• Title/Summary/Keyword: 수분 안정성

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Reliability Evaluation of Semiconductor using Ultrasound (초음파를 이용한 반도체의 신뢰성 평가)

  • Jang, Hyo-Seong;Ha, Job;Jhang, Kyung-Young
    • Journal of the Korean Society for Nondestructive Testing
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    • v.21 no.6
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    • pp.598-606
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    • 2001
  • Recently, semiconductor packages trend to be thinner, which makes difficult to detect defects therein. A preconditioning test is generally performed to evaluate the reliability of semiconductor packages. The test procedure includes two scanning acoustic microscope (SAM) tests at the beginning and end of the entire test, in order to help detect physical defects such as delaminations and package cracks. In particular, of primary concern are package cracks and delaminations caused by moisture absorbed under ambient conditions. This paper discusses the failure mechanism associated with the moisture absorbed and encapsulated in semiconductors, and the use SAM to detect failures such as tracks and delaminations grown during the preconditioning test.

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Preparation of crosslinkable imide oligomers and Applications in Polyether Imides for Dual-ovenable Packaging (가교형 이미드 올리고머 제조 및 듀얼 오브너블 용기(Dual-Ovenable Packaging) 용 폴리에테르이미드에 대한 적용 연구)

  • Seo, Jongchul;Park, Su-Il;Choi, Seunghyuk;Jang, Wongbong;Han, Haksoo
    • Korean Chemical Engineering Research
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    • v.48 no.1
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    • pp.45-52
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    • 2010
  • Two different imide oligomers(6FDA-ODA/APA and 6FDA-MDA/MA) having crosslinkable end groups were prepared by using a solution imidization method and their properties were investigated. Also, semi-interpenetrating polymer networks(semi-IPN) were prepared using the blends of imide oligomers with polyetherimide $Ultem^{(R)}$, which is used in dual-ovenable packaging materials. The characteristic properties of semi-IPN films were interpreted by using TGA, Thin Film Diffusion Analyzer, and WAXD. Molecular weights of imide oligomers were successfully controlled utilizing 2-aminophenylacetylene(APA) and maleic anhydride(MA) as an endcapping agent. Exotherm reactions by crosslinking appeared and the amount of exthotherm heat was linearly increased as the content of imide oligomers was increased. For semi-IPNs of $Ultem^{(R)}$ and imide oligomers, 5% and 10% weight loss temperatures increased as the contents of imide oligomers were increased. Diffusion coefficient and water uptake of semi-IPNs decreased as the content of imide oligomers was increased, which might be resulted from hydrophobic fluorine group and high packing density. It was concluded that relatively low thermal stability and hydrolytic stability of polyetherimide $Ultem^{(R)}$ were improved by incorporating new developed imide oligomers.

Dissolution Profile Analysis of Hydroxypropyl Methylcellulose-based Vitamin C Tablets (Hydroxypropyl methylcellulose를 활용한 비타민 C 지속성 정제의 용출 특성 분석)

  • Cha, Ja-Hyun;Hong, Jun-Kee;Lee, Sung-Wan;Cha, Jae-Uk;Ko, Won-Hwa;Baek, Hyon-Ho;Park, Hyun-Jin
    • Korean Journal of Food Science and Technology
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    • v.44 no.3
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    • pp.274-279
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    • 2012
  • The objective of this study was to develop oral matrix tablets for the sustained release of vitamin C. In this study hydroxypropyl methylcellulose (HPMC) has been utilized as an excipient, as it is one of the most widely used polymers, for use during long periods of time in formations. The vitamin C tablet formulation depends on the molecular weight and concentration of sustained-delivery in HPMC. Anti-oxidants have been added as a dissolution medium in order to prevent vitamin C degradation in water. The dissolution test was carried out in a distilled water medium, and the release model equation was applied to analyze the vitamin C release pattern. The results demonstrated that the release and lasting power of vitamin C tablets, containing HPMC, lasted for more than 12 h.

The development of biodiesel production technology for additional improvement of Rapeseed (유채의 부가가치 향상을 위한 바이오디젤 생산 기술 개발)

  • Lu, Jeong-Woo;Park, Gi-Don;Kwon, En-Suk;Ko, Jeong-Hwan
    • 한국신재생에너지학회:학술대회논문집
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    • 2006.11a
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    • pp.537-540
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    • 2006
  • 국제 유가의 상승으로 대체 에너지개발의 필요성이 대두되고 있는 지금 수송연료인 디젤의 대체 원료로 바이오디젤이 부각되었다. 차세대 대체연료인 바이오디젤의 합성 원료의 국산화로 수급의 안정성과 농가소득향상을 위해서 국내산 유채 착유기의 개발 및 유지의 함량을 측정하고 바이디젤로서의 적용가능성을 살펴보며 유박에서의 유지 추출 Biomass활용방안을 도출한다 국내산 유채 착유기 및 착유기술 평가를 통해 중소형 유채 착유기의 제작과 기본 조건을 도출을 위해 유채 착유실험을 진행하였다. 유채유의 착유온도에 따른 물성변화와 산가, 수분, 착유율의 변화와 영향을 확인하기 위해 roaster의 온도를 고온과 저온으로 나누어 착유하여 각각의 물성 실험과 산가, 수분, 착유율을 측정 비교하였다. 유채유는 저온보다 고온에서 착유량이 높으나 많은 검질과 높은 산가로 인해 바이오디젤 합성과정에 많은 어려움을 나타내었다. 유채의 유박을 바이오디젤과 에탄올로 각각 Extraction.한 결과 바이오디젤보다는 에탄올이 적용 가능성이 높음을 확인하였다.

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돈육의 사후 처리시간이 유화형 소시지의 품질에 미치는 영향

  • Yang, Han-Sul;Jeong, Jin-Yeon;Ali, Sawoocut;Ju, Seon-Tae;Park, Gu-Bu
    • Proceedings of the Korean Society for Food Science of Animal Resources Conference
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    • 2005.10a
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    • pp.157-160
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    • 2005
  • 사후처리시간에 따른 유화형소시지의 제조시 강직근의 낮은 pH는 제품의 유화안정성 및 가열감량을 높여 최종제품의 결착력 및 형태에 부정적인 영향을 미치는 것으로 사료되나, 이러한 낮은 수분보습력의 결과와는 달리 강직근 및 강직후근에 비해 낮은 명도 및 높은 적색도를 보여 온도체육의 가공 특성인 발색 향상과 일치하는 것으로 나타나 이에 대한 연구가 더 이루어져야할 것으로 판단된다. 또한 온도체육의 낮은 brittleness, hardness 및 gumminess은 제품의 결착력 감소에 따른 결과이며, 강직근의 높은 brittleness, hardness 및 gumminess은 사후강직을 통한 낮은 수분보습력에 기인한 것으로 사료된다.

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Study on the Physical Property of Epoxy Polymer Related with Degree of Permeation to Soil for Moving Historical Site (유구 이전용 에폭시 폴리머의 토양 침투도와 관련된 물성에 관한 고찰)

  • Wi, Koang-Chul;Seo, Jeong-Ho
    • Journal of Conservation Science
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    • v.25 no.2
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    • pp.155-160
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    • 2009
  • This study is designed to optimize the method of using SE-101 for strengthening the durability and the stabilization of moving historical site. The permeability and the shear strength of The epoxy SE-101 with low viscosity were measured on different particle sizes and moisture content of soil. Like it can be expected from the data of viscosity, as the soil particle size was increased, the permeability was also increased, while the shear strength was decreased. And especially, it is noted that the deviation of permeability can be more extreme according to the different hardening speed of macromolecule and mineral additives. As the rate of moisture content in soil sample is increased, the deviation between permeability and shear strength is also increased. Even though among the same soil sample, some parts of it can be weaker than others, which cause the breakages of epoxy products. Thus, it is necessary that the soil should be dried over 50% of permeation depth of SE-101 before use.

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Experimental Study for Thermal Characteristics of Frozen Soil Samples (동토 시료의 열적 특성 분석을 위한 실험적 연구)

  • Sewon, Kim;Sangyeong, Park;Jongmuk, Won;YoungSeok, Kim
    • Journal of the Korean Geosynthetics Society
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    • v.21 no.4
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    • pp.31-40
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    • 2022
  • Recently, the Arctic resource development project, where undeveloped energy resources (oil, natural gas, etc.) are deposited, is actively being promoted for the perspective of diversifying the construction market and developing future energy resources. However, the frozen ground always has problems such as sinking and frost-heaving due to extreme weather. Therefore, it is necessary to analyze the thermal characteristics of the frozen soil to secure the stability of the ground structure. In this study, a series of laboratory tests were performed to evaluated the thermal characteristics of frozen soil samples in the oil sand field in Alberta, Canada. In additon, it was compared with the results of domestic(Gangwond-do) sample performed under the same conditions. As a comparison results of the experiments, it was clarified that the different frozen water content and thermal conductivity characteristics by temperature after completion of freezing could affect the frozen soil behavior.

Highly Stable Graphene Field-effect Transistors using Inverse Transfer Method (역전사법을 활용한 고안정성 그래핀 기반 전계효과 트랜지스터 제작)

  • Lee, Eunho;Bang, Daesuk
    • Journal of Adhesion and Interface
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    • v.22 no.4
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    • pp.153-157
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    • 2021
  • Graphene, a two-dimensional carbon allotrope, has outstanding mechanical and electrical properties. In particular, the charge carrier mobility of graphene is known to be about 100 times higher than that of silicon, and it has received attention as a core material for next-generation electronic devices. However, graphene is very sensitive to environmental conditions, especially vulnerable to moisture or oxygen. It becomes a disadvantage in that the stability of the graphene-based electronic device, so various attempts are being made to solve this problem. In this work, we report a method to greatly improve the stability by controlling the surface energy of the polymer layer used for transferring the insulating layer of the graphene field-effect transistor. As the surface energy of the polymer used as the insulating layer was lowered, the stability could be improved by effectively controlling the adsorption of impurities in the atmosphere such as water molecules or oxygen.

화학증착법으로 제조한 실리카/알루미나 복합막의 기체분리특성과 stability에 관한 연구

  • 김성일;하홍용;남석우;홍성안;김인원
    • Proceedings of the Membrane Society of Korea Conference
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    • 1997.04b
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    • pp.27-28
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    • 1997
  • 최근 들어 분리공정의 발달과 산업의 고도화에 따라 기체 및 액체분리의 중요성이 강조되면서 열적, 화학적 그리고 기계적 안정성이 좋으며, 수명이 길고, 세척과 재생이 용이하며, 미생물에 의한 손상이 없는 무기막에 대한 연구가 진행중이다. 무기막은 기공의 크기에 따라 크게 다공성 막과 비다공성 막의 두 종류로 구분된다. 비다공성 금속막은 특정 기체에만 투과성을 가지며, 이때 기체는 용해-확산(solution-diffusion)기구에 의해 금속막을 투과하므로 특정기체에 대한 선택도는 매우 크나 투과도가 매우 작고 가격이 비싼 단점을 가지고 있다. 다공성 막은 기체 투과율이 큰 반면 기체 선택도가 작은 단점을 가지고 있다. 현재 기체분리에 사용되고 있는 무기막은 기공크기가 40${\AA}$ 이상으로 기체 분리가 Kundsen diffusion에 의해 이루어지므로, 기체 투과도는 큰 반면에 기체에 대한 선택도는 그리 크지 않다. 따라서 최근 들어서는 다공성 담체에 기공이 작은 ($d_{pore}<20{\AA}$)박막을 담지시켜 기체의 분리 선택도를 향상시키기 위한 연구가 활발히 이루어지고 있다. 본 연구에서는 유기금속 화학증착법(metal-organic chemical vapor deposition:MOCVD)을 이용하여 수소 선택성을 가지는 $SiO_2/Al_2O_3$ 복합막을 비율별로 제조하여 증착속도를 알아보고, 열과 수분에 노출시켜 박막의 기체투과도 변화를 살펴보았다.

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Weathering Properties and Slope Stability Evaluations of Bedrock under the Chokseongnu Pavilion, Jinjuseong Fortress, Korea (진주성 촉석루 성곽지반의 풍화특성과 사면안정성 평가)

  • Jo, Young-Hoon;Lee, Myeong-Seong;Lee, Sun-Myung;Lee, Chan-Hee
    • Journal of Conservation Science
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    • v.20
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    • pp.89-103
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    • 2007
  • The bedrock beneath the Chokseongnu pavilion consists of sandstone with alternate dark-gray to light-brown siltstone and dark-gray shale of the Jinju Formation, where bedding is well developed toward the Chokseongmun gate. Large to small joints and overbreak from the erosion weathering have been developed in the bedrock. Besides, water leakage from development of discontinuity planes, fragmentation of shale, crack and joint by tree roots are observed on the bedrock. While shale and siltstone showed high sensitivity in physical and chemical weathering, respectively, sandstone indicated the highest weathering sensitivity in both. As the results of structural stability analysis, the whole bedrock has high instability in wedge failures, and especially section No. II slope is more instable than section No. I. Therefore, it is necessary for the bedrock to be strengthened by improvement method for soft foundations and the surface reinforcement. The trees causing mechanical collapse of the bedrock should be also removed and a water flow prevention measure or a water exhaust are required.

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