• Title/Summary/Keyword: 분광 측정기

Search Result 84, Processing Time 0.025 seconds

Studies on Eriophyes kuko Kishida and its Galls III. Quantitative Changes of Nucleic Acid in Growing Galls (구기자혹응애(Eriophyes kuko Kishida) 및 그 혹에 관한 연구 III. 혹의 성장에 따르는 핵산함량의 변동)

  • Kim Chang Hyo
    • Korean journal of applied entomology
    • /
    • v.10 no.2
    • /
    • pp.103-107
    • /
    • 1971
  • In this report, an experiment has been conducted to test the quantitative changes of nucleic acids in the nuclei of the epidermal cell of the galls, caused by Eriophyes kuko Kishida on the leaf of Lycium chinense Mill by means o( microspectrophotometric techniques, the two-wave-length methods. And the sizes of the epidermal cells and nuclei have been measured. The experimental results were summarized as follows: 1) It has been found that as the gall grows, the diameter of the epidermal cells and their nuclei increased and they were larger than those of tile healthy ones. 2) Microspectrophotometric measurement of nuclei by the 'Two-wave-length method' after staining with Feulgen reagent showed no changes in DNA content in the early stage of the gall. As the gall matured, however, DNA content of the gall increased more than that of the healthy leaf. 3) RNA-measurement of nuclei stained with Azur-B in DNase treated epidermal cells of the gall revealed that temporary increase in RNA content occurred in early to middle stages after the gall formation. As the gall matured, however, RNA content of the gall decreased more as against that of the healthy leaf.

  • PDF

Synthesis and Magnetic Properties of Expanded Graphite Oxide/Magnetic Nanoparticle Composite (Expanded Graphite 산화물과 자성 나노입자의 복합화와 자기적 특성)

  • Roh, Il-Pyo;Yim, Hyun-Joon;Kang, Myung-Chul;Rhee, Chan-Hyuk;Shim, In-Bo
    • Journal of the Korean Magnetics Society
    • /
    • v.22 no.1
    • /
    • pp.11-14
    • /
    • 2012
  • The composites of expanded graphite oxide and magnetic nanoparticle (Ni and Co) were synthesized by using simple chemical method. From the raw material natural graphite, the expanded graphite was fabricated using sulfuric acid and $1^{st}$ heat treatment at $600^{\circ}C$ for 1 hour. The expanded graphite was changed to expanded graphite oxide by 2nd heat treatment at $1050^{\circ}C$ for 15 sec and chemical oxidation. The expanded graphite oxide/1-methyl-2-pyrrolidone solution reacts with the magnetic nanoparticle to form a magnetic graphite oxide composite. These graphite-based materials were characterized by x-ray diffractometer, Raman spectroscopy, transmission electron microscope, and vibration sample magnetometer. We expect that these results of this paper were become basis research of graphite oxide composite.

The Hyperfine Interaction for the FeIn2S4 by Mössbauer Spectroscopy (뫼스바우어 효과를 통한 FeIn2S4에서의 Fe2+ 초미세 상호 작용 연구)

  • Son, Bae-Soon;Kim, Sam-Jin;Kim, Chul-Sung
    • Journal of the Korean Magnetics Society
    • /
    • v.17 no.1
    • /
    • pp.30-33
    • /
    • 2007
  • The $FeIn_2S_4$ exhibits an inverse spinel which Fe ions are occupied to the octahedral(B) site, while In ions are occupied to both the tetrahedral(A) and the octahedral(B) site. The $N\'{e}el$ temperature($T_N$) is determined to be 13 K. The effective moment of $FeIn_2S_4$ found to be $5.094{\mu}_B$ from the fit of Curie-Weiss inverse susceptibility for the temperature range over $T_N$, implying angular momentum contribution. The angular momentum contribution is shown in $M\"{o}ssbauer$ spectra for the antiferromagnetic ordering region($T{\leq}\;13K$), too. A weak $Fe^{2+}(B)-S^2-Fe^{2+}(B)$ interaction is responsible for a low $N\'{e}el$ temperature($T_N$) in $FeIn_2S_4$ system. The temperature dependence of electric quadrupole interaction is explained by z-axial crystalline field energy.

Investigation of High Frequency Properties of Y-type Hexaferrite Dependence on Synthesis Condition (소결 조건에 따른 Y-type Hexaferrite의 고주파 특성)

  • Lim, Jung Tae;Kim, Chul Sung
    • Journal of the Korean Magnetics Society
    • /
    • v.24 no.2
    • /
    • pp.56-59
    • /
    • 2014
  • The samples of $Ba_2CoZnFe_{12}O_{22}$ was synthesized by the solid-state reaction method. The toroids of $Ba_2CoZnFe_{12}O_{22}$ were sintered with various sintering temperature at 1050, 1100, 1150, and $1200^{\circ}C$, and studied by x-ray diffractometer, vibrating sample magnetometer, network analyzer, and Mssbauer spectrometer. From the XRD patterns, the density of samples increased with increasing sintering temperature. From the magnetic hysteresis curves up to 10 kOe at 295 K, the saturation magnetization ($M_s$) of $Ba_2CoZnFe_{12}O_{22}$ samples in various sintered at 1050, 1100, 1150 ,and $1200^{\circ}C$ were showed around $M_s$= 33.0 emu/g. However, With increasing sintering temperature, the coercivity ($H_c$) of samples decrease. Complex permeability and permittivity of samples in various sintering temperatures were measured between 100MHz to 4 GHz. With increasing sintering temperature, the permeability of samples increase.

Crystallographic and Magnetic Properties of $CoFe_{1.9}Ga_{0.1}O_4$ ($CoFe_{1.9}Ga_{0.1}O_4$의 결정학적 및 자기적 성질)

  • 이승화;김동회;김우철;홍성렬;김철성
    • Journal of the Korean Magnetics Society
    • /
    • v.9 no.1
    • /
    • pp.1-6
    • /
    • 1999
  • The crystallographic and magnetic properties of the ferrimagnetic $CoFe_{1.9}Ga_{0.1}O_4$ have been studied by X-ray, M$\"{o}$ssbauer measurements. The crystal structure is found to be inverse spinel structure with the lattice constant $a_0=8.386{\pm}0.005{\AA}$. M$\"{o}$ssbauer spectra of $CoFe_{1.9}Ga_{0.1}O_4$ have been taken at various temperatures ranging from 13 to 840 K. The isomer shifts indicate that the valence states of the Fe ions for tetrahedral (A) and octahedral (B) sites have ferric character. Debye temperatures for the A and B sites are found to be 882$\pm$5 K and 209$\pm$5 K, respectively. Atomic migration form the A to the B sites starts near 350 K and increases rapidly with increasing temperature to such a degree that 73% of the ferric ions at the A sites have moved over to the B sites by 700 K. by 700 K.

  • PDF

Fundamental study of electrolyte cathode atomic discharge for development of on-line monitoring system (On-line monitoring system 개발에 관한 음극 액상 글로우 방전의 기초 연구)

  • Kim, Kyung-Mi;Woo, Young-A;Cho, Won-Bo;Kim, Hyo-Jin
    • Analytical Science and Technology
    • /
    • v.15 no.6
    • /
    • pp.496-501
    • /
    • 2002
  • The electrolyte cathode glow discharge (ELCAD) is a new optical system for direct determination of trace heavy metals in flowing water. ELCAD has been successfully developed for on-line monitoring of heavy metals in flowing water. The application of an atmospheric glow discharge between an electrolyte solution cathode and a platinum rod anode led to the development of stable discharge. The fundamental aspects of new plasma source have been investigated. The fundamental study of ELCAD system has been measured plasma temperature using Einstein-Boltzmann equation after searching Fe atomic emission lines. The spectrum of each elements such as Cu, Pb, Fe, Ni and Cr show only major elemental line and no ionic line possibly due to low temperature plasma source. The detection limits of each elements are also investigated. These informations show that this type of plasma may apply for monitoring of heavy metals in waste water which consists of complex matrix.

Effect of the Surfactant Concentration on the Formation of Water Glass-based Porous Hollow Silica Microsphere (Porous한 물유리 기반 실리카 중공 미세구 형성에 대한 계면활성제 농도의 영향)

  • Lee, Jihun;Kim, Younghun;Kim, Taehee;Park, Hyung-Ho
    • Journal of the Microelectronics and Packaging Society
    • /
    • v.28 no.4
    • /
    • pp.79-83
    • /
    • 2021
  • In this study, hollow silica microspheres (HSM) of various sizes formed according to the concentration of surfactants using water glass as a precursor, which is advantageous for commercialization due to its lower unit cost compared to conventional silicon alkoxide (tetraethyl orthosilicate, TEOS) was synthesized. The physical properties of the silica hollow microspheres according to the concentration of surfactant were analyzed using Fourier transform infrared, contact angle measurement, Brunauer-Emmett-Teller and Barrett-Joyner-Halenda analyzers and field emission scanning electron microscopy. When porous water glass-based hollow silica spheres were prepared by adding a surfactant at an appropriate concentration, it was confirmed that excellent hollow silica spheres were formed with a specific surface area of 169 m2/g, an average particle size of 25.3 ㎛, and a standard deviation of 6.25.

Diagnosis of Nitrogen Content in the Leaves of Apple Tree Using Spectral Imagery (분광 영상을 이용한 사과나무 잎의 질소 영양 상태 진단)

  • Jang, Si Hyeong;Cho, Jung Gun;Han, Jeom Hwa;Jeong, Jae Hoon;Lee, Seul Ki;Lee, Dong Yong;Lee, Kwang Sik
    • Journal of Bio-Environment Control
    • /
    • v.31 no.4
    • /
    • pp.384-392
    • /
    • 2022
  • The objective of this study was to estimated nitrogen content and chlorophyll using RGB, Hyperspectral sensors to diagnose of nitrogen nutrition in apple tree leaves. Spectral data were acquired through image processing after shooting with high resolution RGB and hyperspectral sensor for two-year-old 'Hongro/M.9' apple. Growth data measured chlorophyll and leaf nitrogen content (LNC) immediately after shooting. The growth model was developed by using regression analysis (simple, multi, partial least squared) with growth data (chlorophyll, LNC) and spectral data (SPAD meter, color vegetation index, wavelength). As a result, chlorophyll and LNC showed a statistically significant difference according to nitrogen fertilizer level regardless of date. Leaf color became pale as the nutrients in the leaf were transferred to the fruit as over time. RGB sensor showed a statistically significant difference at the red wavelength regardless of the date. Also hyperspectral sensor showed a spectral difference depend on nitrogen fertilizer level for non-visible wavelength than visible wavelength at June 10th and July 14th. The estimation model performance of chlorophyll, LNC showed Partial least squared regression using hyperspectral data better than Simple and multiple linear regression using RGB data (Chlorophyll R2: 81%, LNC: 81%). The reason is that hyperspectral sensor has a narrow Full Half at Width Maximum (FWHM) and broad wavelength range (400-1,000 nm), so it is thought that the spectral analysis of crop was possible due to stress cause by nitrogen deficiency. In future study, it is thought that it will contribute to development of high quality and stable fruit production technology by diagnosis model of physiology and pest for all growth stage of tree using hyperspectral imagery.

Magnetic Properties of Superparamagnetic Ni-Zn Ferrite for Nano·Bio Fusion Applications (나노·바이오 융합응용을 위한 초상자성 Ni-Zn Ferrite의 자기적 특성연구)

  • Lee, Seung-Wha;Ryu, Yeon-Guk;Yang, Kea-Joon;An, Jung-Su;Kim, Chul-Sung
    • Journal of the Korean Magnetics Society
    • /
    • v.15 no.2
    • /
    • pp.100-105
    • /
    • 2005
  • $Ni_{0.9}Zn_{0.1}Fe_2O_4$ nanoparticles have been prepared by a sol-gel method. The structural and magnetic properties have been investigated by DTA/TGA, XRD, SEM, and $M\ddot{o}ssbauer$ spectroscopy, VSM. $Ni_{0.9}Zn_{0.1}Fe_2O_4$ powder that was annealed at $300^{\circ}C$ has spinel structure and behaved superparamagnetically. The estimated size of superparammagnetic Ni-Zn ferrite nanoparticle is around 10 nm. The hyperfine fields at 13 K for the A and B patterns were found to be 533 and 507 kOe, respectively. The blocking temperature ($T_B$) of superparammagnetic $Ni_{0.9}Zn_{0.1}Fe_2O_4$ nanoparticle is about 250 K. The magnetic anisotropy constant and relaxation time constant of $Ni_{0.9}Zn_{0.1}Fe_2O_4$ nanoparticle were calculated to be $1.6\times10^6\;ergs/cm^3$ and ${\tau}_0=5.0{\times}10^{-13}$ s, respectively. Also, Temperature increased up to $43^{\circ}C$ within 10 minutes under AC magnetic field of 7 MHz. It is considered that $Ni_{0.9}Zn_{0.1}Fe_2O_4$ powder that was annealed at $300^{\circ}C$ is available for biomedicine application such as hyperthermia, drug delivery system and contrast agents in MRI.

Review of applicability of Turbidity-SS relationship in hyperspectral imaging-based turbid water monitoring (초분광영상 기반 탁수 모니터링에서의 탁도-SS 관계식 적용성 검토)

  • Kim, Jongmin;Kim, Gwang Soo;Kwon, Siyoon;Kim, Young Do
    • Journal of Korea Water Resources Association
    • /
    • v.56 no.12
    • /
    • pp.919-928
    • /
    • 2023
  • Rainfall characteristics in Korea are concentrated during the summer flood season. In particular, when a large amount of turbid water flows into the dam due to the increasing trend of concentrated rainfall due to abnormal rainfall and abnormal weather conditions, prolonged turbid water phenomenon occurs due to the overturning phenomenon. Much research is being conducted on turbid water prediction to solve these problems. To predict turbid water, turbid water data from the upstream inflow is required, but spatial and temporal data resolution is currently insufficient. To improve temporal resolution, the development of the Turbidity-SS conversion equation is necessary, and to improve spatial resolution, multi-item water quality measurement instrument (YSI), Laser In-Situ Scattering and Transmissometry (LISST), and hyperspectral sensors are needed. Sensor-based measurement can improve the spatial resolution of turbid water by measuring line and surface unit data. In addition, in the case of LISST-200X, it is possible to collect data on particle size, etc., so it can be used in the Turbidity-SS conversion equation for fraction (Clay: Silt: Sand). In addition, among recent remote sensing methods, the spatial distribution of turbid water can be presented when using UAVs with higher spatial and temporal resolutions than other payloads and hyperspectral sensors with high spectral and radiometric resolutions. Therefore, in this study, the Turbidity-SS conversion equation was calculated according to the fraction through laboratory analysis using LISST-200X and YSI-EXO, and sensor-based field measurements including UAV (Matrice 600) and hyperspectral sensor (microHSI 410 SHARK) were used. Through this, the spatial distribution of turbidity and suspended sediment concentration, and the turbidity calculated using the Turbidity-SS conversion equation based on the measured suspended sediment concentration, was presented. Through this, we attempted to review the applicability of the Turbidity-SS conversion equation and understand the current status of turbid water occurrence.