• Korean Journal of Food Science and Technology
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• v.19 no.2
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• pp.97-101
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• 1987

Physicochemical properties of heat-moisture (18, 21, 24 and 27%) treated naked barley (Youngsanbori) starch indicated that crystailinity of the starch was decreased upon treatment and water-binding capacity drastically increased as the moisture level increased. The swelling power was decreased, but the solubility increased by heat-moisture treatment. Apparent viscosity in aqueous sodium hydroxide solution was repressed as moisture-treatment level increased. Amylograph hot paste vicosities were decreased upon treatment except initial pasting temperature.

• Korean Journal of Food Science and Technology
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• v.19 no.5
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• pp.435-440
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• 1987

Gelatinization properties of heat-mositure treated potato and sweet potato starches were investigated. Water-binding capacity of starch was increased by heat-mositure treatment, which was more pronounced in sweet potato starch. Blue value was not affected by the treatment. Amylograph viscosities were decreased by heat-mositure treatment, which was more pronounced in potato starch. Critical concentration of NaOH for gelatinization of starch increased as moisture level increased. Gel volume of starch upon KSCN gelatinization was higher in potato starch. Gelatinized starches showed Binghamapseudoplastic behavior. Consistency index and yield stress were drastically decreased upon heat-moisture treatment.

• Korean journal of food and cookery science
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• v.22 no.2 s.92
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• pp.147-157
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• 2006

To improve the properties of non-waxy rice flours for baking, soaked-wet milled rice flour (SWRF) was adjusted moisture content (MC) to 30 and 50 % and heated at 50 and $70^{\circ}C$ in a shaking water bath for 6 and 18 hrs, respectively. Moisture-heat treated rice flours were investigated with regard to particle size distribution, and morphological, physicochemical and pasting properties for comparing dry and wet milled flours. The particle size of rice flour treated with 30% MC was distributed between $4-20{\mu}m\;and\;100-200{\mu}m$, like SWRF. The particles above $200{\mu}m$ in the flour were produced at higher heating temperature. By SEM, starch granules were found in the rice flours treated with 30% MC, who whereas aggregated starch granules were shown in the flours treated with 50% MC. Moisture-heat treatment using higher MC and heating temperature decreased the lightness and increased the yellowness of non-waxy rice flours. Water binding capacity of 30% moisture treated rice flour was similar to that of SWRF. In the same moisture treated rice flour, swelling power was higher, but solubility was lower at $50^{\circ}C$ than at $70^{\circ}C$. The initial pasting temperature by RVA increased after moisture-heat treatment. The peak viscosity of moisture-heat treated rice flour was higher for 30% moisture than that of the others. The rice flour treated with 30% MC and heated at $50^{\circ}C$ showed low setback and increased stability for retrogradation.

• Korean Journal of Food Science and Technology
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• v.52 no.1
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• pp.31-39
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• 2020

The effects of heat-moisture treatment (HMT) on the functional properties of high amylose rice starches (HARSes) purified from Korean rice varieties (A-type Goami and Singil and B-type Dodamssal and Goami2) were investigated. HMT was accomplished with moisture contents of 18 and 27% and heated at 100℃ for 16 h. While the amylose content, swelling power and solubility decreased after HMT, the water binding capacity and resistant starch (RS) content increased with increasing moisture content after HMT. The X-ray diffraction patterns of all HARSes did not change after HMT, but a decrease in the intensity of peak at 2θ=5° was observed in B-type HMT HARSes. While the starch granules aggregated after HMT, their shape and size remained unchanged. B-type HARSes exhibited higher gelatinization temperatures and lower pasting viscosities than A-type HARSes following HMT. The results, thus, suggest that while the crystalline intensity of B-type Dodamssal and Goami2 rice starches did not change after HMT, the RS content, water binding capacity, and pasting temperatures of all HARSes increased with increasing moisture content after HMT.

• Applied Biological Chemistry
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• v.40 no.6
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• pp.508-513
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• 1997

Thermal characteristics and granular morphology on enzyme-resistant starches (RS) formed during heat-moisture treatment (HMT) and retrogradation were investigated in high amylose corn starches, Hylon V and Hylon VII. With each treatment, both starches showed a similar trend in the increase of RS, but RS yield of Hylon VII is higher than that of Hylon V. Specially, RS was increased remarkably by HMT. It was more than doubled from 11.4% to 26.6% for Hylon V and from 15.9% to 32.8% for Hylon VII. A small increase of RS resulted from retrogradation. HMT on starch increased gelatinization temperature, decreased enthalpy. Retrograded starch exhibited small three endothermic transitions at $94^{\circ}C$, $110^{\circ}C$ and $140^{\circ}C$ in differential scanning calorimetry (DSC) thermogram due to the remained ungelatinized starch granules, dissociation of amylose-lipid complex and melting of recrystallized amylose, respectively. Enzyme-resistant starches isolated from native and heat-moisture treated starches showed a broad endothermic transition at higher temperature than native starch, while retrograded starch exhibited a very sharp peak at ${\sim}150^{\circ}C$ due to the melting of amylose crystallites. Under microscopy, starch granules with HMT was not changed, but retrograded starches showed the aggregates of starch granules because amylose leached out during gelatinization. Iodine stained RS clearly showed the differences in enzyme hydrolysis on the native, heat-moisture treated and retrograded starches.

• Applied Biological Chemistry
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• v.27 no.4
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• pp.252-258
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• 1984

Physicochemical properties of arrowroot starch, which was adjusted to 18, 21, and 24% moisture and heated at $100^{\circ}C$ for 16hr, were investigated. X-ray diffraction pattern was changed from C- to A-pattern upon treatment(24% moisture). The swelling powere and solubility decreased by heat-moisture treatment. The treated sample was gelatinized at higher temperature than untreated one. Water-binding capacity was drastically increased as the moisture level was decreased. Amylograph hot paste viscosities were decreased upon treatment.

• Applied Biological Chemistry
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• v.30 no.3
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• pp.242-249
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• 1987

Physicochemical properties on heat-moisture treatment of sweet potato starch were investigated. Starch granules of sweet potato observed by photomicroscope, polarized-light microscope and scanning electron microscope were round and polygonal. X-ray diffraction pattern was changed from Ca-pattern to A-pattern upon heat-moisture treatment. Water binding capacity was drastically increased as the moisture level was increased. The swelling power and solubility at the same temperature were decreased by heat-moisture treatment. Transmittance of 0.1% starch suspensions was increased rapidly from $65^{\circ}C$ in case of untreated starch and from $70^{\circ}C$ in case of treated starch. The starch on heat-moisture treatment was gelatinized over higher temperature range than the untreated starch.

• Polymer(Korea)
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• v.27 no.2
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• pp.113-119
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• 2003

The thermal properties and crystallization behaviors of poly(ethylene terephthalate) (PET) were investigated by controlling the annealing conditions of PET sample, such as relative humidity, temperature, and time. The variations of moisture content, glass transition temperature ($T_g$) and cold crystallization temperature ($T_{\propto}$) were examined after annealing the PET sample. Subsequently crystallization process was performed with the annealed PET specimen, and then the degree of crystallinity and heat distortion temperature (HDT) of variously crystallized PET specimen were examined. Residual stress relaxation in the injection molded PET sample after annealing was also observed through polarized films. Moisture content in the PET specimen increased up to 6000 ppm with increasing the relative humidity, temperature, and time of annealing. $T_g$ and $T_{\propto}$ of the annealed PET specimen decreased with increasing moisture content. The degree of crystallinity increased as increasing moisture content in the PET specimen. However for same moisture content, the degree of crystallinity varied with annealing conditions. The relaxations of residual stress in the PET sample differed from annealing conditions, and the maximum degree of crystallinity increased with decreasing residual stress in the PET sample.

• Korean Journal of Food Science and Technology
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• v.18 no.6
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• pp.437-442
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• 1986

Physicochemical properties of chestnut starch, which was adjusted at 14, 18, 21 and 24% moisture and heated for 16 hr at $100^{\circ}C$, were investigated. The cystallinity, swelling power and solubility of the starch were decreased upon heat-moisture treatments. The swelling power of the heat-moisture treated starch showed an inverse relation with moisture levels, while the solubility showed opposite trend. The swelling power and the solubility of both raw and heat-moisture treated starches held a liner relationship. The. water binding capacity of the starch was drastically increased upon heat-moisture treatments. Amylograms revealed that the heat-moisture treated starches had higher initial pasting temperature and lower viscosity than untreated starch. No peak viscosity was observed for the heat treated starches above 21% moisture. The minimum moisture contents for gelatinization of raw and heat-moisture (18%) treated starches were 45 and 40%, respectively. The gelatinization temperature of raw and heat-moisture (18%) treated starches was $65^{\circ}C$.

• Applied Biological Chemistry
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• v.33 no.1
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• pp.1-7
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• 1990

Starch samples of rice and glutinous rice starches were adjusted to 27 % of moisture and heated at $100^{\circ}C$ for 16 hours, respectively. After the treatment, their physicochemical properties were investigated. The granule shapes of all the starches were polygonal and they became slightly bigger in their sizes after the treatment. All their X-ray diffraction patterns were A types. The specific gravity of the starches decreased to 1.03-1.09 by the treatment. The water binding capacity of rice starches increased, while that of glutinous counterparts slightly decreased. Almost no change in the amount of amylose included was found. Swelling power and solubility were increased with the increase of temperature. At a certain temperature, however, the solubility of the treated starches increased when the swelling power decreased. The initial gelatinization temperatures of Akkibare, Yongmun, and Taebaek starches were $60{\sim}65^{\circ}C$ but those of glutinous rice starch and U.S.A. rice starch were $55{\sim}60^{\circ}C$ and $70{\sim}75^{\circ}C$, respectively, as measured by transmittance. The gelatinization temperature of the treated starches was higher than that of the untreated starches.