efficiency than that of 100% of the pore volume of the support. Furthermore, the sorbents showed a higher adsorption capacity at an adsorption temperature of $75^{\circ}C$ than at $30^{\circ}C$ due to the thermal expansion of synthesized polyaminosilanes inside the pore of silica. The N-[3-(trimethoxysilyl)propyl]ethylenediamine (2NS) sorbent with 70% of the pore volume functionalized showed the highest adsorption capacity of 9.2 wt% at $75^{\circ}C$.

Quality Characteristics of Cirsium setidens Nakai by Different Drying Method (건조 방법에 따른 곤드레 나물의 품질 특성)

  • Park, Sung Jin;Lee, Dae Won;Park, Sung Hye;Rha, Young-Ah
    • Culinary science and hospitality research
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    • v.22 no.2
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    • pp.104-114
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    • 2016
  • In this study, the quality characteristics of different drying methods of Cirsium setidens Nakai, which contains large amounts of biological substances, were investigated for the improvement of their practical use. During the drying period, the weight reduction was the highest with hot-air drying(82.7%). As for the general component and mineral contents analysis results of Cirsium setidens Nakai, there were no significant difference. Cyclic low pressure drying resulted highest amount of total phenolic components and 1,1-diphenyl-2-picrylhydrazyl (DPPH). Hence, cyclic low pressure drying method is the best method for enhancing antioxidant activity of Cirsium setidens Nakai.

Flexural Behavior Characteristics of Steel I-Beam Strengthened by the Post-tensioning Method on the Field Experiment (현장실험을 통한 외부 후긴장 Steel I-Beam의 휨 거동 특성)

  • Cho, Doo-Yong;Park, Dae-Yul;Park, Sun-Kyu
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.6 no.3
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    • pp.151-158
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    • 2002
  • Recently, the externally prestressed unbonded steel I-beam bridges have been increasingly built. The mechanical behavior of prestressed steel I-beams which are with external unbonded tendon is different from that of normal bonded PSC beams in a point of that the slip of tendons at deviators and the change of tendon eccentricity occurs, when external loads are applied in external unbonded steel I-beams. The concept of prestressing steel structures has not been widely considered, in spite of long and successful history of prestressing concrete members. In this study, The field experiment on prestressed steel I-beams has been performed in the various aspects of prestressed I-beam including the tend on type and profile.

Evaluation of Carbonation and Strength of High Strength Binary Concrete Used Ground Granulated Blast Furnace Slag (고로슬래그 미분말을 사용한 2성분계 고강도 콘크리트의 강도 및 중성화 특성)

  • Kim, Hyun-Joong;Kim, Hong-Sam;Lee, Chan-Young;Cheng, Hai-Moon;Ahn, Tae-Song
    • Proceedings of the Korea Concrete Institute Conference
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    • 2008.04a
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    • pp.409-412
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    • 2008
  • There are many methods to improve the performance of concrete. Especially, admixture materials used in concrete as the replacement materials of cement, could fluidity, strength and durability of concrete. So recently, the terminology "High-Performance Concrete(HPC)" has been introduced into the construction industry. Most hige-performance concrete have a high cementitious content and a low water-cementitious material ratio. The proportions of the individual constituent vary depending on lacal preferences and local materials. Therefore, many trial batches are usually necessary before a successful mix is developed. The objective of this experiments is to investigate the fundamental properties of high performance concrete based binary cimentitious materials such as ordinary portland cement and ground granulated blast furnace slag. In this study, Use granulated blast furnace slag (30%, 45%, 60%) and water cementitious content (26%, 30%, 34%) take the gauge of capacity that strength, carbonation and XRD, X-Ray Diffraction test

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Analysis of Cutting Characteristic of the Sapphire Wafer Using a Internal Laser Scribing Process for LED Chip (LED 칩 제조용 사파이어 웨이퍼 절단을 위한 내부 레이저 스크라이빙 가공 특성 분석)

  • Song, Ki-Hyeok;Cho, Yong-Kyu;Kim, Byung-Chan;Kang, Dong-Seong;Cho, Myeong-Woo;Kim, Jong-Su;Ryu, Byung-So
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.16 no.9
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    • pp.5748-5755
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    • 2015
  • Scribing is cutting process to determine production amount and characteristic of LED chip. So it is an important process for fabrication of LED chip. Mechanical process and conventional scribing process with laser source has several problems such as thermal deformation, decreasing of material strength and limitation of cutting region. To solve these problems, internal laser scribing process that generates void in wafer and derives self-crack has been researched. However, studies of sapphire wafer cutting by internal laser scribing process for fabrication of LED chip are still insufficient. In this paper, cutting parameters were determined to apply internal laser scribing process for sapphire wafer for fabrication of LED chip. Then, foundation of cutting condition was established to set up internal laser scribing system through investigation of cutting characteristics by several experiments.

Pyrolysis Characteristics of Hemp By-products (Stem, Root and Bast) (헴프 부산물의 열분해 특성 연구)

  • Choi, Gyeong-Ho;Kim, Seung-Soo;Kim, Jinsoo;Joo, Dong-Sik;Lee, Janggook
    • Applied Chemistry for Engineering
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    • v.22 no.5
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    • pp.508-513
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    • 2011
  • Hemp is known as one of the most productive and useful plants, which grows quickly in a moderate climate with only moderate water and fertilizer. Traditionally in Korea, hemp bast is used to natural fibres, and remaining such as stem and root is treated as waste. Those of hemp by-products can be transformed to bio fuel such as bio-oil and activated carbon. To understand pyrolysis characteristics, thermogravimetric analysis were carried out in TGA, in which hemp by-products were mostly decomposed at the temperature range of $270{\sim}370^{\circ}C$. The corresponding kinetic parameters including activation energy and pre-exponential factor were determined by differential method over the degree of conversions. The values of activation energies for pyrolysis were increased as the conversion increased from 10 to 90%.

GIS spatial D/B formation of geothermal data and Distribution of Heat Flow of Korea (한국의 지열자료 GIS 공간 D/B 구축과 지열류량 분포)

  • Kim, Hyoung-Chan;Lee, Young-Min;Park, Jeong-Min
    • 한국신재생에너지학회:학술대회논문집
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    • 2006.06a
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    • pp.459-460
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    • 2006
  • 현재 남한의 지열류량 측정값으로는 총 363개 지점의 자료가 측정 및 수집되어 있다. 이것은 Mizutani et at. (1970), 장정진 외(1970), 그리고 서정희(1976) 등의 자료, 총 35개의 자료도 추가된 것이다. 1989년 이후부터 측정된 지열류량 자료는 217개 자료이며(임정웅 외, 1989; 임정웅 외, 1996; Lim and Kim, 1997; 염병우 외, 1997), 모두 직접 측정한 것이나, 1989년 이후 보고된 지열류량 자료에 약간의 오류가 있어 이번 연구에서 수정 보완하였다. 또한 과거의 자료 35개 자료는 이미 지열류량 측정치가 논문화 되어 있는 것으로 암석시료는 없다 1989년 이후 2004년까지 자료 217개 2005년도 추가 자료 111개의 지열류량 자료는 암석시료도 있으며, 측정기기가 서로 달라 오차가 있을 수 있어 서로 보정을 해야 할 필요가 있어 시추공 주변 암석을 새로 수집해서 신장비로 다시 측정 보정하였다. 지열류량 D/B 구축은 각 자료의 일련번호, 고유번호 (Sn.), 위경도 좌표 (longitude, lattitude), 암석의 열전도도(thermal conductivity), 지온경사 (thermal gradient), 지열류량 (heat flow)등으로 구성되어 있다. 지열류량 자료 공간 데이터베이스는 점 속성을 가지며 자료형태는 각종 소프트웨어와 호환성이 좋은 shape 파일 형태로 작성하였다. 또만 최근 천부 토양 및 암석 열물성을 이용한 냉난방시스템 즉, Heat Pump System 설계를 위하여 반드시 들어가야 하는 요소인 열확산율, 공극율, 밀도, 비열 등 열물성 특성을 추가하여 GIS 공간 D/B구축하였다. 대륙붕 자료 4개 자료를 제외하고 359개의 지열류량 자료를 이용하여 한반도 남부, 즉 남한의 지열류량 분포도를 작성 분석해 본 결과(그림 1), 우리나라의 지열류량 이상대는 아산만 주변, 보령, 유성, 진안, 울진, 포항, 부산 지역과 포천, 속초, 충주, 수안보 등 지역에서 나타난다 이러한 이상대 주변에는 대개 온천이 발달되어 있었거나 새로 개발되어 있는 곳이다. 온천에 이용하고 있는 시추공의 자료는 배제하였으나 온천이응으로 직접적으로 영향을 받지 않은 시추공의 자료는 사용하였다 이러한 온천 주변 지역이라 하더라도 실제는 온천의 pumping 으로 인한 대류현상으로 주변 일대의 온도를 올려놓았기 때문에 비교적 높은 지열류량 값을 보인다. 한편 한반도 남동부 일대는 이번 추가된 자료에 의해 새로운 지열류량 분포 변화가 나타났다 강원 북부 오색온천지역 부근에서 높은 지열류량 분포를 보이며 또한 우리나라 대단층 중의 하나인 양산단층과 같은 방향으로 발달한 밀양단층, 모량단층, 동래단층 등 주변부로 NNE-SSW 방향의 지열류량 이상대가 발달한다. 이것으로 볼 때 지열류량은 지질구조와 무관하지 않음을 파악할 수 있다. 특히 이러한 단층대 주변은 지열수의 순환이 깊은 심도까지 가능하므로 이러한 대류현상으로 지표부근까지 높은 지온 전달이 되어 나타나는 것으로 판단된다.

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Implementation of Electrical and Optical characteristics based on new packaging in UV LED (UV LED의 광효율 및 방열성능 향상을 위한 new packaging 특성 연구)

  • Kim, Byoung Chol;Park, Byeong Seon;Kim, Hyeong-Jin;Kim, Yong-Kab
    • Smart Media Journal
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    • v.11 no.9
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    • pp.21-29
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    • 2022
  • Ultra Violet(UV) is gradually being replaced with LED instead of general UV lamps. However, the light efficiency of UV LED is still lower than that of the general lamp, and the light efficiency is also low. Due to the current environment and technical problems of UV lamps, the LED replacements are gradually being made. In this study, a new package design and analysis were performed to increase the lifetime and performance of UV LEDs. A new packaging for UV LED were designed and implemented. The new packaging for UV LED was constructed to improve light efficiency. And the electrical and optical characteristics were analyzed respectively. To improve the optical efficiency in UV LED package, the Al has been used based on high reflectivity and applying the optimal lens focusing. Compared to the existing silver Ag, the light efficiency was improved by about 30% or more, and it was confirmed that the light output degradation characteristic was improved by about 10% in the newly applied optical device chip.

Convergence Study of Cell Viability and Vascular Relaxtion of Hanbang-tea Prescrpition (한방차 조성물의 세포활성과 혈관이완 효과에 대한 융합적 연구)

  • Park, Sung-Hye;Min, Je-Ho
    • Journal of the Korea Convergence Society
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    • v.8 no.2
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    • pp.291-297
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    • 2017
  • This study was aimed to secure the basis for developing the hangbang-tea may help promote healthy blood vessels by natural herbal ingredients formulated in accordance with the basic principles of oriental medicinal theory. We investigated the vessels contracted by concentrations and safety assessment carried out by the cell viability of Taraxaci Herba, Gardeniae Fructus, Chrysanthemum indicum and Lonicerae Flos composition and concentration. We found cell survival were higher than the control group show a beneficial trend in the growth of normal liver and kidney cells. As a results of this study will be the basis to develop the hangbang-tea differentiated in the future oriental medicine resources. Medicinal resources will be hangbang-tea based on clinical trials utilizing herbal western and oriental medicine convergence principle and vascular relaxation mechanism.

Effect of Hollow Composite Yarn Characteristics to the Comfort Property of Fabrics for High Emotional Garment (중공 복합사 특성이 고감성 의류용 직물의 쾌적성에 미치는 영향)

  • Kim, Hyun-Ah
    • Science of Emotion and Sensibility
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    • v.17 no.4
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    • pp.71-78
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    • 2014
  • Composite draw textured yarns(DTY) and air jet textured yarns(ATY) with hollow PET filament have been used for making high emotional fabrics including light weight sports wear garments. This study investigated effect of hollow composite yarns and fabric structural parameters to the comfort properties related to the moisture and thermal transport phenomena for the composite fabrics made of DTY and ATY with hollow PET filament. Wicking property of hollow composite fabric was superior at the high pore size fabric and was not influenced by fabric cover factor. Wicking property of the fabric with ATY was better than that of the fabric with DTY. On the other hand, drying rate of fine pore sized fabric was shorter than that of large pore sized fabric and drying rate of high multi yarn fabric with low cover factor and small pore size was superior than that of hollow composite fabric. The pore size of the fabric was dominant factor in the air permeability and thermal conductivity of hollow composite fabric. High pore sized fabric showed high air permeability and thermal conductivity of hollow composite fabric was nonlinearly inversely proportional to pore size of the fabric.