• Title/Summary/Keyword: 미소시편

Search Result 69, Processing Time 0.028 seconds

Effects of Property Transformation and Marginal Gap Depending on Heat-Treatment of Metal-Porcelain by Gold Electro-Forming System (전기성형법을 이용한 치과용 금속-도재관의 소성에 따른 물성 변화가 변연 간격에 미치는 영향)

  • Kim, Chi-Young;Chung, In-Sung;Choi, Sung-Min
    • The Journal of the Korea Contents Association
    • /
    • v.10 no.6
    • /
    • pp.352-359
    • /
    • 2010
  • The objective of this paper is to study on the property transformation for materials and to evaluate the precision through marginal gap depending on heat-treatment of metal-porcelain by the gold electro-forming system. Specimens for evaluating property of hardness treat non-treat(HC), once(H1), twice(H2), and three times(H3) by heating, respectively. Specimens for marginal gap classified as each groups of special bonder(FS), special bonder, opaque(FO), special bonder, opaque, body(FB) and non-treatment(FC). As a result for micro-hardness test, the level of hardness on each groups of H1, H2, H3 decreased rather than HC group(p<0.05). In addition, marginal gap was not affected by the number of times being treated by heating. Therefore, the marginal fitness and the precision for mterials were not affected by the heat-treatment on the process to make GES metal-porcelain.

Development and Verification of Large Triaxial Testing System for Dynamic Properties of Granular Materials (조립재료 동적물성 산정을 위한 대형삼축압축시험장비 구축 및 검증)

  • Lee, Sung-Jin;Kim, Yun-Ki;Choo, Yun-Wook;Lee, Sei-Hyun;Kang, Tae-Ho
    • Journal of the Korean Geotechnical Society
    • /
    • v.26 no.12
    • /
    • pp.5-17
    • /
    • 2010
  • Coarse granular material is used as important fill material in most of large embankments such as railway, road, dam and so on. Therefore, the accurate design parameters of the coarse granular material are necessarily required in design and construction. The behavior of the coarse granular material was not well understood because of the lack of large testing equipment capable of coarse granular material. A large triaxial testing system was developed in this research, capable of large specimens of 500 mm, 300 mm and 150 mm in diameter. In the new large triaxial testing system, the load cell is installed inside the triaxial cell and axial displacement is measured locally on a specimen in order to improve control and measurement in small strain level. Urethane specimens of 300 mm and 50 mm in diameter were prepared. The large triaxial tests were performed on the 300 mm diameter urethane specimens while RC/TS and impact echo tests on the 50 mm diameter urethane specimens to verify this testing system. In this verification test results, we could ascertain the reasonable test results of the KRRI large triaxial testing system.

Recrystallization TEP Behavior of Zr-based alloy by addition of Nb and Sn (Nb과 Sn 첨가에 따른 Zr 합금의 재결정 및 TEP 거동)

  • Jeong, Heung-Sik;O, Yeong-Min;Jeong, Yong-Hwan;Kim, Seon-Jin
    • Korean Journal of Materials Research
    • /
    • v.11 no.2
    • /
    • pp.104-114
    • /
    • 2001
  • To investigate the effects of the addition of Nb and Sn on the recrystallization of Zr- Sn-Nb alloys, both Vickers micro-hardness test and TEP measurement were carried out on cold-worked specimens annealed at various temperatures from $300^{\circ}C$ to 75$0^{\circ}C$. The microstructures of heat treated specimens were analyzed by optical microscope, SEM, and TEM. The study of microhardness and microstructures showed that both recrystallization process and grain growth were retarded as the activation energy was increased by the addition of Nb and Sn. Especially, the addition of Sn was more effective on retarding recrystallization. Precipitates were formed more easily when Nb was added because the solubility of Nb into Zr is lower than that of Sn. However, the recrystallization process was affected more by Sn than Nb because the strain field formed by substitutional Sn repressed the dislocation movement. TEP was increased due to the decrease of electron scattering as recovery and recrystallization were proceeded and saturated when the recrystallization completed. However, when precipitates formed, TEP was increased because the decrease of solute concentration near the precipitates caused the decrease of electron scattering.

  • PDF

Multi-scale Progressive Fatigue Damage Model for Unidirectional Laminates with the Effect of Interfacial Debonding (경계면 손상을 고려한 적층복합재료에 대한 멀티스케일 피로 손상 모델)

  • Dongwon Ha;Jeong Hwan Kim;Taeri Kim;Young Sik Joo;Gun Jin Yun
    • Composites Research
    • /
    • v.36 no.1
    • /
    • pp.16-24
    • /
    • 2023
  • This paper presents a multi-scale progressive fatigue damage model incorporating the model for interfacial debonding between fibers and matrix. The micromechanics model for the progressive interface debonding was adopted, which defined the four different interface phases: (1) perfectly bonded fibers; (2) mild imperfect interface; (3) severe imperfect interface; and (4) completely debonded fibers. As the number of cycles increases, the progressive transition from the perfectly bonded state to the completely debonded fiber state occurs. Eshelby's tensor for each imperfect state is calculated by the linear spring model for a damaged interface, and effective elastic properties are obtained using the multi-phase homogenization method. The fatigue damage evolution formulas for fiber, matrix and interface were proposed to demonstrate the fatigue behavior of CFRP laminates under cyclic loading. The material parameters for the fiber/matrix fatigue damage were characterized using the chaotic firefly algorithm. The model was implemented into the UMAT subroutine of ABAQUS, and successfully validated with flat-bar UD laminate specimens ([0]8,[90]8, [30]16) of AS4/3501-6 graphite/epoxy composite.

Effects of Aging on Properties of MgO-Partially Stabilized Zirconia (마그네시아 부분안정화 지르코니아 소결체의 특성에 미치는 열처리 효과)

  • 정형진;오영제;이홍림
    • Journal of the Korean Ceramic Society
    • /
    • v.24 no.3
    • /
    • pp.243-250
    • /
    • 1987
  • The effects aging on some properties and thermal-shock behavior of zirconia partially stabilized with 9 mol% MgO (9MZ) were studied. 9MZ specimens were aged over $1200^{\circ}$-$1400^{\circ}C$ for 12hours subsequently, after sintering at $1650^{\circ}C$ for 4 hours. Fracture strength(both before and after thermal-shock test), linear thermal expansion, monoclinic fraction and phase transition by XRD, density, galvanic potential and microstructure were measured. Quantitative chemical analysis around the grain-boundary of the specimen aged at $1350^{\circ}C$ was also conducted by EDX. The aging of 9MZ specimen causes a thermal decomposition of cubic-$ZrO^{2}$ into the formation metastable tetragonal-$ZrO^{2}$ and MgO. The former increases the residual strength after thermal-shock test and the latter improves the thermal-shock resistance due to thermal conduction through the continuous magnesia phase and the formation of monoclinic phase content in matrix were increased with decreasing the aging temperature from $1400^{\circ}C$ to $1200^{\circ}C$. Galvanic potential of the aged specimen exhibited a proper emf characteristic.

  • PDF

Damage Evaluation of Glass Fiber/PET Composite Using Acoustic Emission Method (음향방출법을 이용한 Glass Fiber/PET 복합재료의 손상평가)

  • 김상태;김덕윤
    • Composites Research
    • /
    • v.14 no.1
    • /
    • pp.1-7
    • /
    • 2001
  • In this study, damage evaluation of glass fiber reinforced thermoplastic composites was investigated with acoustic emission method. Specimens of 1.7mm thickness laminate were made from PET and 7 layers o171ass fabrics. Notch and impact loading were added to the specimen and normal tensile test and tensile test with the dead load were carried out. AE signal was measured as the functions of notch ratio to the width0 and impact energy in order to find out the correlation between fracture mode and AE parameters. The result has shown that low amplitude of AE signal was due to the microcrack of matrix and its growth, whereas the amplitude in the mid range was the response to the delamination and interfacial separation. In the range of high amplitude above 90dB. the fracture of glass fabric was found. Tensile strength decreased with increasing notch ratio to the width and impact energy because of tile effect or delamination, the cracking of matrix and stress concentration. In proportion to the size of damaged area. AE signal showed its wider range of frequency and energy as well as increased number of hits.

  • PDF

Production Process Development and Prototype Evaluation for Roller Tappet Housing of Valvetrain (밸브트레인용 롤러태핏 하우징의 제작 공정 개발 및 시제품 평가)

  • Gwak, Eun-Jo;Park, Sung-Young
    • Journal of the Korea Academia-Industrial cooperation Society
    • /
    • v.17 no.11
    • /
    • pp.223-229
    • /
    • 2016
  • In this study, a cold forging process was developed for the roller tappet housing of an engine valvetrain system. A tappet sample was manufactured and subjected to an endurance test. The material properties were obtained from a compression test, and forging analysis was carried out to design a forging process using a commercial program, Deform-3D. The forging process was set up based on the analysis results, and a die set and sample tappet housing were manufactured. To evaluate the sample, the dimensional accuracy, surface roughness, parallelism, and concentricity were measured and confirmed. To evaluate the actuation and durability, a special test rig was developed to simulate the valvetrain system of the engine. An actuation test was performed based on the idle speed of a general diesel engine, and an endurance test was done based on the maximum speed. The results show minor wear of 0.002 mm. The developed test rig will be used to evaluate the actuation and durability of other valvetrain parts.

The Power Loss Characteristics of Mn-Zn Ferrites at MHz Region with Sintering Condition (소성조건에 따른 MHz 대역의 Mn-Zn ferrite 전력손실 특성)

  • Suh J.J.;Song B.M
    • Resources Recycling
    • /
    • v.12 no.6
    • /
    • pp.26-31
    • /
    • 2003
  • The power loss characteristics of Mn-Zn ferrite were observed with the sintering temperature. In case of $1150 ^{\circ}C$ sintering, the core loss increased with measuring temperature, and does not have minimum value at the point where the magnetocrystalline anisotropy be 'zero'. This reason mainly due to the change of core loss mechanism with grain size which affects residual loss. The grain size and sintered density slightly increased with equilibrium oxygen partial pressure at$ 1150 ^{\circ}C$ sintering. The resistivity and initial permeability showed no significance with atmosphere, these results due to complex effect of $Fe^{2+}$ concentration and microstructure change. The core loss at $100^{\circ}C$ decreased as the equilibrium oxygen partial pressure increased.e increased.

Manufacturing Functional Nano-Composites by Using Field-Aided Micro-Tailoring Manipulation (Field-Aided Micro-Tailoring에 의한 기능성 나노복합재 제조)

  • Cho, Hee-Keun;Rhee, Juhun;Sim, Eun-Sup
    • Composites Research
    • /
    • v.25 no.6
    • /
    • pp.178-185
    • /
    • 2012
  • One of a unique technique in manipulating a multifunctional composite is demonstrated in this study. An electric field is applied to a liquid suspension in order to align the inclusions along with the direction electric field. This is called FAiMTa(Field Aided Micro Tailoring). It makes orthotropic polymer composites by arranging the micro and/or nano size particle inclusions in chain-line formation. Several kinds of particles such as $Al_2O_3$, graphite, CNT(Carbon Nano Tube), W(Tungsten) are tested to verify the effectiveness of the FAiMTa. The particles redistributed in an epoxy suspension and their coupons show that mechanical and thermal properties of orthotropic and random composites containing those particles depend on the trend of particles' alignment. The micro-images of the functional composite from FAiMTa have been captures and their physical properties demonstrate their wide-range and state-of-the-art application for advanced multifunctional composites.

Test method for Young's Modulus of Parallel Graded Coarse Granular Materials by Large Triaxial Test (대형삼축압축시험을 이용한 상사입도 조정 재료의 탄성계수 산정시험)

  • Lee, Sung Jin;Choo, Yun Wook;Hwang, Su Beom;Kim, Ki Jae
    • KSCE Journal of Civil and Environmental Engineering Research
    • /
    • v.32 no.5C
    • /
    • pp.211-220
    • /
    • 2012
  • Coarse granular materials such as gravel, rubble is used as major fill materials in earth structures of railway, road and dam. Therefore, it is essential to accurately evaluate properties of these materials for reasonable design and construction. In the precedent study, we built large triaxial testing system and verified system compliance with a focus on the dynamic properties. And we could secured the reliability of the system. In this study, the cyclic triaxial tests were performed in various experimental conditions on coarse granular material. Two series of parallel graded samples are prepared by mixing crushed rock. The influence of grain size, loading pattern, loading frequency, and fine contents were analyzed and discussed.