• Title/Summary/Keyword: 등변환법

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The Effect of Extrusion Temperature on Microstructure and Thermoelectric Properties of Rapidly Solidified P-type $P-type Bi_{0.5}Sb_{1.5}Te_3$ alloy (급속응고된 $P-type Bi_{0.5}Sb_{1.5}Te_3$ 합금 열전재료의 미세조직과 열전특성에 미치는 압출 온도의 효과)

  • 이영우;천병선;홍순직;손현택
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2001.11a
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    • pp.28-28
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    • 2001
  • $Bi_2Te_3$계 열전반도체 재료는 200 ~ 400K 정도의 저온에서 에너지 변환 효율이 가장 높은 재료로서 열전냉각 및 발전재료로 제조볍 및 특성에 관한 많은 연구가 진행되어 왔다. 전자냉각 모듈의 제조에는 P형 및 N형 $Bi_2Te_3$계 단결정이 주로 사용되고 있으나. $Bi_2Te_3$ 단결정은 C축에 수직한 벽개면을 따라 균열이 쉽게 전파하기 때문에 소자 가공사 수윤 저하가 가장 큰 문제점으로 지적되고 있다. 이에 따라 최근 열전재료의 가공방법에 따른 회수율 증가 및 열전특성 향상에 관한 열간압출, 단조와 같은 연구가 활발히 이루어지고 있다. 본 연구는 가스분사법(gas atomizer)을 이용하여 용질원자 편석의 감소, 고용도의 증가,균일고용체 형성, 결정립미세화 둥 급속응고의 장점을 이용하여 화학적으로 균질한$Bi_2Te_3$계 열전재료 분말을 제조하고, 제조된 분발을 압출가공하여 기계적성질, 소자의 가공성 및 열전 성능 지수율 향상시키는데 연구 목적이 있다. 본 설험에서는 99.9%이상의 고순도 Bi. Te. Se. Sb를 이용하여, 고주파 유도로에서 Ar 분위기로 용융하고, 가스분사법를 이용하여 균질한 $Bi_2Te_3$계 열전재료 분만을 제조하였다. 분말표면의 산화막을 제거하기 위하여 수소분위기에서 환원처리를 행하였고, 된 분말을 Al 캔 주입하여 냉간성형 한 후 진공중에서 압출온도를 변화시켜 열간압출 가공을 행하였다. 압출 온도변화에 따른 압출재의 미세조직 및 열전특성에 중요한 영향을 미치는 C면 배향에 대한 결정방위 해석, 압출재의 압축강도 등을 분석하였으며, 압출온도에 따삼 미세조직 변화와 결정방위의 변화에 따른 열전특성의 관계를 해석하였다성시켰고 이들이 산인 HNO3에서 녹았기 때문이다. 본 연구에서 개발된 새로운 에칭 용액인 90H2O2 - 10HNO3 (vol%)의 에칭 원리가 똑같이 적용 가능한 다른 종류의 초경 합금에서도 사용이 가능할 것으로 판단된다.로 판단된다.멸과정은 다음과 같다. 출발물질인 123 분말이 211과 액상으로 분해될 때 산소가스가 배출되며, 이로 인해 액상에서 구형의 기공이 생성된다. 이들 중 일부는 액상으로 채워져 소멸되나, 나머지는 그대로 남는다. 특히, 시편 중앙에 서는 수십-수백 마이크론 크기의 커다란 기공이 다수 관찰된는데, 이는 기공의 합체로 만들어진 것이다. 포정반응 열처리 시 기공 소멸로 만들어진 액상포켓들은 주변 211 입자와 반응하여 123 영역으로 변한다. 이곳은 다른 지역과 비교하여 211 밀도 가 낮기 때문에, 미반응 액상이 남거나 211 밀도가 낮은 123 영역이 된다. 액상으로 채워지지 못한 구형의 기공들 중 다수가 123 결정 내로 포획되며, 그 형상은 액상/ 기공/고상 계면에너지에 의해 결정된다.단의 경우, 파단면이 매끄럽고 파변상의 결정립도 매우 미세하였으며, 산확물 의 용집도 찾아보기 어려웠 나, 접합부 파단의 경우에는 파변의 굴곡이 비교척 심하고 연성 입계파괴의 형태를 보였£며, 결정립도 모채부 파단의 경우에 비해 조대하였다. 조대하였다. 셋째, 주상기간 중 총 에너지 유입률 지수와 $Dst_{min}$ 사이에 높은 상관관계가 확인되었다. 특히 환전류를 구성하는 주요 입자의 에너지 영역(75~l13keV)에서 가장 높은(0.80) 상관계수를 기록했다. 넷째, 회복기 중에 일어나는 입자들의 유입은 자기폭풍의 지속시간을 연장시키는 경향을 보이며 큰 자기폭풍일수록 현저했다. 주상에서 관측된 이러한 특성은 서브스톰 확장기 활동이 자기폭풍의

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A Study of Enhancing Reliability for Determining the Resistance to Surface Wetting by Imaging Process (이미징 기반의 발수도 판별을 통한 측정 신뢰도 향상에 관한 연구)

  • Kim, Sung-wuk;Chun, Sang Hee;Park, Jae Woo
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.18 no.7
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    • pp.483-489
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    • 2017
  • The purpose of this study was to propose useful suggestions for enhancing reliability to determine the resistance against surface wetting, KS K 0590, by an imaging process. We validated the standard spray test rating chart for determining quantification standard using JAVA script-based imaging process program. All of the acquired images were processed with the image software, Image J (NIH, Nethesda, MD, USA). The study results are as follows. We established the surface area measurement-based quantitative criteria for determining resistance to surface wetting. The standard spray test rating chart was converted into a numerical standard which leads easy-to-determine ratings. We also validated the procedure for imaging treatment by analyzing quantitative data. We introduced the fluorescence image for determining ratings by enabling threshold settings and binary image conversion as an optimal imaging process. It is expected that imaging-based determination for resistant to surface wetting will serve as an accurate and reliable method for KS K 0590.

Raising Visual Experience of Soccer Video for Mobile Viewers (이동형 단말기 사용자를 위한 축구경기 비디오의 시청경험 향상 방법)

  • Ahn, Il-Koo;Ko, Jae-Seung;Kim, Won-Jun;Kim, Chang-Ick
    • Journal of KIISE:Computing Practices and Letters
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    • v.13 no.3
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    • pp.165-178
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    • 2007
  • The recent progress in multimedia signal processing and transmission technologies has contributed to the extensive use of multimedia devices to watch sports games with small LCD panel. However, the most of video sequences are captured for normal viewing on standard TV or HDTV, for cost reasons, merely resized and delivered without additional editing. This may give the small-display-viewers uncomfortable experiences in understanding what is happening in a scene. For instance, in a soccer video sequence taken by a long-shot camera techniques, the tiny objects (e.g., soccer ball and players) may not be clearly viewed on the small LCD panel. Moreover, it is also difficult to recognize the contents of the scorebox which contains the elapsed time and scores. This renuires intelligent display technique to provide small-display-viewers with better experience. To this end, one of the key technologies is to determine region of interest (ROI) and display the magnified ROI on the screen, where ROI is a part of the scene that viewers pay more attention to than other regions. Examples include a region surrounding a ball in long-shot and a scorebox located in the comer of each frame. In this paper, we propose a scheme for raising viewing experiences of multimedia mobile device users. Instead of taking generic approaches utilizing visually salient features for extraction of ROI in a scene, we take domain-specific approach to exploit unique attributes of the soccer video. The proposed scheme consists of two modules: ROI determination and scorebox extraction. The experimental results show that the proposed scheme offers useful tools for intelligent video display on multimedia mobile devices.

Application of linear array microtremor survey for rock mass classification in urban tunnel design (도심지 터널 암반분류를 위한 선형배열 상시진동 탄성파탐사 적용)

  • Cha Young Ho;Kang Jong Suk;Jo Churl Hyun;Lee Kun
    • 한국지구물리탐사학회:학술대회논문집
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    • 2005.05a
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    • pp.157-164
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    • 2005
  • Urban conditions such as underground facilities and ambient noises due to cultural activity restrict the application of conventional geophysical techniques in general. We used the refraction microtremor (REMI) technique as an alternative way to get the geotechnical information, in particular shear-wave (S-wave) velocity information, at a site along an existing rail road. The REMI method uses ambient noises recorded using standard refraction equipment to derived shear-wave velocity information at a site. It does a wavefield transformation on the recorded wavefield to produce Rayleigh wave dispersion curve, which are then picked and modeled to get the shear-wave velocity structure. At this site the vibrations from the running trains provided strong noise sources that allowed REMI to be very effective. REMI was performed along the planned new underground rail tunnel. In addition, Suspension PS logging (SPS) were carried out at selected boreholes along the profile in order to draw out the quantitative relation between the shear wave velocity from the PS logging and the rock mass rating (RMR) determined from the inspection of the cores recovered from the same boreholes, These correlations were then used to relate the shear-wave velocity derived from REMI to RMR along the entire profile. The correlation between shear wave velocity and RMR was very good and so it was possible to estimate the RMR of the total zone of interest for the design of underground tunnel,

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Application of linear-array microtremor surveys for rock mass classification in urban tunnel design (도심지 터널 암반분류를 위한 선형배열 상시진동 탄성파 탐사 적용)

  • Cha, Young-Ho;Kang, Jong-Suk;Jo, Churl-Hyun
    • Geophysics and Geophysical Exploration
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    • v.9 no.1
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    • pp.108-113
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    • 2006
  • Urban conditions, such as existing underground facilities and ambient noise due to cultural activity, restrict the general application of conventional geophysical techniques. At a tunnelling site in an urban area along an existing railroad, we used the refraction microtremor (REMI) technique (Louie, 2001) as an alternative way to get geotechnical information. The REMI method uses ambient noise recorded by standard refraction equipment and a linear geophone array to derive a shear-wave velocity profile. In the inversion procedure, the Rayleigh wave dispersion curve is picked from a wavefield transformation, and iteratively modelled to get the S-wave velocity structure. The REMI survey was carried out along the line of the planned railway tunnel. At this site vibrations from trains and cars provided strong seismic sources that allowed REMI to be very effective. The objective of the survey was to evaluate the rock mass rating (RMR), using shear-wave velocity information from REMI. First, the relation between uniaxial compressive strength, which is a component of the RMR, and shear-wave velocity from laboratory tests was studied to learn whether shear-wave velocity and RMR are closely related. Then Suspension PS (SPS) logging was performed in selected boreholes along the profile, in order to draw out the quantitative relation between the shear-wave velocity from SPS logging and the RMR determined from inspection of core from the same boreholes. In these tests, shear-wave velocity showed fairly good correlation with RMR. A good relation between shear-wave velocity from REMI and RMR could be obtained, so it is possible to estimate the RMR of the entire profile for use in design of the underground tunnel.

Uranium Recovery from Nuclear Fuel Powder Conversion Plant Filtrate and its Thermal Decomposition Characteristics (핵연료분말 제조공정에서 발생된 여액으로부터 우라늄 회수 및 회수된 우라늄 화합물의 열분해 특성)

  • Jeong, Kyung-Chai;Jeong, Ji-Young;Kim, Byung-Ho;Kim, Tae-Joon;Choi, Jong-Hyeun
    • Journal of the Korean Ceramic Society
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    • v.39 no.2
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    • pp.204-209
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    • 2002
  • In this study, $UO_4{\cdot}2NH_4F$, the precipitates which has low solubility, was obtained by chemical precipitation method to recover and reuse the trace uranium from the liquid waste producing in AUC process and for this compound it was characterized by means of chemical analysis, TG-DTA, XRD and FT-IR analyses. This compound was analyzed as $UO_4{\cdot}2NH_4F$ and shape of this precipitate was hexagonal type, having the size of 2∼3 ${\mu}m$. Also, the intermediates were obtained as $UO_4F,\;UO_4,\;UO_3,\;and\;U_3O_8$ by the thermal decomposition over the temperature of 220, 310, 515 and 640$^{\circ}C$, respectively. It is concluded that under the condition of a constant heating rate of 5$^{\circ}C$/min in air atmosphere range of between room temperature and 800$^{\circ}C$, thermal decomposition reaction mechanism of $UO_4{\cdot}2NH_4F$ is as follow; $UO_4{\cdot}2NH_4F{\rightarrow}UO_4F{\rightarrow}UO_4{\rightarrow}UO_3{\rightarrow}U_3O_8$.

Characterization of Crosslinks of Maleic Anhydride-Grafted EPDM/Zinc Oxide Composite Using Dichloroacetic Acid/Toluene Cosolvent and Extraction Temperature (디클로로아세트산/톨루엔 공용매와 추출 온도를 이용한 무수말레산-그래프트 EPDM/산화 아연 복합체의 가교 특성 분석)

  • Kwon, Hyuk-Min;Choi, Sung-Seen
    • Elastomers and Composites
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    • v.48 no.4
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    • pp.288-293
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    • 2013
  • Crosslink characteristics of maleic anhydride-grafted EPDM (MAH-g-EPDM)/zinc oxide composite were investigated by weight losses after dichloroacetic acid (DCA)/toluene cosolvent extraction at different temperatures and by measurement of crosslink densities. The chemical changes were analyzed using attenuated total reflectance-Fourier transform infrared spectroscopy (ATR-FTIR). The weight losses by extraction at high temperature ($90^{\circ}C$) were remarkably greater than those at room temperature and those by DCA/toluene cosolvent extraction were greater than those by toluene one by more than 5 times. The crosslink densities were measured after the solvent extraction, and the second crosslink densities were higher than the first ones. The first crosslink density was lower when the extraction temperature was high, and it was much lower for the toluene extraction than for the DCA/toluene cosolvent extraction. The second crosslink density of the sample extracted with DCA/toluene cosolvent was greater than that extracted with toluene. The extracted components were depending on the extraction solvents and temperatures, for example; only strong crosslinked networks were remained when extracting with DCA/toluene cosolvent at high temperature, while only uncrosslinked polymer chains were extracted when extracting with toluene at room temperature. Therefore, crosslink characteristics of the MAH-g-EPDM/zinc oxide composite can be analyzed by comparison of the extracted components according to the extraction solvents and temperatures and by measurement of successive crosslink densities.

An Electric Load Forecasting Scheme with High Time Resolution Based on Artificial Neural Network (인공 신경망 기반의 고시간 해상도를 갖는 전력수요 예측기법)

  • Park, Jinwoong;Moon, Jihoon;Hwang, Eenjun
    • KIPS Transactions on Software and Data Engineering
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    • v.6 no.11
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    • pp.527-536
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    • 2017
  • With the recent development of smart grid industry, the necessity for efficient EMS(Energy Management System) has been increased. In particular, in order to reduce electric load and energy cost, sophisticated electric load forecasting and efficient smart grid operation strategy are required. In this paper, for more accurate electric load forecasting, we extend the data collected at demand time into high time resolution and construct an artificial neural network-based forecasting model appropriate for the high time resolution data. Furthermore, to improve the accuracy of electric load forecasting, time series data of sequence form are transformed into continuous data of two-dimensional space to solve that problem that machine learning methods cannot reflect the periodicity of time series data. In addition, to consider external factors such as temperature and humidity in accordance with the time resolution, we estimate their value at the time resolution using linear interpolation method. Finally, we apply the PCA(Principal Component Analysis) algorithm to the feature vector composed of external factors to remove data which have little correlation with the power data. Finally, we perform the evaluation of our model through 5-fold cross-validation. The results show that forecasting based on higher time resolution improve the accuracy and the best error rate of 3.71% was achieved at the 3-min resolution.

A Development of Real-time Vibration Monitoring and Analysis System Linked to the Integrated Management System of Ministry of Public Safety and Security (국민안전처 통합관리시스템 연계 가능한 시설물 진동 감지 및 분석 시스템 개발)

  • Lim, Ji-Hoon;Jung, Jin-Woo;Moon, Dae-Joong;Choi, Dong-Ho
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.20 no.3
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    • pp.130-139
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    • 2016
  • A frequency of earthquake occurrence in the Republic of Korea is increasing over the past few decades. In this situation, an importance of earthquake prevention comes to the fore because the earthquake does damage to structures and causes severe damage of human life. For the earthquake prevention, a real-time vibration measurement for structures is important. As an example, the United States of America and Japan have already been monitoring real-time earthquake acceleration for the important structures and the measured acceleration data has been managed by forming database. This database could be used for revising the seismic design specifications or predicting the damage caused by earthquake. In Korea, Earthquake Recovery Plans Act and Enforcement Regulations are revised and declared lately. Ministry of Public Safety and Security is constructing a integrated management system for the measured earthquake acceleration data. The purpose of this research is to develop a real-time vibration monitoring and analysis system for structures which links to the integrated management system. The developed system contains not only a monitoring function to show real-time acceleration data but also an analysis system to perform fast fourier transform, to obtain natural frequency and earthquake magnitude, to show response spectrum and power spectrum, and to evaluate structural health. Additionally, this system is designed to be able to link to the integrated management system of Ministry of Public Safety and Security. It is concluded that the developed system can be useful to build a safety management network, minimize maintenance cost of structures, and prevention of the structural damage due to earthquake.

Photoelectric Properties of PbTe/CuPc Bilayer Thin Films (PbTe/CuPc 이층박막의 광전 특성)

  • Lee, Hea-Yeon;Kang, Young-Soo;Park, Jong-Man;Lee, Jong-Kyu;Jeong, Jung-Hyun
    • Journal of Sensor Science and Technology
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    • v.7 no.1
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    • pp.67-72
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    • 1998
  • The crystallized CuPc and PbTe films are formed by thermal evaporation and pulsed ArF excimer laser ablation. Structural and electrical properties of thin film is observed by XRD and current-voltage(I-V) curves. From XRD analysis, both PbTe and CuPc thin films show a-axis oriented structure. For the measurement of photovoltaic effect, the transverse current-voltage curve of CuPc/Si, PbTe/Si and PbTe/CuPc/Si junctions have been analyzed in the dark and under illumination. The PbTe/CuPc/Si junction exthibits a strong photovoltaic characteristics with short circuit current($J_{sc}$) of $25.46\;mA/cm^{2}$ and open-circuit voltage($V_{oc}$) of 170 mV. Quantum efficiency and power conversion efficiency are calculated to be 15.4% and $3.46{\times}10^{-2}$, respectively. Based on the results of QE and ${\eta}$, the photocurrent process of PbTe/CuPc/Si junction can be explained as following three effective steps; photocarrier generation in the CuPc layer, carrier separation at PbTe/CuPc interface, and finally a transportation of electrons through the PbTe layer.

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