• 제목/요약/키워드: 미소재료

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Development and Verification of Large Triaxial Testing System for Dynamic Properties of Granular Materials (조립재료 동적물성 산정을 위한 대형삼축압축시험장비 구축 및 검증)

  • Lee, Sung-Jin;Kim, Yun-Ki;Choo, Yun-Wook;Lee, Sei-Hyun;Kang, Tae-Ho
    • Journal of the Korean Geotechnical Society
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    • v.26 no.12
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    • pp.5-17
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    • 2010
  • Coarse granular material is used as important fill material in most of large embankments such as railway, road, dam and so on. Therefore, the accurate design parameters of the coarse granular material are necessarily required in design and construction. The behavior of the coarse granular material was not well understood because of the lack of large testing equipment capable of coarse granular material. A large triaxial testing system was developed in this research, capable of large specimens of 500 mm, 300 mm and 150 mm in diameter. In the new large triaxial testing system, the load cell is installed inside the triaxial cell and axial displacement is measured locally on a specimen in order to improve control and measurement in small strain level. Urethane specimens of 300 mm and 50 mm in diameter were prepared. The large triaxial tests were performed on the 300 mm diameter urethane specimens while RC/TS and impact echo tests on the 50 mm diameter urethane specimens to verify this testing system. In this verification test results, we could ascertain the reasonable test results of the KRRI large triaxial testing system.

Fabrication and Electromechanical Behaviors of a SWNT/PANi Composite Film Actuator (탄소나노튜브/도전성폴리머 복합재 엑츄에이터의 제조 및 특성실험)

  • Zhang, Shuai;Kim, Cheol
    • Composites Research
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    • v.19 no.5
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    • pp.7-11
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    • 2006
  • The improved SWNTs/PANi composite actuator films applicable to an artificial muscle were fabricated successfully using a new process of manufacture that consists of 90% pure single-walled carbon nanotubes (SWNT) and chemical polymerization. PANi is electrically conducting polyaniline polymer. The conductivities of the composite SWNTs/PANi film-type actuators and the pure PANi films fabricated were measured as 56.15 S/cm and 17.38 S/cm, respectively, by the 4-prove method. The conductivity of the composite actuator is 3.2 times higher than the pure PANi film. The fabricated composite actuator showed higher conductivity than any other similar ones. The quality of samples was investigated by an electron scanning microscope (SEM). To measure the actuating strains, a specially designed beam balance apparatus was developed and strains of the composite actuators was measured by a laser displacement sensor subjected to electric currents. During the operation, the sample was soaked in the $NaNO_3$ solution and the sine-wave voltage in the range of $+1V{\sim}-1V$ was applied. The length of the composite actuator changed from $l_0=12.690$ mm to $l_1=12.733$ so that the change of length was l=0.043 mm and the strain was 0.34 %. This is a very high strain for this kind of a composite actuator. Other result reported by Tahhan showed 0.23 % strain, so that the present result is improved by 48%.

The Study on Peak Disappearance of Minor Phase and Formation of ${Al_3}Ti$ in Mechanically Alloyed Al-Ti Samples (기계적 합금화한 Al-Ti 시료에서 미소상 피이크의 소멸현상과 ${Al_3}Ti$ 형성에 관한 연구)

  • Kim, Jin-Gon;Kim, Hye-Seong;Kim, Byeong-Hui
    • Korean Journal of Materials Research
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    • v.11 no.12
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    • pp.1035-1041
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    • 2001
  • The refining process and solubility of Ti in Al matrix during mechanical alloying (MA) were investigated by using X-ray diffraction (XRD), transmission electron microscopy (TEM) as functions of alloy composition, milling time and ball to powder ratio (BPR). Mechanical alloyed samples were annealed for investigating their stability and the formation behavior of$Al_3Ti$in the temperature range from$200{\circ}C$to$600{\circ}C$. It is observed from present experimental that disappearance of Ti peaks in mechanically alloyed Al-10wt%Ti is not simply attributable to the dissolution of Ti into Al, but associated mainly with extreme refining and/or heavy straining of Ti particles The annealing of the mechanically alloyed Al-Ti powders show differences in aluminide formation behavior when Ti content in Al is equal to or less than l0wt% and higher than l5wt%Ti. When Ti-content in Al is equal to or less than l0wt%, the MA powders transform directly to a global equilibrium state forming $DO_{22}- type\;Al_3$Ti above$400{\circ}C$. In the Al-Ti samples with equal to or higher than l5wt%Ti, transitional phases of cubic$Al_3Ti$and tetragonal $Al_{24}Ti_8$ are formed above$400{\circ}C$. They are stable only below$500{\circ}C$, and, $DO_{22}-type\;Al_3Ti$ becomes dominant aluminide at temperature higher than$ 600{\circ}C$.

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A Study on Bonding Strength and Interfacial Structure of Copper-Stainless Steel Brazed Joint(ll) (동-스테인리스 강 브레이징 접합부의 계면조직과 접합강도에 관한 연구(ll))

  • Lee, U-Cheon;Gang, Chun-Sik;Jeong, Jae-Pil;Lee, Bo-Yeong
    • Korean Journal of Materials Research
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    • v.3 no.6
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    • pp.668-677
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    • 1993
  • The microstructural and shear tests of STS304/, STS430/ and low-C steel/Cu joints brazed using Cu-P, Cu-P-Sn(four type) and Cu-P-Sn-Ag(three type) filler metals at 1003 and 1033K for 1.2ks in Ar atomsphere were performed. Interfacial microstructures were divided into three type ; first, reaction layer contained cracks second, dispersed layer without cracks third, dispersed layer and reaction layer contained cracks. The joints composed only of dispersed layer without cracks have the high shear strength of above 40-60 MPa and result in failure in copper base metal. Low shear strength and joint failure result from the formation of reaction layer which induced cracks. The reaction layer is a Fe-P compound. This tendency of microstructure and shear strength depends on the existence and/or nonexistence of Sn in filler metals as well as Ni (and Cr) in base metals.

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Finite Element Analysis of Ultrasonic Wave Propagation and Scattering (초음파 전파 및 산란 문제의 유한요소 해석)

  • Jeong, Hyun-Jo;Park, Moon-Cheol;Park, Yun-Won
    • Journal of the Korean Society for Nondestructive Testing
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    • v.22 no.4
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    • pp.411-421
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    • 2002
  • The accurate analysis of ultrasonic wave propagation and scattering plays an important role in many aspects of nondestructive evaluation. A numerical analysis makes it possible to perform parametric studies, and in this way the probability of detection and reliability of test results can be improved. In this study, a finite element method was developed for the analysis of ultrasonic fields, the accuracy of results was checked by solving several representative problems. The size of element and the integral time step, which are the critical components for the convergence of numerical results, were determined in a commercial finite element code. Several propagation and scattering problems in 2-D isotropic and anisotropic materials were solved and their results were compared with known analytical or experimental results.

High Temperature Creep Characteristics Evaluation for Degraded Heat Resistance Steel of Power Plant by Mini-Specimen (미소시험편에 의한 재질열화된 내열강의 고온 크리프 특성 평가)

  • Lyu, Dae-Young;Baek, Seung-Se;Yu, Hyo-Sun
    • Korean Journal of Materials Research
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    • v.13 no.7
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    • pp.429-435
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    • 2003
  • In this study the new creep test using miniaturized specimen(10${\times}$10${\times}$0.5 ㎣) was performed to evaluate the creep characteristics for degraded materials of 2.25Cr-1Mo steel. For this creep test, the artificially aged materials for 330 hrs and 1820hrs at $630^{\circ}C$ were used. The test temperatures applied for the creep deformation of miniaturized specimens was X$630^{\circ}C$ and the applied loads were between 45 kg∼80 kg. After creep test, macro- and microscopic observation were conducted by the scanning electron microscope(SEM). The creep curves depended definitely on applied load and microstructure and showed the three stages of creep behavior like uniaxial tensile creep curves. The load exponents of virgin, 330 hrs and 1820 hrs materials based on creep rate showed 14.8, 9.5 and 8.3 at $550^{\circ}C$ respectively, The 1820 hrs material showed the lowest load exponent and this behavior was also observed in the case of load exponent based on creep rupture time. In contrast to virgin material which exhibited fined dimple fractography, a lot of carbides like net structure and voids were observed on the fractography of degraded materials.

Engineering Characteristics of Diatom Modified Soil Mixture (Diatom 혼합토의 공학적 특성)

  • Kim, Kyu-Sun
    • Journal of the Korean Geotechnical Society
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    • v.28 no.5
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    • pp.77-84
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    • 2012
  • The engineering characteristics of natural sediments containing diatom microfossils have been investigated for their abnormal deformation and strength behavior for a few decades. The presence of disk or hollow shape diatoms causes low compressibility, high hydraulic conductivity, and high shear strength of sediments. Some of these unusual differences show the characteristic of diatom owing to the interlocking of large interparticle porosity and angular particles. This phenomenon implies the possible use of diatom as modification materials to change the engineering performance of soil mixtures. This paper describes the engineering characteristics of diatom-kaolin mixture to investigate the engineering properties of diatom modified soils using conventional geotechnical tests and elastic and electromagnetic wave propagation tests. Experimental test results show the performance improvement by increasing diatom contents and the performance degradation by the breakage of interlocking between diatom particles under high effective stress.

A study on fatigue properties of plasma carburized low carbon Cr-Mo steel (플라즈마 침탄한 저탄소 Cr-Mo강의 피로특성에 관한 연구)

  • Park, Kyeong-Bong;Sin, Dong-Myung;Lee, Chang-Youl;Lee, Ktung-Sub
    • Korean Journal of Materials Research
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    • v.10 no.7
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    • pp.505-514
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    • 2000
  • The carburizing behavior and fatigue properties of the plasma carburized low carbon Cr-Mo steel(0.176C-1.014Cr-0.387Mo) have been investigated. The effective case depth in plasma carburized steel increased up to 50% in comparison with that of gas carburizing, and this case depth increased with the increasing surface carbon content. With increasing time in plasma carburizing, the surface carbon content increased but its increasing rate decreased. Fatigue properties were studied in terms of microstructure, case depth, retained austenite and residual stress near the surface. The fatigue limit of the plasma carburized steel was higher than that of gas carburized one. The initiation of microcracks and initial crack propagation were retarded due to a relatively little surface and internal oxidation layer in plasma carburized steel. Fractography showed the crack initiated at the surface, and transgranular fracture at surface layer was more predominant in plasma carburized steel compared to that of gas carburized steel.

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A Study of the Effects of Small Amount of Eu Impurities in α-Fe2O3 (α-Fe2O3 에 첨가한 미소량 EU 불순물의 효과에 대한 연구)

  • 오창헌
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.16 no.6
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    • pp.532-537
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    • 2003
  • Crystallographic, electric, magnetic and heat transition properties of $\alpha$-Fe$_2$O$_3$ have been studied with a small addition of Eu impurities. Hematite($\alpha$-Fe$_2$O$_3$) is a basic ferromagnetic material having rhombohedral structure, which is similar to perovskites structure. Eu is a rare earth element that has an electric configuration of 4f$^{7}$ 6s$^2$. X-ray diffraction pattern of Fe$_{1-x}$ Eu$_{x}$O$_3$ (x = 0.00, 0.04, 0.06) shows an increament of a value when the amount of Eu impurities increased. The VSM data show an increment of magnetization by increasing the amount of Eu impurity. The one with x=0.06 shows the largest increment of magnetic remanence. The magnetic remanence varied from 0.49$\times$10$^{-3}$ emu/g to 0.62$\times$10$^{-3}$ emu/g when Eu impurity is increased by 2 %. Coercivity is decreased as Eu impurity is increased. Resistances is reduced significantly by Eu impurity. There is a clear difference in temperature-dependent resistance depending on the amount of Eu impurities. Especially, there are cusps between 150 K to 175 K. It indicates the change of electronic quantum states inside the atoms by rare earth impurities in rhombohedral structure. Temperature-dependent heat capacity shows that the most effective amount of Eu impurities is 6 %. %.

A Study on the Recrystallization Behavior and Microstructure of Zr, Zircaloy-4 and Zr-Nb Alloys (Zr, Zircaloy-4, Zr-Nb 합금의 미세조직 및 재결정 거동에 관한 연구)

  • Lee, Myeong-Ho;Choe, Byeong-Gwon;Baek, Jong-Hyeok;Jeong, Yong-Hwan
    • Korean Journal of Materials Research
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    • v.10 no.6
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    • pp.422-429
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    • 2000
  • To investigate the effect of annealing temperature and time on the recrystallization behavior and microstructure of Zr-based alloys, the specimens of Zr-0.8Sn-0.4Nb-0.4Fe-0.2Cu, Zr-1Nb, Zircaloy-4, and unalloyed Zr were cold-worked and annealed at 400, 500, 600, 700, 800, $900^{\circ}C$ for 30 to 5000 minutes. The hardness, microstructure and precipitate of the specimens were investigated by using micro-hardness tester, optical microscope and transmission electron microscope, respectively. The recrystallization of Zr-based alloys occurred between $400^{\circ}C$ and $600^{\circ}C$. As the content of alloying elements increased, the hardness and recrystallization temperature of the alloys increased though the grain sizes after recrystallization decreased. It was supposed that the hardness of Zr-based alloy with Fe or Cu increased during recovery by the formation of Fe or Cu precipitates.

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