• Title/Summary/Keyword: 물회수

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Isolation and Purification of Tocopherols and Sterols from Distillates of Soy Oil Deodorization (대두유 탈취 증류분에 함유된 토코폐롤 및 스테롤의 분리정제)

  • Kim, Sun-K.;Rhee, Joon-S.
    • Korean Journal of Food Science and Technology
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    • v.14 no.2
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    • pp.174-178
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    • 1982
  • Various separation methods such as solvent extraction, chemical treatment and molecular distillation were tested for the separation of tocopherols and sterols from soy oil scum. The end products of these methods were tocopherol concentrates and sterol crystals. In the solvent extraction, purity and yield of tocopherols were 21.2% and 28.3%, and those of sterols were 69.2% and 2.6%. In the chemical treatment, purity and yield of tocopherols were 11.8% and 76.4% and those of sterols were 85.1% and 34.3% respectively. In the molecular distillation, purity and yield of tocopherols were 45.0% and 68.0%, and those of sterols were 49.3% and 57.0% respectively. The end products from the methods were characterized by HPLC. Based on the results of this study, the molecular distillation method was found to be more efficient than any other method tested.

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Recovery of Tin from Waste Tin Plating Solution by Ion Exchange Resin (주석도금폐액으로부터 이온교환수지를 이용한 주석 회수)

  • Shin, Gi-Wung;Kang, Yong-Ho;Ahn, Jae-Woo;Hyeon, Seung-Gyun
    • Resources Recycling
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    • v.24 no.3
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    • pp.51-58
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    • 2015
  • In order to recover tin from the waste tin plating solution, we used the ion exchange method using three types of ion exchange resins. The ion exchange resin with tertiary functional group(Lewatit TP 272) has not adsorption ratio of tin. The ion exchange resin with iminodiacetic functional group(Lewatit TP 207) has high adsorption ratio of tin, but impurity content in the recovered tin solution was relatively high. Whereas, in case of the ion exchange resin with functional group of ethylhexyl-phosphate(Lewatit VP OC 1026), adsorption ratio of tin was less than that of Lewatit TP 207. However, it was possible to remove impurities in the recovered tin solution by controlling the pH of the solution. High purity tin solution can be recovered by removing the organic materials with water washing process.

Study on the Recovery Process and Risk Management for Fusion Hydrogen Isotopes (핵융합 수소동위원소의 회수공정과 위험관리에 관한 연구)

  • Jung, Woo-Chan;Moon, Hung-Man;Chang, Min-Ho;Lee, Hyeon-Gon;Hwang, Myung-Whan;Woo, In-Sung
    • Journal of the Korean Institute of Gas
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    • v.23 no.6
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    • pp.81-89
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    • 2019
  • This study deals with a process for recovering hydrogen isotopes from fusion exhaust gas. The goal of this process is to remove impurities, maximally recover only pure hydrogen isotopes. Experiments using hydrogen and deuterium were conducted to confirm the possibility of the recovery of hydrogen isotopes. In the exhaust gas containing H2, impurities was removed in the membrane process, and only pure H2 was recovered. And the H2 in the exhaust gas of the He-GDC(Glow Discharge Cleaning) process was recovered using a cryogenic adsorption process. In addition, HAZOP analysis was performed for qualitative risk assessment. For scenario analysis, the damage prediction ALOHA program was used to calculate the range of influence. Finally measures were sought to improve safety.

A Study on the Estimation of Relative Compaction on the Subgrade using a Portable FWD (소형 FWD를 이용한 노상토의 다짐도 추정에 관한 연구)

  • Kang, Hee-Bog;Kim, Kyo-Jun;Kang, Jin-Tae;Kim, Jong-Ryeol
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.11 no.6
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    • pp.213-219
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    • 2007
  • This study was intended to estimate of relative compaction on the ground under the load using of portable FWD. The outcome in the wake of the study is highlighted as below. Viewing the variation of dynamic deflection modulus depending on a number of compaction, when a number of compaction increased to 8 (18.3MPa) from 4 (15Mpa), a dynamic deflection modulus increased 27%, and when a number reached to 12 (27.9MPa), it doubled the value indicated in 4. Viewing the relationship between dry density and dynamic deflection modulus in line with the increase in a number of compaction, a number of compaction by the roller reaching to the degree of compaction equivalent to 95% of max dry density was 13, with a dynamic deflection modulus indicating 27MPa ~ 29MPa.

Recovery of Presource from Sewage Sludge by a Struvite-forming Method (Struvite 결정화를 이용한 하수슬러지내의 인 자원 회수에 관한 연구)

  • Choi, Won-Joon;Park, Kyu-Man;Yoon, Bae-Geun;Kim, Min-Chul;Oh, Kwang-Joong
    • Journal of Korean Society of Environmental Engineers
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    • v.31 no.7
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    • pp.557-564
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    • 2009
  • The objective of this study is to efficiently recover phosphorus contained in sewage sludge by a struvite-forming method. The performances were evaluated under various operating conditions(elution with the kind of acid, Mg-compound and temperature) in order to reach the optimum conditions of struvite-forming. As a result, as an elution solution, the elution efficiency of $H_2SO_4$ was 2.65 times higher than that of HCl. Also, the precipitation efficiency of struvite was the highest (97.4%) in case of using $MgCl_2{\cdot}6H_2O$ as Mg-compounds at $25^{\circ}C$. However, the side reaction by Fe, Al and Zn appeared in process of phosphorus recovery. To solve some problems caused by side reacton, large quantities of co-precipitation materials produced by side reaction were removed by precipitating phosphorus compounds in pH 7. Consequently, the recovery efficiency of phosphorus by a struviteforming method was 82.99%, and purity of the recovered struvite product was high.

Influence of Midsummer Drainage Times on Growth and Lodging of Rice Plant in Direct Seeding on Flooded Paddy Surface (벼 담수표면직파 재배시 중간낙수 회수가 생육 및 도복에 미치는 영향)

  • Back, Nam-Hyun;Kim, Sang-Su;Park, Hong-Gyu;Shin, Hyun-Tak;Cho, Soo-Yeon;Lee, Seon-Yong
    • KOREAN JOURNAL OF CROP SCIENCE
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    • v.42 no.6
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    • pp.722-728
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    • 1997
  • This experiment was conducted to establish the cultural practice for reduction of lodging by the effective water management under direct seeding on flooded paddy surface as treated by the drainage times using Dongjinbyeo at National Honam Agricultural Experiment Station during 1994-1995. As the increased midsummer drainage times, the field lodging were reduced by reduction of culm length and large amounts of root with favorable distribution in deep soil, indicating low canopy architecture could promote the light transmission in the plants and favorable root growth. The yield performance was high by increased drainage times which contributed to mainly percentage of ripened grain and 1, 000-grain weight. As a result, two to three times midsummer drainage as effective water management during plant growth was desirable.

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A Study on Heat Transfer Characteristics of Humidifier/HRU for MCFC (MCFC용 가습기 및 HRU의 열전달 특성 연구)

  • Park, Sungho;Kal, Hanjoo;Jeong, Youngsik;Lee, Sanghoon;Lee, Jaejun;Oh, Yongmin;Kim, Seonhwa
    • 한국신재생에너지학회:학술대회논문집
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    • 2011.05a
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    • pp.97.2-97.2
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    • 2011
  • 본 연구는 연료전지 중 용융탄산염을 전해질로 하는 MCFC의 MBOP에 포함된 부품으로 매우 중요한 역할을 하는 가습기와 이때 발생되는 폐열을 회수하기 위한 장치인 HRU에 관한 것이다. 가습기는 연료와 물이 가습기 상부로 유입되어 가습기 하부로 유입되는 배가스와 열교환을 하면서 물이 스팀화 되어 연료가 가습된 상태로 가습기 출구로 일정온도를 유지하며 배출된다. 또한 HRU는 가습기에서 배출된 고온의 배가스를 물을 이용하여 열교환을 통해서 열을 회수하여 난방 및 온수로 사용할 수 있는 열교환 장치를 말한다. 먼저 이들의 특성을 파악하기 위해 가습기 및 HRU를 설계, 제작하여 각각의 특성을 확인하였다. 가습기와 HRU의 성능 향상을 위해 먼저 열교환부에 적용될 튜브의 수치해석적 분석을 통해서 최적의 열전달 성능을 얻을 수 있는 가습기 및 HRU를 설계, 제작하였으며 이들의 성능을 파악하기 위해 120,000kcal/h 용량을 테스트 할 수 있는 장치를 구축하여, 이들의 열전달 특성, 압력강하, 회수 열량, 가습기 온도 등의 특성을 파악하였다. 이 장치를 통해서 확인된 가습기와 HRU의 특성은 수치해석을 통해서 얻은 값과 거의 유사함을 확인할 수 있었으며, 가습 성능도 효과적으로 달성할 수 있었다. 가습기와 HRU의 특성 중 압력강하 부분은 지속적인 연구가 필요한 부분이며, 가습기와 HRU의 일체화를 통하여 소형화 및 설치공간 축소 효과를 얻을 것으로 본다.

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Recovery of High Purity Calcium Nitrate from Blast Furnace Slag (고로수재슬래그로부터 고순도 질산칼슘 회수에 관한 연구)

  • Yoo Jeong Kun;Lee Man Seung;Kim Kyung Soo;Choi Seung Hoon
    • Resources Recycling
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    • v.13 no.2
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    • pp.33-38
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    • 2004
  • Concepts and experimental results for the unique utilization process which we could obtain the high purity calcium nitrate from blast furnace slag in the steel industry are described. Firstly we reacted the blast slag with nitric acid and separatively removed the insoluble silica by filtration. We adjust the pH of filtrate to 6∼8 with calcined lime, and then precipiated out the metal components like Fe, Al, Mg in the forms of hydroxides. Consequently concentration of the mother liquor and crystallization processes make us obtain the high purity (>98 wt%) calcium nitrate tetrahydrates, which is expected the valuable fertilizers.

A Study on the Recovery of Aluminum from Aluminum dross (알루미늄 드로스로부터 알루미늄의 회수에 관한 연구)

  • 김홍진;김용현;이병우;이광학
    • Resources Recycling
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    • v.6 no.1
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    • pp.5-10
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    • 1997
  • The aluminum was recovered from the middle size (Q1.0-12.0 mm) aluminum drosses using NaCl and KC1 mixuture as a basic salt flux. The maximum aluminum recovery was about 76.9% when 40% basic salt flux was added to aluminum dross at 850$^{\circ}$C for two hours. Also, aluminum remvery increased with increasing fluoride (1%-5%) addition to basic salt flux. But, there was no considerable effect due ta the increasing of viscosity when the fluorides were added over 5%, respectively. E s p d y , the most aluminum recovery was about 83.5% when 5% cryolite was added to 40% basic salt flux.

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A Tandem Water and Hexane Washing Method for Economical Recovery of Paclitaxel from Biomass (바이오매스 유래 파클리탁셀의 경제적인 회수를 위한 물과 헥산의 순차적 세척 방법)

  • Lee, Myeong-Gi;Kim, Jin-Hyun
    • Korean Chemical Engineering Research
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    • v.60 no.1
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    • pp.169-174
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    • 2022
  • In this study, a tandem water and hexane washing process was developed to improve the recovery efficiency of paclitaxel derived from Taxus chinensis. The polar impurities contained in the sample were effectively removed by washing with water at a sample/water ratio of 1:40 (w/v) for 10 min. In addition, the non-polar impurities were effectively removed by washing with hexane at a sample/hexane ratio of 1:160 (w/v) for 20 min. A high purity of paclitaxel (>30.0%) was obtained in a short operating time (~30 min) by sequential washing with water and hexane.