• Korean Journal of Mineralogy and Petrology
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• v.33 no.4
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• pp.419-426
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• 2020

Understanding the pore structure including pore shape and connectivity in unconventional reservoirs is essential to increase the recovery rate of unconventional energy resources such as shale gas and oil. In this study, we found analysis condition to probe the nanoscale pore structure in shale reservoirs using Focused Ion Beam (FIB) and Ion Milling System (IMS). A-068 core samples from Liard Basin are used to probe the pore structure in shale reservoirs. The pore structure is analyzed with different pretreatment methods and analysis condition because each sample has different characteristics. The results show that surface milling by FIB is effective to obtain pore images of several micrometers local area while milling a large-area by IMS is efficient to observe various pore structure in a short time. Especially, it was confirmed that the pore structure of rocks with high content of carbonate minerals and high strength can be observed with milling by IMS. In this study, the analysis condition and process for observing the pore structure in the shale reservoirs is established. Further studies are needed to perform for probing the effect of pore size and shape on the enhancement of shale gas recovery.

• Journal of the Korean Crystal Growth and Crystal Technology
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• v.26 no.6
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• pp.232-237
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• 2016

Cocrystallization of active pharmaceutical ingredients has been widely recognized as a versatile tool to regulate the physical properties of pharmaceutical compounds through designed crystal structures. Grinding or milling has been especially useful to screen the feasibility of cocrystal formation, and the addition of a small amount of liquid is routinely necessary. In the present study, the effect of temperature was studied for the milling cocrystallization of ibuprofen and nicotinamide to establish a liquid-free method. The milling-induced cocrystallization was more effective with liquid nitrogen cooling than at room temperature, which was confirmed by XRD and DSC analyses. This behavior was attributed to the limited molecular mobility below the glass transition temperatures of the cocrystal components, which made it effective to destruct the crystals of raw materials and consequently form the ibuprofen/nicotinamide cocrystal. Further studies would be necessary to establish the utility of the current conclusion to the field of pharmaceutical crystallization.

• Journal of Dental Rehabilitation and Applied Science
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• v.38 no.3
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• pp.127-137
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• 2022

Zirconia is fabricated through various processes. Each element in fabricating process can affect the physical properties of the definitive prosthesis. In particular, both the milling process and the sintering process can affect the final integrity of the zirconia prosthesis. Most of the milling machines adopt the ultra-precision 5-axis machining method, and the results vary depending on which milling method was used and how the milling equipment was managed. Milling blocks are selected according to cutting efficiency and aesthetic reproducibility. The sintering method can affect the grain growth and optical properties, and an accurate evaluation can be made only with additional research on the recent speed sintering procedure. Not only the sintering temperature but also the temperature holding time can affect the quality of definitive prosthesis.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.33 no.3
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• pp.210-217
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• 2009

This paper presents the analytical prediction of stability lobes in milling. The stability lobes are obtained by measuring the frequency response function (FRF) of a machining center at the cutting point of the end mill cutter, identifying cutting constants, and approximating cutting force coefficients. The stability lobes are experimentally verified through cutting tests.

• Journal of Hydrogen and New Energy
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• v.14 no.4
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• pp.313-320
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• 2003

볼밀링법을 이용하여 타이타늄 스펀지와 칩 또는 스크랩으로부터 상온애서 직접 타이타늄 수소와 분말을 재조하는 실험을 행하였다. 실험결과 진공중에서 볼링을 행한 타이타늄 스펀지와 칩의 경우 24시간외 후 합금분말의 크기는 약 20 um 정도의 크기를 갖는 것을 확인하였다. 그러나 수소화 분위기에서 볼밀링을 행한 경우에 12시간 후 수소화분말의 입도는 0.1-0.2 um로 극히 미세한 합금 분말이 제조되었다. 수소분위기에서의 볼밀링에 의한 타이타늄 분말제조는 기존의 방법에 비해 열을 가하지 않고 타이타늄 수소화분말을 얻을 수 있다는 장점과 나노크기의 미세한 수소화 분말을 얻을 수 있음을 알 수 있었다.

• Journal of Surface Science and Engineering
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• v.20 no.2
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• pp.77-85
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• 1987

최근 10년간 공구의 耐마모 코우팅 분야는 급속한 발전을 하여 왔다. 처음에는 초경 합금 인서트를 TiC로 단층 코우팅하였다. 코우팅 효과를 고려함에 따라 TiC, Ti(C,N), TiN으로 코우팅하게 되었고 또한 $Al_2O_3$ 코우팅도 많이 사용하였다. 처음의 코우팅은 공정작업의 어려움으로 극히 어려웠으나, 밀링작업에 대한 코우팅은 발달하여 왔다. 그림1.은 선반가공과 밀링작업을 하기 위한 초경 합금 인서트를 공구지지대로 지지하고 코우팅 한 것이다. 코우팅의 발전은 공구 코우팅과 강의 마모부분에 코우팅 하는 것으로 많이 발전하였다. 현재 CVD방법이 코우팅에 쓰이고 있으며 저온에서 강에 코우팅하는 작업에는 PVD방법을 도입하기에 이르렀고, 공구의 수명은 3~10배 증가하였으며 코우팅의 효과는 아래와 같이 요약된다. 1. 마찰력 감소, 열발생 감소, 절삭력 감소 2. 고속 절삭시 공구의 표면과 칩사이 확산 감소(코우팅은 확산 장벽으로 작용함) 3. 갤링(galling)을 막아줌. 공구의 수명 연장과 여러분야에 사용하기 위한 최적의 요구 조건은 다음과 같다. -공구재와 접촉시 화학적 안정성 -耐 산화성 -耐 마모성 -갤링의 방지 -耐 충격성 耐 열주기 -모재에 대한 코우팅 재의 충분한 접착성.

• Transactions of the Korean Society of Mechanical Engineers
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• v.9 no.5
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• pp.590-597
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• 1985

A recursive geometric adaptive control method to compensate for machining straightness error in the finished surface due to tool deflection and guideway error generated by end milling process is developed. The relationship between the tool deflection and the feedrate is modeled by a modified Taylor's tool life equation. Without a priori knowledge on the variations off cutting parameters, time varying parameters are then estimated by an exponentially windowed recursive least squares method with only post-process measurements of the straightness error. The location error is controlled by shifting the milling bed in the direction perpendicular to the finished surface and adding a certain amount of feedrate with respect to the tool deflection model before cutting. The waviness error is compensated by adjusting the feedrate during machining. Experimental results show that location error is controlled within a range of fixturing error of the bed on the guideway and that about 60% reduction in the waviness error can be achieved within a few steps of parameter adaption under wide operating ranges of cutting conditions even if the parameters do not converge to fixed values.

• Proceedings of the Korean Society of Precision Engineering Conference
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• 1994.04a
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• pp.415-419
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• 1994

공정계획(Process planning)이란 소재로 부터 제품을 경제적, 효율적으로생산하는데 필요한 방법의 체계적 인 결정이라고 정의 할수 있다. 일반적으로 공정계획에 관한 지식은 전문가의 오랜 경험을 통해 얻어지므로 공정계획을 수행하기 위해 전문가를 양산하기에는 많은 어려움의 따른다. 그리고 전문가의 지식 및 가공방법 자체가 여러가지 경우의 수를 가지는 불명확한 것이 많으므로 이를 체계적으로 지식 베이스(knosedge base)화 하여 이것을 이용한 자동공정계획시스템의 개발이 필연적이다. 본 연구에서는 절삭가공의 핵심이 되는 밀링가공을 대상으로 하며, AutoCAD 로 부터 자동 또는 대화식으로 부품의 형상 및 치수 데이타를 인식하고, 이 데이타를 기준으로 가공의 지식 베이스와 이론을 접목시켜 개발한 규칙을 통해 공구결정과 가공 표준시간 계산을 수행 하고자 한다. 본 연구에서 사용된 언어는 형상특징인식을 위한 ADS(AutoCAD Deveolpment System)와 객체지향적 언어인 Borland C 이다.

• The Journal of Korean Academy of Prosthodontics
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• v.55 no.4
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• pp.394-402
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• 2017

Purpose: The purpose of this study is to evaluate the displacement of artificial tooth of monolithic complete denture manufactured by milling and 3D printing method in which the denture base and the artificial teeth are simultaneously made. Materials and methods: Twelve upper and lower complete dentures for each were made by milling and 3D printing method. Group Up and Group Lp are a group of upper and lower dentures made by printing, and Group Um and Group Lm are denture groups made by milling. Group Uc and Group Lc are is a group of finally designed upper and lower dentures respectively. Measurements were performed between both central incisors (AB, ab), both canines (CD, cd), both first molars (EF, ef), between an incisor and a first molar (AE, ae), and between incisor and lingual point (AG, ag) for each upper and lower denture. Results: AG and ag value between printed dentures and original ones as well as between milled dentures and original ones showed a statistically significant difference (One-way ANOVA, P<.05) in both lower and upper monolithic dentures. In the lower monolithic ones, ab, cd and ef value revealed a significant difference between Group Lp and Group Lm (One-way ANOVA, P<.05). Conclusion: Dentures made using milling or 3D printers revealed statistically significant difference compared with those of original data. However, it showed clinically very accurate reproducibility.

• Proceedings of the Korean Society of Precision Engineering Conference
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• 2013.05a
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• pp.219-220
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• 2013