• Korean Journal of Food Science and Technology
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• v.45 no.1
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• pp.25-33
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• 2013

Clenbuterol and ractopamine, which are ${\beta}$-agonists, have been misused as a growth promoting agent in meat producing animals. Clenbuterol was banned for veterinary drug in Korea because of its problems regarding safety. Due to their adverse effects, such as cardiovascular and central nervous diseases on human health proper control and monitoring should be conducted. The existing analytical method of clenbuterol and ractopamine in the Food code was improved through our present study. The bovine muscle samples were subjected to enzymatic hydrolysis, extracted with ethyl acetate and defatted by hexane-methanol partitioning. A molecular imprinted polymer (MIP) solid phase extraction cartridge was used for clean-up and LC-MS/MS was operated in positive multiple reaction monitoring (MRM). Clenbuterol-$d_9$ and ractopamine-$d_3$ were used as an internal standard. The renewed method was validated according to the CODEX guideline. The limits of quantitation for clenbuterol and ractopamine were 0.2 and 0.5 ${\mu}g/kg$, respectively. The mean recoveries ranged in 104.2-113.5% for clenbuterol and in 107.6-118.1% for ractopamine. The improved method was able to save both time and expenses.

• Journal of the Korean Geosynthetics Society
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• v.18 no.4
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• pp.115-127
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• 2019

The low-flow grouting injection technique, the target construction method for this study, is a method of pouring mortar into the ground by non-emission replacement principle, which can be expected to increase the density of the ground, and, in some cases, be used as a base file using the strength of the high injection solids, along with low noise, low pollution, and high durability. To verify that the dynamic characteristics of the ground are improved by the low-flow injection technique, the test work was conducted on the site and physical tests were performed, and the quality of the improvement formed in the ground was verified through the indoor test on the core and core recovery rate was analyzed. The density logs test layer calculated the volume density of the ground layer by using the Compton scattering of gamma-rays, and the sonic logs was tested on the ground around the drill hole using a detector consisting of sonar and receiver devices inside the drill hole. As a result of the measurement of the change in physical properties (density and sonic logs) before and after grouting, both properties were basically increased after infusion of grout agent. However, the variation in density increase was greater than the increase in speed after grouting, and the ground density measurement method was thought to be effective in measuring the fill effect of the filler. Strength and core recovery rates were measured from specimens taken after the age of 28 days, and the results of the test results of the diffusion and strength test of the improved products were verified to satisfy the design criteria, thereby satisfying the seismic performance reinforcement.

• Journal of the Korea Institute of Building Construction
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• v.17 no.2
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• pp.141-147
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• 2017

The purpose of this study is to develop an inorganic filling adhesive using MKP and borax based on Dead-burn magnesia and fly ash. First, basic experiments was conducted to derive the proper addition rate of MKP. And this experiment was carried out according to addition ratio of borax. The test items are measured for pot life, flexural strength, compressive strength, adhesive strength, tensile strength, ratio of temperature change, ratio of hardening shrinkage, radon gas and formaldehyde emission. As a result, the proper addition rate of phosphate was 35%. The pot time is about 10minutes, 15minutes and 25minutes according to addition rate of borax. The flexural strength and compressive strength were obtained at 12hours for minimum flexural strength of 8.0MPa and minimum compressive strength of 31.0MPa. The tensile strength was the least 4.1MPa, and the ratio of hardening shrinkage was maximum 2.4% and ratio of heat change was maximum - 0.3%, which satisfied all of the quality standards of 'KS F 4923' (epoxy resin for repairing concrete structures). Both Radon gas and formaldehyde emission was not detected.

• Korean Journal of Environmental Agriculture
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• v.20 no.4
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• pp.238-243
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• 2001

Mass reduction and physicochemical properties of the produced compost were investigated during composting domestic food wastes without additive. A small composter used in this study had the height of 15 cm from the center of bottom half circle (diameter 24 cm) up to under the lid, the side length of 50 cm and the horizontal lid angle of $50^{\circ}$ and was operated at the heating unit temperature of $85^{\circ}$. It was mixed by the rotating arm for two minutes in every half hour while supplied with air flow at 3 L/min for 10 minutes in every half hour. This condition was found in a preliminary experiment as optimal for keeping the water content of composting material in the optimal range without adding any bulking materials. The domestic food wastes were added into the composter at the rate of 1 kg/day without additives during composting. The results were as follows; during the composting process, water content maintained in the range of $51.0{\sim}53.5%$. Hemicellulose and lignin contents did not show any tendency, but cellulose content decreased. During the composting process, $NH_3-N$ and $NO_2-N$ were not detected due to nitrification. The contents of inorganic compounds did not increase during the composting process. They were in the range of $1.32{\sim}1.71%\;P_2O_5$, $1.29{\sim}1.48%\;CaO$, $0.41{\sim}0.49%\;MgO$, and $0.38{\sim}0.74%\;K_2O$. For 20 days, weight reduction rate was 67.5% in wet basis, and decomposition rate was 48% in dry basis. Concentration of heavy metals (Cu, Cr, Cd, Pb, Zn, Hg, As) was less than the limiting value of the compost. Maturity of the produced compost was 3 grade through reaching maximum temperature of $46{\sim}48^{\circ}C$.

• Economic and Environmental Geology
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• v.36 no.3
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• pp.149-157
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• 2003

Deep sea core samples were taken in the southwestern part of the Ulleung Basin in order to characterize the properties of shallow gases in the sediment. Amount of shallow gases in the sediments were calculated by head space techniques, and chemical and isotopic compositions of hydrocarbon gases were analyzed. Geochemical analyses were carried out on the gas bearing sediments to find out relationship between natural gas contents and organic characteristics of the sediments. Seismic characteristics of shallow gases in the sediments were also examined in this study. The amount of the hydrocarbon gases in the sediments range from 0.01% to 11.25%. Calculation of volume of gas per volume of wet sediment varies from 0.1 to 82.0 ml HC/L wet sediment. Methane consists 98% of the total hydrocarbon gases except for two samples. Based on the methane content and isotopic composition$(\delta^{13}c)$: -94.31$\textperthousand$~-55.5$\textperthousand$), the hydrocarbon gases from the sediments are generated from bacterial activities of methanogenic microbes. Contents of hydrocarbon gases are variable from site to site. Volume of shallow gases in the sediments shows no apparent trends vs. either characteristics of organic matter or particle sizes of the sediments. Gas concentration is high in the area of seismic anomalies such as blanking zone or chimney structures in the section. Physicochemically the pore water and the formation water systems are saturated with gases in these areas. Concentration of hydrocarbon gases in the sediments in these area shows favorable condition for generation of gas hydrate, as far as the other conditions are satisfied.

• Journal of the Korea Institute of Information Security & Cryptology
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• v.28 no.5
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• pp.1119-1127
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• 2018

Most of the cyber attacks are caused by malicious codes. The damage caused by cyber attacks are gradually expanded to IoT and CPS, which is not limited to cyberspace but a serious threat to real life. Accordingly, various malicious code analysis techniques have been appeared. Dynamic analysis have been widely used to easily identify the resulting malicious behavior, but are struggling with an increase in Anti-VM malware that is not working in VM environment detection. On the other hand, static analysis has difficulties in analysis due to various packing techniques. In this paper, we proposed malware classification techniques regardless of known packers or unknown packers through the proposed model. To do this, we designed a model of supervised learning and unsupervised learning for the features that can be used in the PE structure, and conducted the results verification through 98,000 samples. It is expected that accurate analysis will be possible through customized analysis technology for each class.

• Korean Journal of Soil Science and Fertilizer
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• v.37 no.1
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• pp.1-6
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• 2004

Agricultural recycling of livestock wastes by composting has lots of beneficial effects on crop production and soil fertility. Most of composts are made from pig manure and water content controller such as saw dust, bark, rice hulls etc. by aerobic processing. But the insufficient supply of saw dust, bark etc. cause the indiscreet use of industrial waste having heavy metals and toxic synthetic chemicals. This research investigated the present quality status of organic by-product fertilizers, and suggested the way of quality interpretation under the statistical approaches based on median, mean and weighted average value. Since the data of one hundred of samples for heavy metal contents (Cd, Pb, Cu, and Cr) and OM/N showed extremely left-skewed distribution, the median was more useful than the mean in representing the characteristics of distribiition for each items. The weighted average value will be a useful index for the quality based on the total amount of producing.

• Journal of the Korean Wood Science and Technology
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• v.41 no.4
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• pp.346-357
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• 2013

In this study, it was conducted to produce wood pellets using domestic forest thinning residues and examine their quality according to Korean pellet quality standard. Raw materials were composed of larch and mixed broad leaves species. Based on the small-end diameter (6 cm), they were classified into four different types of raw materials such as LM (larch with middle diameter), LS (larch with small diameter), MM (mixed broadleaf with middle diameter), and MS (mixed broadleaf with small diameter). After crushing and drying process, wood pellets were produced by a ring-die type pelletizer using each raw material. Wood pellets made from four different types of raw materials were tested for their quality such as calorific value, moisture content, ash content, inorganic matters and so on. As results of quality analysis, the calorific values of all wood pellets were higher than 198 kcal/kg, and satisfied with the first grade of Korea wood pellet standard. The ash content was slightly increased after pelletizing. Mechanical durability of wood pellets was highly dependent on the types of raw materials. The quality differences among wood pellets were turned out due to different physical and chemical characteristics of raw materials even though the same pelletizing condition was applied.

• Clean Technology
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• v.17 no.2
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• pp.166-174
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• 2011

The xAl-yCe oxide catalysts with different mol ratios of Al/(Al+Ce) were prepared by a co-precipitation method and Pt supported on xAl-yCe oxide catalysts were synthesized by an incipient wetness impregnation method. The catalysts were characterized by X-ray Diffraction (XRD), $N_2$ sorption, and $H_2$/CO-temperature programmed reduction ($H_2$/CO-TPR) to correlate with catalytic activities in co oxidation. Among the catalysts studied here, Pt/1Al-9Ce oxide catalyst showed the highest activity in dry and wet reaction conditions and the catalytic activity showed a typical volcano-shape curve with respect to Al/(Al+Ce) mol ratio. When the presence of 5% water vapor in the feed, the temperature of $T_{50%}$ was shifted ca. $30^{\circ}C$ to lower temperature region than that in dry condition. From CO-TPR, the desorption peak of $CO_2$ on Pt/1Al-9Ce oxide catalyst showed the highest value and well correlated the catalytic performance. It indicates that the Pt/1Al-9Ce oxide catalyst has a large amount of active sites which can be adsorbed by co and easy to supplies the needed oxygen. In addition, the amount of pentacoordinated $Al^{3+}$ sites obtained through $^{27}Al$ NMR analysis is well correlated the catalytic performance.

• Journal of the Korean Wood Science and Technology
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• v.39 no.3
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• pp.221-229
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• 2011

Due to the increase of oil price and the environmental issue such as the emission of volatile organic compounds, the necessity for developing alternative resins of petroleum-based adhesive resins, which have extensively been used for the manufacture of wood-based products, has been speculation since the early 1990. In our study, rapeseed flour (RSF), which is the by-product of bio-diesel produced from rapeseed, were hydrolyzed by enzymes. As a crosslinking agents of the RSF hydrolyzates, phenol-formaldehyde prepolymers (PF) were prepared. The RSF hydrolyzates and PF were mixed to complete the formulation of RSF-based adhesive resins, and the resins were applied to make the laminated veneer lumber (LVL). The physical and mechanical properties of the LVL were measured to examine whether RSF can be used as raw materials of adhesive resins for the fabrication of LVL or not. The average moisture content and soaking delamination rate of the LVL bonded with RSF-based adhesive resins exceeded the minimum requirement of KS standard. Moreover, thermal analysis of the RSF-based resins showed similar tendencies except for the RSF-based adhesive resins formulated with pectinase-hydrolyzed RSF. The bending strengths of the LVL were higher than that of the LVL made with commercial PF resins. These results showed the potential of RSF as a raw material of alternative adhesives for the production of LVL. Further works on the optimal conditions of RSF hydrolysis and spreading characteristics for RSF-based adhesive resins is required to improve the adhesive performance of RSF-based resins.