• Title/Summary/Keyword: 세선

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성장시 zinc nitrate의 농도에 따른 ZnO 나노구조체의 미세구조와 광학적 성질

  • Yang, Hui-Yeon;Park, Gyeong-Hun;Lee, Dae-Uk;Kim, Tae-Hwan
    • Proceedings of the Korean Vacuum Society Conference
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    • 2010.02a
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    • pp.187-187
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    • 2010
  • ZnO의 나노 구조는 화학적으로 안정하고 큰 결합에너지를 가지는 성질 때문에 청색 영역에서 작동하는 광전소자의 제작에 대단히 유용하다. ZnO 나노 구조들은 화학 기상 성장법, 기상 에피텍시 성장법, 화학적 용액 성장법과 같은 여러 가지 방법으로 성장하고 있다. 여러 가지 성장방법 중에서도 전기 화학 증착법으로 성장된 ZnO의 나노 구조는 가격이 저렴하고 낮은 온도에서 성장이 가능하며 대면적화를 할 수 있는 장점이 있다. 전기 화학 증착법으로 ZnO을 성장할 때 3개의 전극을 사용하여 성장하였다. ITO 기판을 음극으로 백금 전극을 양극으로 사용하였고 기준 전극은 Ag/AgCl을 사용하였다. Zinc Nitrate의 몰 농도를 변화하면서 ZnO 나노구조를 성장 하였다. 성장한 ZnO 나노구조를 $400^{\circ}C$에서 2 분정도 열처리를 하였다. 성장된 ZnO을 X-선회절장치를 분석하게 되면 (0002) 피크가 $34.35^{\circ}$에서 주되게 나타났다. 주사 전자 현미경상은 Zinc Nitrate의 몰 농도가 낮을 때 성장한 ZnO 는 나노세선 형태로 형성되었음을 보여주었다. Zinc Nitrate의 농도가 높아지게 되면 ZnO 나노구조가 나노 막대 또는 나노 접시 모양으로 변화되었다. 300 K에서 광루미네선스 스펙트럼은 형성된 나노구조가 엑시톤과 관련된 주된 피크가 Zinc Nitrate 농도에 따라 변화하게 되는 것을 알 수 있었다. 이 실험결과는 ZnO 나노구조의 미세구조와 광학적 성질이 Zinc Nitrate의 농도에 영향을 많이 받는 것을 알 수 있었다.

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Stress Intensity Factor Measurement of Inclined Crack in Tensile Plates by Use of Photoelasticity (광탄성법을 이용한 인장판의 경사균열 응력확대계수 측정)

  • Baek, Tae-Hyun;Lee, Chun-Tae;Kim, Young-Chul
    • Asia-pacific Journal of Multimedia Services Convergent with Art, Humanities, and Sociology
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    • v.5 no.2
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    • pp.215-222
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    • 2015
  • This paper presents the measurement of stress intensity factors of inclined cracks by use of photoelasticity. The distributions of isochromatics near a crack tip of the specimen loaded by uniaxially tensile load are used for analysis. Accuracy and reliability is enhanced by twice multiplying and sharpening the measured isochromatics using digital image processing. Photoelastic results are compared with those obtained by finite element method. Good agreement between them shows that the photoelastic analysis is reliable.

A Compare Study of Traditional Copper Alloy in East 3 Nations. (동양 3국의 전통 동합금에 관한 비교연구)

  • 임옥수
    • Archives of design research
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    • v.16 no.2
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    • pp.291-300
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    • 2003
  • In metalcraft, there are two kind of skills, one is forming and the other is decoration. And we could discern these skills as metal casting and metal hammering.. In metal casting, there are sand mould, cire perdus, stone mould and sealed monld; In metal hammering, metal forging, repousse technique and metal sheet making. After make form, craftman can use the decoration skills. There are chasing hammering, line carving, dotted line engraving, hair line engraving, kicking line engraving, ring punched ground, inlay, filigee and granulation skills. In korean traditional copper alloy, the craftman used forming and decoration skills. In Korea, tradionally the clatter use bronze for copper alloy; in case of Japan, they use violet coloring, and in case of Chinese, they like to use bronze used copper alloy. In case of Alloy, korean craftman used bronze traditionally, but recently the copper alloy skill is usually used; in case of Japan shibuichi and shakudo skills are used; and in Chinese copper, brass and cupronikel alloy are used.

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Analysis of Stress Distribution around a Central Crack Tip in a Tensile Plate Using Phase-Shifting Photoelasticity and a Power Series Stress Function (위상이동 광탄성법과 멱급수형 응력함수를 이용한 인장시편 중앙 균열선단 주위 응력장 해석)

  • Baek, Tae-Hyun
    • Journal of the Korean Society for Nondestructive Testing
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    • v.29 no.1
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    • pp.1-9
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    • 2009
  • This paper presents stress distribution around a central crack tip in a tensile plate using phase-shifting photoelasticity and a power series stress function. Isochromatic data along the straight lines far from the crack tip were obtained by phase shifting photoelasticity and were used as input data of the hybrid experimental analysis. By using the complex-type power series stress equations, the photoelastic stress distribution fields in the vicinity of the crack and the mode I stress intensity factor were obtained. With the help of image processing software, accuracy and reliability was enhanced by twice multiplying and sharpening the measured isochromatics. Actual and reconstructed fringes were compared qualitatively. For quantitative comparison, percentage errors and standard deviations of the percentage errors were calculated for all measured input data by varying the number of terms in the stress function. The experimental results agreed with those predicted by finite element analysis and empirical equation within 2 percent error.

Micropattern generation by holographic lithography and fabrication of quantum wire array by MOCVD (홀로그래픽 리소그래피에 의한 미세패턴 형성과 MOCVD에 의한 양자세선 어레이의 제작)

  • Kim, Tae-Geun;Cho, Sung-Woo;Im, Hyun-Sik;Kim, Young;Kim, Moo-Sung;Park, Jung-Ho;Min, Suk-Ki
    • Journal of the Korean Institute of Telematics and Electronics A
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    • v.33A no.6
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    • pp.114-119
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    • 1996
  • The use of holographic interference lithography and removal techniques to corrugate GaAs substrate have been studied. The periodic photoresist structure, which serves as a protective mask during etching, is holographically prepared. Subsequently periodic V-grooved pattern is formed on the GaAs substrate by conventional a H$_{2}$SO$_{4}$-H$_{2}$O$_{2}$-H$_{2}$O wet etching. The linewidth of a GaAs pattern is about 0.4$\mu$m and the depth is 0.5$\mu$m A quantum wires(QWRs) array is well formed on the V-grooved substrate by MOCVD (metalorganic chemical vapor deposition) growth of GaAs/Al$_{0.5}$Ga$_{0.5}$As (50$\AA$/300$\AA$) quantum wells. The formation of QWR array is confirmed by the temperature dependent photoluminescence (PL) measurement. The intensive PL peak with a FWHM of 6meV at 21K shows the high quality of the QWR array.

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Analysis of Photoelastic Stress Field Around Inclined Crack Tip by Using Hybrid Technique (하이브리드 기법에 의한 경사균열 팁 주위의 광탄성 응력장 해석)

  • Chen, Lei;Seo, Jin;Lee, Byung-Hee;Kim, Myung-Soo;Baek, Tae-Hyun
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.34 no.9
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    • pp.1287-1292
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    • 2010
  • In this paper, a hybrid technique is presented. First, the isochromatic fringe data of a given set of points are calculated by the finite element method and are used as input data in complex variable formulations. Then the numerical model of the specimen with a central inclined crack is transformed from the physical plane to the complex plane by conformal mapping. The stress field is analyzed and the mixed-mode stress intensity factors are calculated for this complex plane. The stress intensity factors are calculated by the finite element method as well as by a theoretical method and compared with each other. In order to conveniently compare these values with each other, both actual and regenerated photoelastic fringe patterns are multiplied by a factor of two and sharpened by digital image processing.

Stress Distribution of a Crane Hook by Photoelasticty Using 4-step Phase Shifting Method and finite Element Method (광탄성 4단계 위상 이동법과 유한요소법에 의한 크레인 훅의 응력분포 비교)

  • Baek, Tae-Hyun;Kim, Whan;Lee, Chun-Tae
    • Journal of the Korean Society for Nondestructive Testing
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    • v.24 no.1
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    • pp.38-44
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    • 2004
  • An experimental study for a crane hook was performed to investigate the stress distribution along a certain line where the maximum and minimum stresses to be developed. On this line, the isoclinic fringe and/or principal stress direction is constant. The crane hook was modeled into a 2-dimensional plate made of urethane rubber called 'Photoflex' The Photoflex is very sensitive to a load and has low photoelastic fringe constant. The Tardy compensation method with the fringe sharpening process and the 4-step phase shifting method, was used for the photoelastic technique. Experimental results by photoelasticity were compared with the calculated stresses from the simple curved beam theory and tile finite element analysis. Ail the results were close to each other.

Numerical Simulation on the Formation and Pinching Plasma in X-pinch Wires on 2-D Geometry (자기유체역학 코드를 이용한 축 대칭 엑스 핀치 플라즈마 구조의 2차원 전산해석)

  • Byun, Sangmin;Na, Yong-Su;Chung, Kyoung-Jae;Kim, Deok-Kyu;Lee, Sangjun;Lee, Chanyoung;Ham, Seunggi;Ryu, Jonghyeon
    • Journal of the Korea Institute of Military Science and Technology
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    • v.24 no.2
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    • pp.211-218
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    • 2021
  • This paper deals with the computational work to characterize the formation and pinching of a plasma in an X-pinch configuration. A resistive magnetohydrodynamic model of a single fluid and two temperature is adopted assuming a hollow conical structure in the (r,z) domain. The model includes the thermodynamic parameter of tungsten from the corrected Thomas-Fermi EOS(equation of state), determining the average ionization charge, pressure, and internal energy. The transport coefficients, resistivity and thermal conductivity, are obtained by the corrected Lee & More model and a simple radiation loss rate by recombination process is considered in the simulation. The simulation demonstrated the formation of a core-corona plasma and intense compression process near the central region which agrees with the experimental observation in the X-pinch device at Seoul National University. In addition, it confirmed the increase in radiation loss rate with the density and temperature of the core plasma.

CdTe 두께에 따른 CdTe/ZnTe 나노구조의 운반자 동역학과 열적 활성화 에너지

  • Han, Won-Il;Lee, Ju-Hyeong;Choe, Jin-Cheol;Lee, Hong-Seok
    • Proceedings of the Korean Vacuum Society Conference
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    • 2012.02a
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    • pp.298-299
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    • 2012
  • 현재 반도체 나노구조는 단전자 트랜지스터, 레이저, LED, 적외선 검출기 등과 같은 고효율 광전자 소자에서의 응용을 위해 활발한 연구가 진행 되고 있다. 이러한 응용 분야를 위한 다양한 종류의 나노구조 성장이 광범위하게 시도 되고 있지만 주로 III-V 족 화합물 반도체에 대한 연구가 주를 이룬 반면 II-VI 족 화합물 반도체에 대한 연구는 아직 미흡하다. 하지만 II-VI 족 화합물 반도체는 III-V 족 화합물 반도체와 비교했을 때 더 큰 엑시톤 결합에너지(exciton binding energy)를 가지는 우수한 특성을 보이고 있으며 이러한 성질을 가지는 II-VI 족 화합물 반도체 중에서도 넓은 에너지 갭을 가지는 CdTe 양자점은 녹색 영역대의 광전자 소자로서 활용되고 있다. 본 연구에서는 분자 선속 에피 성장법(molecular beam epitaxy; MBE)과 원자 층 교대 성장법(atomic layer epitaxy; ALE)으로 CdTe 두께에 따른CdTe/ZnTe 나노구조의 광학적 특성을 연구하였다. 광루미네센스(photoluminescence; PL)를 통해 CdTe/ZnTe 나노구조에서 CdTe 두께에 따른 에너지 밴드와 열적 활성화 에너지를 관찰하였다. 또한 시분해 광루미네센스(Time-resolved PL)를 통해 CdTe 두께에 따른 CdTe/ZnTe 나노구조의 운반자 동역학을 조사하였다. 저온 광루미네센스 측정 결과 CdTe 두께가 증가할수록 각 샘플의 피크는 더 낮은 에너지 영역대로 이동하는 것을 관찰할 수 있다. 1.2 에서 2.0 ML로 증가할 때 광 루미네센스의 작은 적색편이를 관찰할 수 있는데, 이는 CdTe 양자우물에서 양자점으로의 구조적인 전이가 일어남에 따라 구속효과가 증가하였기 때문이다. 또한 2.0 에서 3.6 ML까지 CdTe 두께가 증가할 때 측정된 적색편이 현상은 양자점의 사이즈 증가함에 따른 것이다. 마지막으로 3.6 에서 4.4 ML로 CdTe 두께가 증가할 때 큰 적색편이 현상을 볼 수 있는데 이는 CdTe 양자점에서 양자세선으로의 구조적 전이에 따라 구속효과가 증가하였기 때문이다. 온도 의존 광루미네센스(Temperature-dependent PL) 측정 결과 1.2 와 3.0 ML 두께의 CdTe/ZnTe 나노구조에서 구속된 전자의 열적 활성화 에너지가 18 과 35 meV로 관찰되었다. 3.0 ML CdTe/ZnTe 나노구조에서 가장 큰 열적 활성화 에너지를 갖는 것은 양자점의 균일도가 좋아지고 저차원 나노구조로의 구조적 전이가 일어나면서 운반자 구속효과에 다른 쿨롱 상호작용이 증가하였기 때문이다.

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High Tc Superconductor Fiber $YBa_2Cu_3O_{7-{\sigma}}$ Synthesized by the Sol-gel Process (Sol-gel 법에 의한 고온 초전도체 $YBa_2Cu_3O_{7-{\sigma}}$ 선재 합성에 관한 연구)

  • Jin Ho Choy;Jong Seok Yoo;Bae Whan Kim;Seung Tae Hong
    • Journal of the Korean Chemical Society
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    • v.33 no.3
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    • pp.326-331
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    • 1989
  • Superconducting fiber of high Tc $YBa_2Cu_3O_{7-{\sigma}}$ was successfully prepared by the sol-gel method. The stoichiometric mixture of Y, Ba and Cu nitrates was dissolved in water, to which citric acid solution was added. Then ammonium hydroxide was added to the mixture in order to increase the pH to a value between 5.8 and 6.2. The mixture was heated carefully to form a homogeneous colloid sol at 358 K. The solution was viscous enough to draw a long gel fiber, which was then heated at 1223K for 8 hrs. under oxygen partial pressure of $Po_2$ = 1 atm., cooled slowly and annealed at 723K for 13 hrs.. The reacted superconducting sample maintained a fiber form with some shrinkage of its volume. The superconducting transition temperatures (Tc, onset and Tc, offset) of $YBa_2Cu_3O_{7-{\sigma}}$ have been determined to be approximately 95K and 82K, respectively. The superconducting phase was also confirmed by Meissner effect at liquid nitrogen boiling temperature.

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