• The Korean Journal of Rheology
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• v.3 no.2
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• pp.135-147
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• 1991

압출공정 중에 화학반응이 수반되는 경우에 화확반응은 온도와 체류시간분포 (Residence Time Distribution (RTD))에 의해 결정되므로 압출기의 설계 및 공정조건의 확 립에 있어서 RTD를 정확히 측정하거나 예측하는 것은 매우 중요하다. RTD를 예측하기 위 해 제안된 종래의 방법은 압출기내에서의 유동을 2차원으로 단순화하여 RTD와 체류시간분 포함수 f(T)와 누적 체류시간 분포함수 F(T)를 해석적으로 구하였다. 그러나 이러한 종래의 RTD에 관한 해석방법은 실제압출기 내부에서 일어나는 3차원적 순환유동(Circulatory Flow)을 정확하게 고려하지 못하는 문제점을 갖고 있다. 본논문에서는 RTD를 정확하게 예 측하기 위하여 3차원 순환유동을 고려한 RTD를 구하는 방식을 제시하고 f(T)에 관한 새로 운 공식을 유도하였다. 새로운 방식을 적용하기 위해서 유사 3차원(Quasi-3-Dimensional) 유한요소 해석법을 이용하여 속도분포를 구한 후에 순환유동을 고려한 RTD 및 f(T), F(T) 를 계산하였다. 순환유동이 고려안된 종래의 방법에 따른 계산 결과와 비교한 결과로서 종 래의 방식은 순환유동이 고려안되었기 때문에 RTD를 과소평가하는 경향이 있음을 알수 있 었다.

• Journal of the Korean Society of Food Science and Nutrition
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• v.32 no.8
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• pp.1270-1277
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• 2003

The extrusion conditions of the soymilk residue and corn grits mixtures were optimized. The experiment was designed according to the D-optimal design of response surface methodology (RSM), which shows 18 experimental points including 4 replicates for three independent variables (screw speed, water content and die temperature). The responses variables such as bending force, expansion ratio, bulk density, water solubility index (WSI), water absorption index (WAI), and color values (L＊, a＊, b＊) were evaluated using response surface analysis. Expansion ratio and WSI decreased with increasing water content, whereas bulk density tended to increase with increasing water content. While greater screw speeds enhanced WSI and yellowness, higher moisture contents decreased the expansion ratio and WSI value. However, die temperature did not influence upon the response variables. The optimum extrusion conditions by numerical and graphical methods were similar: the screw speed, water content, and die temperature were 250 rpm, 22.43% and l28.16$^{\circ}C$ by the numerical method; 250 rpm, 22.43%, and 128.02$^{\circ}C$ by graphical method.

• Korean Journal of Food Science and Technology
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• v.47 no.2
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• pp.149-157
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• 2015

The effects of feed moisture content (25, 35, and 45%), screw speed (230, 250, and 270 rpm), and barrel temperature (130, 140, and $150^{\circ}C$) on the product yield and soluble arabinoxylan (SAX) content from destarched corn fiber (DCF), and its optimization were investigated. The yield and SAX content of corn fiber gum (CFG) from the extruded destarched corn fiber (EDCF) were higher than those of DCF. Statistical analyses revealed that the feed moisture content and barrel temperature had a significant effect on the CFG yield and total SAX content. The optimum extrusion pretreatment conditions were as follows: feed moisture content, 30%; screw speed, 260 rpm; barrel temperature, $133^{\circ}C$. This study showed that the response surface methodology was suitable for the optimization of the extrusion conditions used to maximize the CFG yield and total SAX content from EDCF.

• Polymer Science and Technology
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• v.9 no.3
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• pp.193-199
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• 1998

• Korean Journal of Food Science and Technology
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• v.28 no.1
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• pp.169-178
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• 1996

Target parameters such as water solubility index (WSI), intrinsic viscosity (IV), water holding capacity (WHC), oil holding capacity (OHC), soluble dietary fiber (SDF) and microstructure were investigated on three different screw configurations during twin-screw extrusion of wheat bran. WSI of raw wheat bran (RWB) was 13.7%, while that of extrudates ranged $16.3{\sim}23.2%$ when extruded using screw configurations with 5 reverse screw elements (RSE). It was found that the moisture content of RWB greatly affected WSI of extrudates. IV of wheat bran extrudates increased from 10.6 ml/g of RWB to $37.86{\sim}44.37\;ml/g$ of extrudates extruded using 3, 4 and 5 RSE, whose trend was highly related to the moisture content of RWB and the extrusion pressure. Multiplication of IV and soluble solid (SS) content exhibited good correlation $(R^2=0.85)$ with specific mechanical energy (SME). The results suggested that SS and molecular size are an important factor governed by the SME in solubilization of wheat bran. WHC increased with increasing feed rate and moisture content, while OHC decreased. SDF increased from 2.68% of RWB to $4.32{\sim}6.48%$ of extruded wheat bran, indicating the significant breakdown of cell wall components. Microstructure of the extrudates showed the distinct patterns of degradation and solubilization of cell wall structure, depending on the moisture content of RWB.

• Clean Technology
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• v.12 no.4
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• pp.198-204
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• 2006

The modification of biodegradable polycaprolactone was accomplished by reactive extrusion with various contents of free radical initiator. Reaction conditions were in the temperature range of $130^{\circ}C$ to $180^{\circ}C$ with initiator contents of 0.1, 0.3, 0.5 and 1.0 wt%. To characterize the modified polycaprolactone (PCL), molecular weight was measured by gel permeation chromatography(GPC) and thermal, mechanical and rheological properties as well as biodegradability were measured. The modified PCL (MPCL) with 1% of initiator showed ca. 20% increase in crystallinity and ca. 50% increase in tensile modulus. Also, a large increase in rheological properties such as complex viscosity, storage and loss modulus was observed. The biodegradability of most MPCL was higher than that of virgin PCL.

• Journal of the Korean Ceramic Society
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• v.41 no.7
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• pp.560-566
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• 2004

To fabricate the continuously porous alumina bodies by multi-extrusion process, carbon powder and ethylene vinyl acetate were used as a pore forming agent and a binder, respectively. As the change of extrusion pass number, reduction ratio as well as the volume fraction of core and tube, the porous alumina bodies having various kind of pore size and porosity could be obtained. The porous bodies showed continuous pore shape, high specific surface as well as high bending strength, which were compared with those of commercial alumina bodies. In-vitro study was carried out using MG-63 osteoblast cells to investigate of their biocompatibility. As a result, the cells grew well on top and bottom as well as inside surface of pore. From the result of in-vivo study of 3-dimensional porous alumina bodies using rats, it was confirmed that any inflammatory response was not found in the subcutaneous tissue around porous body. Also the porous bodies removed from the rats were fully covered with well-developed fibrous tissues and showed the formation of new capillary blood vessels.

• Journal of the Korean Society of Food Science and Nutrition
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• v.33 no.10
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• pp.1742-1747
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• 2004

Effects of raw material composition, feed moisture and process temperature on chemical, physical and sensory properties of extrudates produced by a single-screw extruder from the mixtures of rice flour, isolated soy protein and file fish were evaluated through response surface methodology (RSM). Nitrogen solubility index (NSI), integrity index (II), rehydration ratio (RR), density, and the external appearance were measured as indices of physicochemical and sensory properties of extrudates. RR was negatively correlated with density (R=-0.742, p<0.0l). Increased amounts of rice flour in feed mixtures resulted in increased RR. The extrudate prepared from the mixtures of ISP, rice flour and file fish showed the highest sensory score at which extrusion temperature was 13$0^{\circ}C$ or above.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 1997.03a
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• pp.94-97
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• 1997

금속을 반고상 상태에서 성형하기 위하여 미세조직학적 거동을 밝히기 위해, 본 연 구에서는 높은 비강도, 내마모성을 가진 과공정 Al-Si 합금을 반응고 가공하였을 때의 미세 조직과 상온 가공 후 반고상 온도로 일정시간 유지하였을 때의 미세조직을 관찰하였다. 일 반주조시의 개량 원소 P과 Sr을 첨가하였으며 쐐기형 주조재, 압연재, Si 입자강화 Alrl 복 합재료를 반고상 상태로 가열한 미세조직을 관찰하여 초정 Si입자의 형상 변화를 관찰하였 다. 반응고 교반시 초기에는 P과 Sr의 첨가에 의해 초정 Si입자가 미세화 되었으나 교반이 지속되어 가면서 이러한 경향은 감소하였으며 구상에 가까운 형태로 변화 하였는데, 이는 교반이 지속되면서 첨가 원소의 효과보다 교반 자체의 미세조직 변화 기구에의 의존도가 높 아지기 때문인 것으로 사료된다. 냉각속도를 달리한 쐐기 형상에서의 금형에서 주조된 미세 조직을 관찰한 결과 냉각속도가 느릴 때에만 첨가원소의 영향이 나타났으며, 반고상 온도 유지 후 초정 크기에는 큰 변화가 없었으나 $\alpha$-halo가 형성되고 미세한 Si입자가 생성되었 다. 이는 입자 크기의 성장에 따른 주위의 농도구배로 인해 생성된 것으로 사료된다. 압연시 첨가원소는 핵생성과 재결정을 촉진시켜 초정 Si의 크기를 크게 감소시켰다. 반용융 처리시 초정 Si입자는 약간 성장하였으며, $\alpha$-halo도 생성되었다. 압출한 시료를 반용융 처리한 경 우 Si입자의 형상 변화는 거의 없었으며, Si입자에 형성되어 있던 산화막이 기지와 초정 Si 압자간의 확산장벽으로 작용하여 $\alpha$-halo가 거의 생성되지 않았다. 반응고 교반시 미세조직 변화 기구로는 취성파괴, 합체, 마모를 제안하였으며, 각 공정에서의 초정 Si결정의 크기를 비교하였을 때 45$\mu\textrm{m}$ 이하의 분말을 섞어 압출하였을 때 가장 작은 초정 Si입자 크기를 얻음 을 볼 수 있었다.

• Korean Chemical Engineering Research
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• v.59 no.3
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• pp.305-315
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• 2021

An intermeshing corotating twin screw extruder is mainly used for compounding polymeric materials. Twin screw extruder can adopt modular-type screw configurations, which directly controls the quality and productivity of the products. The types, shapes, and specifications of the screw and kneading elements are summarized, and the effects of screw configuration on the processabiliy of the materials are discussed. The principles of screw configuration universally applied to mass production of general-purpose resins are explained, and the guidelines of screw combination according to the roles of feeding, melt mixing, and metering zones are listed. The strategies of screw combination suitable for various cases, such as side feeding of liquid additives or inorganic fillers, reactive extrusion, devolatilization process, production of products requiring bright color and transparency, and processing of materials with low apparent specific gravity, are presented.