• The Korean Journal of Nuclear Medicine Technology
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• v.16 no.1
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• pp.108-114
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• 2012

Purpose: Immunosorbent assay most commonly used in the laboratory and commercial third-party quality control material is a substance that provided by BIO-RAD. However, in Reference Sheet by radioimmunoassay test kit or a measuring device for the mention of Acceptable Range is somewhat lacking. Radioimmunoassay for the inspection of test results by setting Acceptable Range to increase the objectivity of the recommendations on the data accumulated by the manufacturer listed in the Reference Sheet is to be issued. Materials and Methods : In our hospital since 2009 partially BIO-RAD using quality control materials in 2011, excluding certain items, some items were most of the BIO-RAD third-party quality control materials are used. Thus, internal quality control data accumulated BIO-RAD's Unity Real Time program by using the items were measured. Results : BIO-RAD using quality control material items were about 50 of the 20 Point Data averages, standard deviations, variation coefficients were calculated to measure the Acceptable Range of kit, automated immunoassay attributed Roche Elecsys / E170 / cobas e Systems the measures and compared. Conclusions : BIO-RAD QC materials commonly used hospital and peer group by setting the measurement kit, suitable for laboratory equipment for radioimmunoassay of Acceptable Range manufacturer recommendation to increase the objectivity of the test results by national and international recognition for radioimmunoassay should seek to increase.

• Journal of Radiation Protection and Research
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• v.40 no.4
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• pp.211-215
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• 2015

In case of radiation emergencies, radioactive materials released into environments can cause internal exposure of members of the public. Even though whole body counters are widely used for direct measurement of internally deposited radionuclides, those are not likely to be used at the field to rapidly screen internal exposure. In this study, we estimated the counting efficiencies of portable NaI detector for different size BOMAB phantoms using Monte Carlo transport code to apply handheld gamma spectrometers for rapid screening of internal exposure following radiological accidents. As a result of comparison for two counting geometries, counting efficiencies for sitting model were about 1.1 times higher than those for standing model. We found, however, that differences of counting efficiencies according to different size are higher than those according to counting geometry. Therefore, we concluded that when we assess internal exposure of small size people compared to the reference male, the body size should be considered to estimate more accurate radioactivity in the human body because counting efficiencies of 4-year old BOMAB phantom were about 2.4~3.1 times higher than those of reference male BOMAB phantom.

• Proceedings of the International Union of Geodesy And Geophysics Korea Journal of Geophysical Research Conference
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• 2003.05a
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• pp.16-16
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• 2003

본 연구는 ILP(International Lithosphere Project) Task Group II-4가 진행하고 있는 상부맨틀에 대한 3차원 구조도 작성 연구의 일환으로 수행되어졌으며 구조도 작성을 위한 데이터 베이스의 구조는 task group의 표준안을 따랐다. 기존 문헌과 기존의 데이터 베이스를 통해서 획득된 자료를 이용해 동해와 그 주변을 대상으로 하는 지역의 ($32-45^{\circ}$E, $122-148^{\circ}$N) 상부 670km까지의 3차원 구조도 작성을 위한 초기 모델을 구축하였으며, 이 절차를 최대한 자동화하는 프로그램을 포트란을 이용해 만들어보았다. 연구 지역에 대한 곡율을 계산하기 위해 표준타원체 모델인 WGS84과 geoid undulation 모델인 EGM96을 사용했으며 지형 고도 자료는 GTOPO30, GLOBE 1.0, 그리고 Smith and Sandwell 데이터베이스를 사용하여 지구 중심으로부터 지표까지의 거리를 구하였다. 연구지역은 $0.25^{\circ}$간격으로 나누었으며 총 5777개의 격자점을 정의하였으며 각각의 격자점에 1차원 수직구조를 부여함으로써 3차원 모델을 구축하였다. 그리고 지형적으로나 지질학적으로 유사한 지역을 하나의 구역으로 정의하고 동일한 수직구조를 부여함으로써 모든 격자점에 1차원 수직구조를 정의하지 않도록 하였다. 본 연구에서는 지표 지질은 모델에 고려하지 않았지만 지형학적으로 의미가 있는 분지나 수평적으로 불균질성이 뚜렷한 지역을 중심으로 연구 지역의 리젼을 정의하였다. 중요 리젼에 대한 지각구조에 대해서는 기존의 문헌을 통해 모델치를 정의하였으며 지각 하부부터 상부 670km에 대한 부분은 Task Group에서 제시한 표준 모델을 이용했다. 모델을 정의하기 위해 주어진 격자점에 대한 지구 중심으로부터 지오이드까지의 거리, 지오이드로부터 지표까지의 거리를 정의해주었으며, 각 격자점의 수직구조를 정의하기 위해 깊이에 따른 각 매질의 밀도, P파의 속도, S파의 속도, P파에 대한 Q값, S파에 대한 Q값을 정의 해주었다. S파의 속도를 구하기 위해서 지구 내부 물질을 포아송 매질이라는 가정 하에, 관계식을 $Vp{\;}={\;}SQRT(3){\;}{\times}{\;}Vs$ 이용하였다. 획득한 모델치들을 이용해 동해와 동해 인근 지역에 대한 초기모델을 구축하였다.

• Analytical Science and Technology
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• v.30 no.5
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• pp.287-294
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• 2017

As the demand for natural gas increases with industrial development, the supply of natural gas is expected to become unstable with a shortage of imported natural gas. It is hence necessary to meet this demand by introducing and developing various types of natural gas, such as pipeline natural gas (PNG) and substituted natural gas (SNG), in addition to liquefied natural gas (LNG). The components included in PNG as well as their concentrations must be measured accurately, and a standard gas should be developed to accurately measure hydrocarbons ($C_6-C_{10}$), which are trace components included in natural gas. The components in the primary standard gas mixtures (PSMs) developed in the present study were hexane, heptane, octane, nonane, and decane with concentrations of $10-30{\mu}mol/mol$ with methane as the balance gas. Standard hydrocarbon ($C_6-C_{10}$) gas mixtures were prepared in aluminum cylinders by a gravimetric method with traceability following ISO 6142 with raw material gases, for which the purity of each component was analyzed completely. The prepared standard gas mixtures were analyzed by to evaluate the preparation consistency between the standard gas mixtures, the adsorbability of the cylinders, the variation of the stability, and the uncertainty. The results showed that aluminum cylinders have little adsorptive loss on their internal surfaces with excellent long-term stability. The developed standard gas mixture, containing hexane, heptane, octane, nonane, and decane with concentrations of $10-30{\mu}mol/mol$, showed an uncertainty in a range of 0.79 % - 1.63 %.

• Journal of Korean Society of Environmental Engineers
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• v.34 no.5
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• pp.316-325
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• 2012

In this study, we suggested adequate control technology by analyzing emission process and main chemical of VOC/HAPs generated from four paint factories in Busan area. And we estimated whether Kapok fiber, which is a natural material, can be commercially used for an absorbent by testing adsorption ability. As a result of this sturdy, above 60% of VOC/HAPs was volatilized and dispersed inside the working place without conducting control system of facilities during manufacturing paints. Concentration profile of VOC/HAPs, which is volatile naturally outside the factories, is surveyed above 70% at Toluene, Ethylbenzene, and Xylene. And a result of evaluation of odor attribution level about the component whose Odor Threshold is known, it is estimated that major cause material of A, B, C factories is Toluene and that of D factory is m/p-Xylene. And that result presented design arguments such as facilities specifications, activated carbon filling volume, and replace cycle of activated carbon as control technology. Also, that result presented emission process improvement such as adsorption of central-controlled ventilation device, installation of inlet flenge, and potable cleaning process. The rate of pollutant adsorption of Kapok fiber, which is natural material, is indicated about 91.9%, 66.7%. That result validated the possibility as replacement of activated carbon.

• Analytical Science and Technology
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• v.17 no.3
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• pp.263-270
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• 2004

A method is described for the analysis of short-chain alkylphenol ethoxylates (APEOs), 4-octylphenol-di-ethoxylate (OP2EO) and 4-nonylphenol-di-ethoxylate (NP2EO), in drinking water or wastewater using reversed phase high-performance liquid chromatography with electrospray ionization mass spectrometry. The solvent system was water and methanol containing $10{\mu}M$ trifluoroacetic acid as an ionization solvent. We acidified 1 L of water samples to less than pH 2 with concentrated $H_2SO_4$ and loaded onto Sep-Pak $C_{18}$, and eluted with acetone. The calibration of OP2EO and NP2EO was performed for the concentration range from 20 to 500 ng/L and the correlation coefficients were 0.999 and 0.990, respectively. The limits of detection were 20 ng/L (OP2EO) and 50 ng/L (NP2EO) at a signal-to-noise ratio of 3. Accuracy and precision of this analytical method were 85.8 ~ 122.1% and 8.2 ~ 18.8%, respectively. The proposed method allowed a sensitive and rapid detection of OP2EO and NP2EO and it could be applied for monitoring of APEOs from environmental samples.

• Korean Journal of Fisheries and Aquatic Sciences
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• v.34 no.6
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• pp.617-623
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• 2001

To predict the seasonal variation of dissolved oxygen (DO) in Hakata bay, Japan, possible 20 time-series of different hourly-solar-radiation intensities were generated based on stochastically changing solar radiation intensity, and a numerical simulation on dissolved oxygen (DO) was carried out for each time series by using the Sediment-Water Ecological Model (SWEM). The model, consisting of two sub-models with hydrodynamic and biological models, simulates the circulation process of nutrient between water column and sediment, such as nutrient regeneration from sediments as well as ecological structures on the growth of phytoplankton and zooplankton, The results of the model calibration followed the seasonal variation of observed water quality well, and generated cumulative-frequency-distribution (CFD) curves of daily solar radiation agreed well with observed ones, The simulation results indicated that the exchange of sea water would have a great influence on the DO concentration, and that the concentration could change more than 1 mg/L in a day. This prediction method seems to be an effective way to examine a solution to minimize fishery damage when DO is depleted.

• Journal of Radiation Protection and Research
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• v.7 no.1
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• pp.1-10
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• 1982

For the purpose of establishment of Reference Korean and estimation of internal and external exposure doses in the Reference Korean, we have surveyed reference values for Koreans, such as physical standards including height, weight and body surface area, food consumption rate of daily intake of radioactive substances and exposure dose from natural radiation. The results obtained are as follows: 1) The age group of the Reference Korean ranged from 20 to 30 years old in both sexes. The height, weight and surface area of the body of the Reference Korean are 167cm, 61kg and $1.67m^2$ in male and 155cm, 51kg and $1.51m^2$, respectively in female. 2) The food consumption of the Korean is 812.8g (669.6g of vegetable food and 143.2g of animal food) per capita per day. 3) Koreans are taken about 1,200 pCi of radioactive substances(${\beta}$-ray) per capita per day. 4) The external and internal radiation exposure doses of the Korean are estimated to be 127 mrem and 8 mrem per year, respectively. However, it is believed that these values will be modified upon the addition of data collection.

• Korean Journal of Food Science and Technology
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• v.32 no.5
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• pp.1015-1021
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• 2000

Volatile flavor components (VFCs) in cooked black rices (Suwon-415 and Chindo) were studied. The major reactions during cooking, which result in aroma volatiles, are the Maillard reaction between amino acids and reducing sugars, and thermal degradation of lipid. Black rices washed with water were soaked in 1.5 folds water and heated at $110^{\circ}C$ in oil bath for 30min. VFCs in cooked black rices were extracted for three hours by SDE and were analyzed by GC and GC/MS. A total of 91, 82 volatiles were identified in Suwon-415 and Chindo black rice, respectively. Suwon-415 was composed of 26 alcohols, 10 aldehydes, 5 acids, 11 esters, 15 ketones, 9 hydrocarbons, 3 furans, 3 nitrogen containing compounds and 9 sulfur containing compounds. Chindo was composed of 28 alcohols, 9 aldehydes, 4 acids, 12 esters, 14 ketones, 5 hydrocarbons, 3 furans, 3 nitrogen containing compounds and 4 sulfur containing compounds.

• Analytical Science and Technology
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• v.28 no.2
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• pp.125-131
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• 2015

A method was developed and fully validated for the determination of terbutaline, a β₂-receptor agonist, in human plasma. Plasma samples were prepared by solid-phase extraction with Sep-Pak silica, followed by high-performance liquid chromatography (HPLC). The terbutaline was pre-separated from the interfering components in plasma on a Luna C18 (2) column, and terbutaline and salbutamol as an internal standard were resolved and determined on a Luna Silica column. The two columns were connected by a switching valve equipped with silica pre-column. The pre-column was used to concentrate the terbutaline in the eluent from the C18 column before back-flushing onto the silica column with fluorescence detection at an excitation/emission wavelength of 276/306 nm. The method was shown to be specific by testing six different human plasma sources. Linearity was established for a concentration range of 0.4-20.0 ng/mL with a correlation coefficient of 0.9999. The lower limit of quantitation was 0.4 ng/mL with a precision of 10.1% as C.V.%.