• Electrical & Electronic Materials
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• v.8 no.4
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• pp.464-471
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• 1995

메그네트론 스퍼터링으로 제작한 고밀도 다층박막($Co_75{{Pt_12}{Cr_13}}$합금) 디스크를 투과전자현미경을 이용해 단면 및 평면의 미세조직의 조사 혹은 미소부위 성분분석을 할 경우, 선행되어야하는 시편준비 경로와 각 단계별 구체적방법 및 그 효과를 연구하였다. Ion밀링시간이 증가함에 따라 시료가 얇게 되는과정에서 스퍼터링된 물질이 관찰될 시편부위의 다른 표면에 증착되므로써 미세조직의 선명도를 해칠 수 있고, 이로인한 해석상의 오류가능성이 시사되었다. 또한, 자기박막 디스크와 같이 다층으로 구성된 단면분석용 시료에서는 서로 맞붙인 실리콘 단결정 접착면을 따라 밀링속도가 선택적으로 커서 우선축이 생김으로써 양질의 시편을 얻기 어려운 문제점이 제기되었다. 이같은 문제를 포함한 전자현미경 시료준비과정에서 생길 수 있는 문제를 해결할 수 있는 실마리와 이를 이용해 수행한 전자현미경 분석결과 및 효과적인 시편준비방법이 본 논문에서 언급되었다.

• KOREAN JOURNAL OF CROP SCIENCE
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• v.64 no.2
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• pp.102-108
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• 2019

Pericarp thickness of vegetable corns such as sweet and waxy corn is one of the crucial traits, contributing to their edible quality. This study was carried out to compare the pericarp thickness of super sweet and waxy corn hybrids measured with kernel samples prepared using different methods at different grain filling periods. The samples comprised excised pericarp from dried, frozen (at $-4^{\circ}C$), and fresh kernels. Analysis of variance performed separately on super sweet and waxy corn hybrids indicated a significant three-way interaction among cultivars, kernel sample preparation methods, and days after pollination (DAP). Dried samples of super sweet corn hybrids presented reasonably stable pericarp thickness measurements during grain filling, while all the sample preparation methods fluctuated less as grains of waxy corn hybrids matured. Waxy corn is best consumed at around 24 days after pollination. Pericarp thickness of waxy kernel samples regardless of preparation methods investigated was the same at 24 DAP with a few exceptions. Overall, the common method of drying kernel samples before pericarp excision can provide reliable data for estimating the tenderness of vegetable corn hybrids.

• Applied Microscopy
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• v.29 no.1
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• pp.67-73
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• 1999

It is practically hard to prepare good TEM specimens from powders which are embedded in epoxy materials for ion milling, because the milling rate difference between powders and epoxy is quite large. In order to overcome this problem, we tried to find methods to increase the density of powders in the embedding epoxy without loosing the adhesive strength between them. Powder density was considerably increased by employing a centrifuge for embedding, compared to the result by a conventional vacuum embedding. In addition, mixing powders of different sizes after sieving also enhanced the final density by allowing smaller particles filling in the gaps of larger particles. Ion milling of powders embedded by these methods resulted in thin specimens good enough for normal TEM works. TEM specimens from spherical, platy and fibrous powders of submicron size were successfully prepared by this centrifuging method.

• Proceedings of the Korean Vacuum Society Conference
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• 2013.02a
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• pp.528-528
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• 2013

대기압 플라즈마 처리에 의한 특성 파악은 플라즈마 처리한 표면의 친수성 또는 소수성의 물성변화를 결합각을 측정하거나 Atomic Force Microscopy (AFM)을 통한 표면 구조의 분석등 고체 표면을 평가하는 방법이 현재 주로 사용되고 있다. 그러나 결합각이나 AFM을 통한 평가법은 고체 표면만을 확인 할 수 있으며 액체 시료의 물성 상태 변화에 따라 정량적 분석을 확인할 수 없다. 이에 액체 시료에 대기압 플라즈마 처리로 미치는 영향을 전기적 특성 평가를 통해 정량적으로 분석하였다. 증류수, 알코올 등 액체 시료로 실험을 진행하였다. 준비된 기판위에 액체시료를 올려 플라즈마 처리를 하였으며, 기판에 양단에 준비된 전극을 통해 Resistance, Capacitance, Inductance 등의 임피던스를 측정하여 액체시료에 인가 된 플라즈마 처리 전과 후의 전기적 특성 변화를 확인하였다.

• Journal of the Korean Magnetics Society
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• v.18 no.1
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• pp.1-8
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• 2008

We have manufactured and evaluated reference samples for the use of low magnetic moment measurements. Before the measurements, SQUID magnetometers were magnetically shielded from external magnetic noise. We considered the purity including magnetic impurities, the optimum thickness, the modification method, and the shape in the preparation of the samples. Three paramagnetic polycrystaline metal plates of Ti, W, and Al with the area of $4mm{\times}6mm$ were prepared finally. The magnetic moments of these three samples are measured very linear up to the field of 5 T without magnetic hysteresis. The temperature deviated ratios of the magnetic moments for Ti, Al, and W from 290 K to 310 K are 0.7, 1.5, and 0.1 %, respectively. The measured magnetic moments for Ti and W samples by our research team are very well agreeable with those by two SQUID magnetometers and a VSM at Quantum Design via international round robin test. The results suggest that the prepared reference samples are well suited for the use in the low magnetic moment measurement with SQUID based magnetometers.

• Journal of the Korean Applied Science and Technology
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• v.35 no.2
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• pp.463-471
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• 2018

In this study, analyzed of changes resulting from the spread of carbon black in casein grafted water dispersed polyurethane using PPG. For this purpose, casein-grafted water-dispersed polyurethane and (PUD and CPUD's) samples were prepared and samples of CPCB's dispersed with carbon black were prepared. As a result of measuring the tensile strength using prepared samples, the tensile strength was increased to $3.01kgf/mm^2$ with CPUD3, which contains highly casein, in CPCB's tensile strength was measured as low as $2.54kgf/mm^2$ with increasing carbon black. Elongation was measured in 278% of PUD samples containing less casein, and CP3CB4 in CPCB's was measured as 157%. The abrasion resistance of the samples was 36.97 mg.loss for CPUD3 and 41.11 mg.loss for CP3CB4. The solvent resistance of the PUD 's sample and the CPCB' s sample were not changed.

• Proceedings of the Korean Society for Emotion and Sensibility Conference
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• 2001.11a
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• pp.19-24
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• 2001

본 연구에서는 국내 7개 기업에서 생산되고 있는 PET POY와 일본과 대만에서 생산되고 있는 PET POY 시료를 준비하여 이들 사의 열수축 특성을 hank 실험방법과 Toray FTA-500 계측기를 사용한 실험 data를 비교 분석하여 최근 도입되어 사용되고 있는 Toray FTA-500 열 수축률 측정계측기의 타당성을 조사하고자 한다. 본 연구를 위해 사용한 시료는 PET POY 85d/72f 그리고 120d/36f 그리고 120d/36f 2가지를 준비했으며 국내 합섬 maker 7개회사별로 각각 같은 굵기의 POY 사를 준비하였다. 그리고 국내 POY와 외국 소재로서 대만과 일본에서 생산되고 있는 소재의 열 수축률 특성치를 Toray FTA-500과 hank 방법을 비교 분석하므로서 감성의류 제조용 PET POY 사의 국내ㆍ외 소재의 차이점을 계측기계와 계측방법의 상이로 나누어 data화가 가능케 함으로서 감성의류소내 개발에 기초자료를 활용코자 한다.

• The Journal of the Petrological Society of Korea
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• v.13 no.3
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• pp.126-132
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• 2004

This study provides detailed sample preparation methods for subgrain zircon analyses, and a simple mineral separation technique which overflows light mineral grains out of beaker using the running water from faucet. Excluding separation steps using of the Wilfley table and heavy liquid, this technique is faster and more efficient than conventional one, and remarkably suitable for collecting small amount of zircon for subgrain analyses.

• 한국전자현미경학회:학술대회논문집
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• 1997.11a
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• pp.37-38
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• 1997

• 한국전자현미경학회:학술대회논문집
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• 1998.05a
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• pp.45-46
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• 1998