• Title/Summary/Keyword: 소결광

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The Properties of Synthetic Calcium Ferrite for Ironmaking and Steelmaking using Industrial By-products - (1) (산업부산물을 활용한 제철·제강용 합성 칼슘 페라이트 특성 - (1))

  • Park, Soo Hyun;Chu, Yong Sik;Seo, Sung Kwan;Park, Jae Wan
    • Resources Recycling
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    • v.23 no.5
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    • pp.3-11
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    • 2014
  • Calcium ferrite is more effective binder for making sintered ore and flux for steel making because of it's low melting temperature. In this Study, calcium ferrite was made by calcinating method in the cement manufacturing process in order to reduce manufacturing costs and increase productivity. Limestone and calcination sludge were used as CaO source, steelmaking sludge, blast furnace dust and iron ore were used as Fe-bearing raw materials. The sintering temperature of specimens is in the range of $950{\sim}1170^{\circ}C$. For Calcium ferrite can be used 'binder for making sintered ore' or 'flux for converter/electric furnace' with a low melting point properties, the raw material characteristics and sintering properties were investigated.

Development of PLT($PbLaTiO_{3}$) pyroelectric materials (PLT($PbLaTiO_{3}$) 초전재료 개발(II))

  • Park, Sung-Kun;Bae, Seung-Choon;Kim, Ki-Wan
    • Journal of Sensor Science and Technology
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    • v.6 no.6
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    • pp.491-499
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    • 1997
  • We fabricated the ceramic PLT tablet which was composed of 5, 10 and 15 mol% lanthanum concentration and thin film PLT to develope pyroelectric materials, and investigated their characteristics. Using TG/DTA, we determined calcination and sintering temperature to sinter the PLT completely and to prevent volatilization of the Pb components. The calcination and sintering temperature were $850^{\circ}C$, $1150^{\circ}C$ respectively, and there was a lot of mass loss at higher sintering temperature. By measuring temperature-dielectric constant characteristics of ceramic tablet we investigated dielectric constant characteristics depends on La concentration. The Curie point of PLT with 5, 10 and 15 mol% lanthanum concentration were $330^{\circ}C$, $269^{\circ}C$ and $210^{\circ}C$ respectively. Using PLT ceramic tablet we observed IR detection characteristics, and then deposited PLT thin film by rf magnetron sputtering. We verified that PLT thin film fabricated with completely sintered PLT target had the same structure to target by investigating lattice constant and optical transparency.

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Reflector Design to Improve the Uniformity of an Irradiated Area Using a Xenon Flash Lamp (제논 플래시 램프 사용 시 조사 영역 균일도 개선을 위한 반사경 설계)

  • Kim, Seo-Young;Lee, Han-Yul;Jun, Won-Kyoun;Kang, Dong-Hwa;Jo, Ye-Ji;Jung, Mee-Suk
    • Korean Journal of Optics and Photonics
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    • v.30 no.5
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    • pp.197-203
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    • 2019
  • In this paper, we studied a reflector design that can improve the illuminance uniformity when using a xenon flash lamp in the photonic sintering process. To achieve complete sintering of substrates in the irradiated area, the light efficiency and illuminance uniformity were set to target performance. Existing elliptical reflectors or parabolic reflectors make it easy to satisfy the target light efficiency, but have difficulty satisfying the illuminance uniformity. In this paper, a twin-concave feature has been added to the center of the parabolic reflector to satisfy the illuminance uniformity. It was confirmed that the illuminance uniformity of the parabolic reflector with a twin-concave feature was improved, compared to that of the traditional reflector.

열.기계적 처리가 Simulate $UO_2$분말의 성질에 미치는 영향에 대한 연구

  • 송근우;김봉구;이정원;배기광;양명승;박현수
    • Proceedings of the Korean Nuclear Society Conference
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    • 1995.05b
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    • pp.739-744
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    • 1995
  • 연소도 33 MWD/kgU에 해당하는 simulate $UO_2$ 소결체를 제조하여, 산화 (대기중 40$0^{\circ}C$), 고온산화 (대기중 110$0^{\circ}C$), 환원 (수소분위기 $600^{\circ}C$)을 차례로 실시하였다. 이 분말을 다시 산화/환원 처리를 반복하면서 분말의 크기, 비표면적, morphology를 조사하였다. 분말의 비표면적은 고온산화에 의해서 크게 감소했다가 산화/환원 cycle이 반복될수록 증가하는 경향을 보인다. attrition 분쇄에 의해서 분말의 비표면적은 매우 커지며, 그 증가폭은 산화/환원 cycle이 많아질수록 커진다. 고온산화 후 산화/환원 cycle을 2회 반복했을 때 소결밀도가 가장 높았다.

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Investigation of the La1-x(Ca or Sr)xCrO3x=0 and 0.25) Interconnect Materials for High Temperature Electrolysis of Steam (고온수증기전기분해용 La1-x(Ca or Sr)xCrO3(x=0 and 0.25) 연결재 재료 연구)

  • Jeong, So-Ra;Kang, Kyoung-Soo;Park, Chu-Sik;Lee, Yong-Taek;Bae, Ki-Kwang;Kim, Chang-Hee
    • Korean Chemical Engineering Research
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    • v.46 no.6
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    • pp.1135-1141
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    • 2008
  • The $La_{1-x}(Ca\;or\;Sr)xCrO_3$(x=0 and 0.25) interconnect materials for high temperature electrolysis of steam were investigated in views of sinterability and electrical conductivity. $LaCrO_3$, $La_{0.75}Ca_{0.25}CrO_3$ (LCC), and $La_{0.75}Sr_{0.25}CrO_3$ (LSC) powders were synthesized by coprecipitation method. Crystal structure was confirmed by X-ray diffraction (XRD). The sintering characteristics were analyzed by relative density and scanning electron microscopy. The electrical conductivity was measured by a DC four probe method. From the analyses of relative densities, it was found that the doped $LaCrO_3$ showed better sinterability than $LaCrO_3$ and the those sinterability increased with decrease of those particle sizes. The XRD results at different sintering temperatures for LCC and LSC revealed that the sinterability is closely related to the second phase transformation, that is, the second phase melting above $1,300^{\circ}C$ for LCC and $1,400^{\circ}C$ for LSC significantly promotes the sinterability. In case of electrical conductivities of LCC and LSC, which had a similar relative density, LCC showed better electrical conductivity than LSC.

A Study on the Characteristics of $CdS_{1-x}Se_x$ Luminescent Devices grown by Electron Beam Evaporation Technique (E-Beam 증착기법에 의해 성장된 $CdS_{1-x}Se_x$ 발광소자의 특성연구)

  • 양동익;박성문;라경숙;최용대
    • Journal of the Korean Vacuum Society
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    • v.3 no.1
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    • pp.111-116
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    • 1994
  • 본 연구는 CdS, CdSe 분말을 불순물, flux와 혼합하여 질소 분위기에서 소결한 후 전자빔으로 증착하여 적절한 조건에서 열처리 하였다, 이 박막의 결정구조를 X-ray 회절 실험을 통하여 조사하고 제작된 CdS1-xSex 발광 소자의 전기적 특성은 Hall 효과 측정을 이용하고 광학적특성은 광발광 및 광전 류 스펙트럼, 감도, 최대 허용소비전력, 응답시간 등을 분서하교, 발광소자로서의 기능을 검토하였다.

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THE STUDY ON THE MANUFACTURE CERAMIC FERRULE AND SLEEVE FOR OPTICAL CONNECTOR (OPTICAL CONNECTOR 용 CERAMIC FERRULE 및 SLEEVE 제조에 관한 연구)

  • Cho, S.H.;Kang, S.I.;Son, S.K.
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1993.05a
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    • pp.6-10
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    • 1993
  • OPTIC COMMUNICATION MIDDLE EMPLOYS LIGHT AS A MEDIUM OF COMMUNICATION IS WIDELY USED AS MANY MIDDLE DISTANCE COMMUNICATION BECAUSE IT HAS MERITS OF LOW LOSS, WIDE OPTIC RANGE AND LARGE CAPACITATIZATION AND IS APPLIED TO OPTICAL UTILIZER NETWORK. LAN(LOCAL AREA NETWORK) FOR GREAT UTILIZER GROUPS. SO IN OPTICAL COMMUNICATION, THIS STUDY IS FOCUSED ON THE INVESTIGATION AND DEVELOPMENT OF A CERAMIC SWITCH CONNECTING WITH OPTICAL FIBERS. THE USED MATERIAL AS A CERAMIC SWITCH WAS A PARTIALLY STABILIZED ZIRCONIA WHICH IS USED AS A COMPOSITION MATERIALS PRECISION FORMING AND SINTERING WERE INVESTIGATED.

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Effect of Heat-Treatment in Se Atmosphere on the Densification of Absorber Layer Using $Cu(In,\;Ga)Se_2$ Nanoparticles ($Cu(In,\;Ga)Se_2$ 나노입자을 이용한 광흡수층 치밀화에 따른 Se 분위기의 열처리 효과)

  • Yoon, Kyung-Hoon;Kim, Ki-Hyun;Ahn, Se-Jin;Ahn, Byung-Tae
    • 한국신재생에너지학회:학술대회논문집
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    • 2006.06a
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    • pp.210-213
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    • 2006
  • 나노입자를 이용하여 치밀한 $Cu(In,\;Ga)Se_2$ 태양전지용 광흡수층을 제조하기 위해 먼저, 콜로이달 방법으로 합성된 20nm이하의 CIGS 나노입자를 저가의 스프레이 법을 이용하여 CIGS 막을 제조하였다. 제조된 CIGS막을 two-zone RTP (rapid temperature Process) 방법으로 Se 분위기 안에서 열처리를 행하였다. 입자의 치밀화를 위해 기판의 온도, Se 증발온도와 수송가스의 유량을 조절하여 CIGS 입자성장을 행하였다. 그러나, Se의 증발온도가 높을수록 CIGS와 MO 박막 사이에서 $MoSe_2$ 층이 형성되었다. 형성된 $MoSe_2$층의 부피 팽창으로 인해 하부의 유리기판과 Mo층 사이에서 peeling off 현상이 발생했다. 이러한 Peeling off현상을 억제하면서 CIGS 나노입자 성장을 하기 위해, Se 공급을 빨리 할 수 있도록 Se의 증기압을 높였으며, 최적조건에서 급속 열처리 공정을 통해 CIGS 나노입자 성장과 치밀화를 위한 소결거동을 관찰하였다.

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Difference of Translucency according to Drying Time after Staining of Dental Zirconia (치과용 지르코니아 착색 후 건조시간에 따른 반투명도의 차이)

  • Lee, Joo-Hee;Park, Jin-Young;Kim, Dong-Yeon
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.22 no.4
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    • pp.124-130
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    • 2021
  • Dental prosthesis translucency importantly contributes to aesthetic outcomes. The purpose of this study was to investigate the effect of drying time and zirconia coloring agent type on translucency. For the experiment, 90 circular specimens were fabricated for each zirconia block. Then, zirconia specimens were treated with a coloring agent for 180 seconds and dried for 0 seconds (undried), 30 seconds (intermediate dry), or 30 minutes (complete dry). Then, a specimen was placed on a black standard tile or a white standard tile, and using a standard D65 light source reflected was measured using the light removal method. A total of three repeated measurements were obtained per specimen. One-way ANOVA was used to compare and analyze the relationship between zirconia translucency and drying time. Zirconia and coloring liquid types were significantly associated with translucency (P < 0.001). Although no significant difference was observed with respect to drying time (P > 0.922), zirconia in the completely dried (30 minutes) state was more translucent.

Strength and Reduction Behaviour of Cold-bonded Pellet for Blast Furnace Burden using Iron-bearing Dust (함철 더스트를 원료로 한 고로용 비소성 펠릿의 강도 및 환원거동)

  • 김태동;백찬영;조종민
    • Resources Recycling
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    • v.4 no.1
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    • pp.60-68
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    • 1995
  • Iron-bearing dust which stems from steelworks were pelletized and bonded with portland cement in order to attempt to use for blast iurnace burdens. The characterist~cs of cold bonded dust pellet were investigated. It was found that the compression strength of cold bonded pellet contaning portland cement of 10 wt.% reached above 150kg/p by proper curing treatment. Direcl contad of carbon with iron oxides seems to greately enhance a reduction reaction and herewxth increased chances to lorn pores at high temperature environment. Tumbler strength, RDI, and swelling of cold bonded pellet were similiar to and/or better than those of iron ore sinter and fired pellet.

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