• Title/Summary/Keyword: 분체특성

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Preparation process of functional particles: III. Preparation of composite particles by rapid expansion of supercritical fluid solutions and release behavior (기능성 미분말의 제조공정에 관한 연구 : III. 초임계 분출법에 의한 복합분체의 합성과 용출특성)

  • ;;;Eiichi Abe
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.9 no.1
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    • pp.55-59
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    • 1999
  • The Rapid Expansion of Supercritical fluid Solutions (RESS) process was applied to particles coating. Microcapsules prepared by spray drying were used as the core particles, and two kinds of paraffin were used as the coating materials. Supercritical $CO_{2}$ solutions of paraffin were expanded through the short nozzle into the bed that was fluidized by air. Extraction temperature and pressure were varied at $50~120^{\circ}C$, $150~200\;kg/\textrm{cm}^2$, respectively. The thickness of theoritical coating layer ws measured, and precipitate coating layer on surface was analyzed by using SEM, FT-IR. The release behaviors of $Mg^{2+}$ ions were inspected by atomic absorbance spectrophtometer.

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Influence of HMDS additive on the properties of YAG:Ce nanophosphor

  • Choi, Kyu-Man;Kim, Yeo-Hwan;Lim, Hae-Jin;Yoon, Sang-Ok
    • The Journal of Korea Institute of Information, Electronics, and Communication Technology
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    • v.4 no.1
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    • pp.61-67
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    • 2011
  • Influence of hexamethyldisilazane(HMDS) in post processing technique by using n-butanol azeotropic distillation on the luminescence properties of YAG:Ce nanophosphor were studied. The organic solvent(n-butanol) azeotropic distillation which prevent powders from conglobation since lager molecules decrease the surface tension and more complete replace the residual water in the precipitate. HMDS that had larger molecules than that of n-butanol was added in azeotropic distillation. The phosphor synthesized from n-butanol azeotropic distillation exhibited lower agglomerate and better photoluminescence properties than that from HMDS added heterogeneous azeotropic distillation.

Development of combustion test device for study of aluminum powder combustion (알루미늄 분말 연소시험을 위한 장치 개발)

  • Hwang, Yong-Seok;Lee, Ji-Hyung;Lee, Kyung-Hun;Kim, Kwang-Yun;Lee, Sung-Woong;Yeo, Tae-Min
    • Proceedings of the Korean Society of Propulsion Engineers Conference
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    • 2011.11a
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    • pp.548-553
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    • 2011
  • The device for studying combustion characteristic of aluminum powder and water was developed. The device has ability to adjust temperature, pressure, and equivalent ratio to some specified value which effect on combustion characteristic of aluminum and water mixture. Methane combustor, water supply device, aluminum powder feeder, and linear combustor are assembled to aluminum combustion test device. Each device has the ability to supply matter to combustor on steady and quantitatively controlled manner and test sequence specified by user can be automatically controlled. The combustion of aluminum powder was observed when integrated device was operated normally.

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A Study of Mixing Characteristics for Cosmetic Pine Powder (화장품용 미분체 혼합공정에서의 분산특성 연구)

  • 이종옥;송건응
    • Journal of the Society of Cosmetic Scientists of Korea
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    • v.19 no.1
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    • pp.85-107
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    • 1993
  • The cosmetic fine powders were mixed with variation of mixing time(5) in the mixers (ribbon mixer, powder mixer, micropulverizer and fine impact mill). The powders were nixed with small amount of ferric oxide. as tracer. The mixed powders ere measured the particle size distribution, specific surface area and surface color with mixing time (s). The color variation, particle size distribution and specific surface area of the mixed powder exist a relationship with mining time(s) that can be expressed as mathematical equations to show the degree of the mixing of the powder mixture. The linear velocity of the impellar tip is the main factor contributing to he mixing efficiency of the mixers un this study. According to the linear velocity, he mixers used are devieded as convection mixing (ribbon mixer), sclera mixing powder mixer) and diffusion mixing (micropulverizer/fine impact mill).

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Construction of Schizosaccharomyces pombe spThp1 Null Mutants and its Characterization (분열효모 Schizosaccharomyces pombe에서 spThp1 유전자 결실돌연변이의 제조와 특성 조사)

  • Yoon Jin-Ho
    • Korean Journal of Microbiology
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    • v.42 no.2
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    • pp.149-152
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    • 2006
  • The sp%pl null mutant was constructed to study the function of fission yeast Schizosaccharomyces pombe spThp1, which is homologous to budding yeast Saccharomyces cerevisiae THP1. Tetrad analysis showed that the spThp1 is not essential for vegetative growth. The spThp1 null mutant also showed no massive poly(A)+ RNA export defect. However, spThp1 null is genetically associated with spMex67 null. These results suggest that spThp1 is involved in mRNA export out of the nucleus.

Construction of spSac3 Null Mutants Defective in mRNA Export (mRNA의 핵에서 세포질로의 이동에 관여하는 spSac3 유전자의 결실돌연변이 제조와 특성 조사)

  • Kang Sook-Hee;Yoon Jin-Ho
    • Korean Journal of Microbiology
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    • v.42 no.2
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    • pp.153-155
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    • 2006
  • We constructed the null mutants of fission yeast Schizosaccharomyces pombe spSac3 gene that is homologous to budding yeast Saccharomyces cerevisiae SAC3 involved in mRNA export out of nucleus. Tetrad analysis showed that the spSac3 is essential for vegetative growth. The spSac3 mutants harboring pREP81X-spSac3 plasmid showed poly(A)+ RNA export defect in the presence of thiamine. These results suggest that spSac3 is also involved in mRNA export from the nucleus.

Recycling and Characteristics of Plasma Melting Slag Materials Produced by Different Cooling Methods (플라즈마 용융방식으로 배출된 슬래그의 냉각방식에 따른 재료적 특성 및 재활용)

  • Chung, Juyoung;Bae, Wookeun;Kim, Moonil;Park, Seyong
    • Journal of the Korean GEO-environmental Society
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    • v.11 no.7
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    • pp.25-31
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    • 2010
  • In this study, it was intended to suggest new cooling method that enables to improve the applicability and added value higher than existing slag by applying new cooling method(powder cooling slag) at the time discharging slag, which is produced from the ash melting system that the plasma torch is used for the first time in Korea. It is suggested the applicative direction in the development of future recycling process by discovering its nature of material and applicative possibility as earthwork material. The ashes produced after the sewage sludge discharged from Y city was incinerated by the fluidized bed method and was used as test materials. As result of XRF(X-Ray Flourescence Spectrometry) analysis, main ingredient of sewage sludge ashes was $SiO_2$(32%) besides CaO, $Al_2O_3$, $Fe_2O_3$, and so on. In addition, as result of XRD analysis, traditional diffuse pattern of glass could be found from granulated air-cooled slags, while a minor crystal phase could be observed from powder cooling slag, because the powder on the surface exists in the state not melted. From EDX(Energy Dispersive X-ray Spectroscopy) analysis, it is deemed that powder ingredient has no change before and after it is used as cooling medium, and accordingly it is thought that the powder can be produced as the material where the function is added if used in different shape.

Rheological Evaluation of Blast Furnace Slag Cement Paster over Setting Time (고로슬래그 혼합 시멘트 페이스트의 응결시간 경과에 따른 레올로지 특성)

  • Cho, Bong-Suk;Ahn, Jae-Cheol;Park, Dong-Cheon
    • Journal of the Korea Institute of Building Construction
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    • v.16 no.6
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    • pp.505-512
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    • 2016
  • Even though high performance concrete was developed according to the trend of bigger and higher of reinforced concrete building, the rheological evaluations such as viscosity, yield stress are not enough to use as input data to accomplish the numerical analysis for the construction design. So there are many problems in the harden concrete such as poor compaction, rock pocket and crack, etc. in the field. In this study, consistency curves were measured by the viscometer as hydration reaction time passed. At the same time the slump flow test and Vicat setting test were carried out for comparing with the results of rheological properties. The fluidity of the W/B 30% decreased as the increase of replacement ratio of blast furnace slag. But in case of W/B 40%, the replacement ration did not significantly influenced to the slump flow value with the passage of hydration time. By the replacement of blast furnace slag to cement, initial setting was delayed and the time gap between initial and final setting became shorten. Through the regression analysis using Bingham model, there are a sudden changes of viscosity and yield stress around initial setting in case of low W/B 30%. The increase of workability by the change of free water in cement paste was offset by the coating effect of impermeable layer in case of W/B 40%.

The Study of Characteristics of Cosmetic Powder by Using Various Grinding mill (화장품용 분체의 분쇄방식에 따른 특성연구)

  • Shim, Seung-Bo
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.9 no.2
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    • pp.500-507
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    • 2008
  • By Using various grinding mill in powder cosmetics manufacturing process; screen milt and pin mill, jet mill, properties of the powder and grinding mills were studied; talc, mica, nylon powder, silica, titanium dioxide. Besides, the experiments fur evaluation of grinding were performed by using iron oxides those are tracers. In powders of plate shape, they were grinded more vertically than horizontally at the screen mill and pin mill, although were all grinded vertically and horizontally at the jet mill. The spheric powders became the primary particles or aggregation by electrostatic interaction at the screen mill and pin mill. But, at the jet mill, they resulted the agglomeration or transformation or damage up to 2bar. Titanium dioxides became the primary particles by all grinding mill. Pin mill has an excellent result in experiments which is a change of the tone of color by grinding. From these results, suggest that the jet mill is used to pre-treat of powders of plate shape in practical cosmetic manufacturing process, and the screen mill and pin mill are used to match the color of powder cosmetics. If industrial process condition is taken into consideration, suggest that 4times of grinding is excellent on grinding effect by the screen mill, and twice grinding by the pin mill and grind air pressure of 1bar by the jet mill.

Acrylamide Polymerization on ceramic Powders(I) : The Process Control of Si2N4 Gelcasting by Polymerization of Acrylamicde (세라믹분체 표면에서 아크릴아마이드 중합(제1보) : 아마이드 고분자중합에 의한 질화규소 겔캐스팅 공정제어)

  • 류병환;김은영;이재도
    • Journal of the Korean Ceramic Society
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    • v.36 no.2
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    • pp.178-185
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    • 1999
  • For the process control of silicon nitride gelcasting, the composition effect of acryamide system on the viscosity of slip and mechanical property of gelcast green body were investigated. The slip was prepared by ball milling of silicon nitride suspension prepared with acrylamide monomer and polyelectrolyte dispersant after premixing them by attritor. The slip mixed with initiator was vacuum deaired and cast into molds, and then polymerized. The consolidated green body was obtained by drying the gelated slip. The viscosity measument and the diametral compression test was done to evaluate the rheological behaviro of slip and mechanical property of gelcast body, respectively. Experimental results showed that the high solid loading of silicon nitride slip was obtained up to 46 vol% with a low viscosity. The mechanical property of gelcast body mainly increased with increasing the concentration of monomer. The gelcast body was machinable above the ∼3 MPa of tensile strength. The relative density of pressured-sintered body was 98.5% at 1760$^{\circ}C$, 3 h.

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