• Title/Summary/Keyword: 고온극복

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An Investigation of In Situ TEM Heating Experiments of Powder Samples (분말 시료의 투과전자현미경 직접 가열 실험법 연구)

  • Kim, Youn-Joong;Jeung, Jong-Man;Lee, Young-Boo;Lee, Su-Jeong;Song, Ji-Ho
    • Applied Microscopy
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    • v.31 no.4
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    • pp.315-323
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    • 2001
  • In situ TEM heating experiments utilizing kaolinite powder samples result in the following facts. (1) The water recirculation system adopted in the Gatan's heating holder is required to prevent specimen drift above $500^{\circ}C$. (2) Since the degree of phase changes depends on the thickness of powders below $600^{\circ}C$, examinations of both thin and thick specimens are required. (3) Sample preparation using Mo-grids is required for TEM heating experiments above $900^{\circ}C$. At these temperature ranges the effect of heating rate and holding time on the phase transition process increases drastically, so that a programmed temperature control is required. (4) TEM heating experiments of the embedded powders by epoxy for the cross-sectional view was limited due to the severe epoxy movement during heating above $300^{\circ}C$. Better methods of sample preparation are required to overcome this problem.

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Stable Production Technique of Paprika (Capsicum annuum L.) by Hydrogen Peroxide Treatment at Summer (여름철 과산화수소를 이용한 파프리카(Capsicum annuum L.) 안정생산기술)

  • Cho, Ill-Hwan;Lee, Woo-Moon;Kwan, Ki-Bum;Woo, Young-Hoe;Lee, Kwan-Ho
    • Journal of Bio-Environment Control
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    • v.18 no.3
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    • pp.297-301
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    • 2009
  • Hydrogen peroxide, which is used in various crops as an oxidizer to improve high temperature adaptation, was evaluated on the effects on productivity and disease incidence in paprika (Capsicum annuum L.) by periodic leaf spray at summer. Hydrogen peroxide treatment not only increased the leaf thickness and SPAD (chlorophyll content) but also the fruit set numbers per plant by 2. Hydrogen peroxide content increase in leaf resulted in increase of catalase and peroxidase activities, and the powdery mildew disease (Leveillula taurica) was also suppressed by the treatment. Transpiration was improved by the reduced leaf stomata resistance in the hydrogen peroxide treatment. Therefore, hydrogen peroxide leaf spray is recommended for improvement of summer productivity in paprika.

Micromechanical Model for the Consolidation Behavior in SiC-Ti Metal Matrix Composites (SiC-Ti금속기 복합재료의 강화거동에 관한 미시역학적 모델)

  • 김준완;김태원
    • Composites Research
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    • v.16 no.3
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    • pp.1-8
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    • 2003
  • Densification occurs by the inelastic flow of the matrix materials during the consolidation processes at high temperature for MMCs, and the results depend on many process conditions such as applied pressure, temperature and volume fraction of fiber and matrix materials. This is particularly important in titanium matrix composites since material failure may occur by either the applied conditions or microstructural parameters through the processes, and thus a generic model based on micro-mechanical approaches enabling the evolution of density over time to be predicted has been developed. The mode developed is then implemented into FEM so that practical process simulation has been carried out. Further the experimental investigation of the consolidation behavior of SiC/Ti-6Al-4V composites using vacuum hot pressing has been performed, and the results obtained are compared with the model predictions.

Trends on the Development of Carbon Nanotube-Based Digital X-ray Tube (탄소나노튜브 기반 디지털 엑스선 튜브 기술개발 동향)

  • Song, Y.H.;Kang, J.T.;Kim, J.W.;Choi, Y.C.;Park, S.;Jeong, J.W.
    • Electronics and Telecommunications Trends
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    • v.31 no.2
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    • pp.116-123
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    • 2016
  • 병원의 X선 및 CT 영상, 반도체 소자 내의 결함분석, 공항의 보안검색 등 다양한 분야에 X선이 사용되고 있다. 지금까지는 이러한 X선을 발생시키기 위해 고온으로 가열하여 전자를 방출시키는 열전자원이 사용됐으나, 높은 소비전력과 디지털 구동의 어려움 등의 단점이 존재한다. 이러한 한계를 극복하기 위해 전계방출원 기술, 특히 탄소나노튜브를 이용한 나노전자원의 제조 및 디지털 엑스선 튜브 응용 기술에 관한 연구가 최근 활발히 진행 중이다. 이 글을 통해 디지털 시대에 부합하는 탄소나노튜브 기반 나노전자원 및 이를 이용한 디지털 엑스선 튜브의 개념 및 제조기술을 소개하고, ETRI 및 다른 기관들에서 개발 중인 최신 기술개발 동향을 소개하고자 한다.

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Preparation of Inorganic Membrane for H$_2$ Separation by 2-step Silica Sol-Gel method (2단계 실리카 솔-젤법을 이용한 수소분리용 무기재료막의 제조)

  • 소재현;양승만;박승빈
    • Proceedings of the Membrane Society of Korea Conference
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    • 1996.10a
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    • pp.55-57
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    • 1996
  • 다공성 무기막은 높은투과도와 뛰어난 내열.내화학성, 그리고 경제성 때문에 기존의 PSA공정이나 증류와 같은 고에너지 분리공정을 대체하는 공정으로 각광을 받고 있다. 무기재료막의 제조하는 방법으로 주로 알콕사이드를 사용하는 솔-젤법(1)과 금속(2) 또는 기상반응(3)을 이용하는 화학증착법이 사용된다. 또한 고온에서 수소를 연속적으로 분리하여 화학평형에 기인한 한계를 극복하여 높은 수율을 얻고자하는 막반응기에 관한 연구가 활발히 진행되고 있다. 본 연구에서는 $\alpha$-알루미나 지지체의 미세한 다공성 구조 내부에서 TEOS(Tetraethylorthosilicate)와 산성의 알코올-물 혼합물을 확산시켜 실리카 솔을 생성시킴과 동시에 젤화시켜 기공의 크기를 감소시켜 막을 제조하였다. 이렇게 제조된 막은 높은 투과도와 낮은 수소선택도(selectivity=3-4)를 보였고, 두번째 단계로 silica sol을 제조하여 진공 하에서 dip-coating을 행하였다. 이렇게 2단계로 기공 구조를 개선시킨 실리카 막은 저압에서 상대적으로 높은 수소의 분리도(selectivity=5-7)를 보였으며 여전히 높은 투과도를 갖는다.

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Thermal Stability Improvement of Nickel-Silicide using PAI in the N-type Substrate (N-type 기판에서 PAI에 의한 Nickel-Silicide의 열안정성 개선)

  • 윤장근;지희환;오순영;배미숙;황빈봉;박영호;왕진석;이희덕
    • Proceedings of the IEEK Conference
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    • 2003.07b
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    • pp.675-678
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    • 2003
  • 본 논문에서는 N-type 기판에서 Nickel-Silicide를 적용하였을 경우에 나타나는 문제점과 PAI (Pre-amorphization Implant)의 효과에 대하여 알아보았다. N-type 기판에 RTP (Rapid Thermal Process)를 통하여 Nickel-Silicide 를 형성하게 되는데, 여기까지는 안정한 Nickel mono-Silicide (NiSi)가 형성됨을 확인하였다. 하지만 후속 열처리 공정 후 심한 응집 현상 (Agglomeration)과 이상 산화 현상 (Abnormal Oxidation Phenomenon), Silicide Island 등 열안정성 (Thermal Stability) 측면에서 여러 가지 많은 문제점들이 나타났다. 이 후속 열처리의 열안정성 취약점들을 극복하는 방안으로 Ge 및 N₂ PAI를 적용하였다. PAI를 적용하였을 경우에는 그렇지 않은 경우에 비하여 고온 열처리 후에도 면저항이 비교적 잘 유지되었으며, 두께가 얇고 안정한 Nickel-Silicide 특성을 확보할 수 있었다. 특히 Ge PAI 에 비하여 N₂ PAI 의 경우가 보다 특성 개선 효과가 크게 나타났다.

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Design of Electric Vehicle Traction Motor using Induction Motor (유도전동기를 사용한 전기자동차 구동용 전동기 설계)

  • Koo, Bonkil;Nam, Kwanghee
    • Proceedings of the KIPE Conference
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    • 2015.11a
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    • pp.109-110
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    • 2015
  • 전기자동차 구동용 전동기는 고토크/고파워 밀도, 고효율, 넓은 구동속도 범위의 특징을 가져야 한다. 영구자석 매입형 동기전동기는 이러한 특성에 가장 부합하는 전동기 형태로서 전기자동차 구동용 전동기로 각광받고 있다. 하지만 강한 자속밀도를 얻기 위하여 희토류 영구자석을 사용해야 하고, 이는 생산단가의 절감문제, 고온에서의 비가역적 감자문제, 인버터 결함 시의 안전성 문제 등의 문제점을 갖고 있다. 이러한 문제들을 극복하기 위하여 전기자동차 구동용 유도전동기 설계를 제안한다. 유도전동기가 가지는 장점들과 함께 설계 시 고려해야 할 내용들을 제시한다.

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Effects of Cutting Management during Summer Season on Growth and Reserve Carbohydrates of Orchardgrass (고온기 예취방법이 Orchardgrass의 생장 및 탄수화물 축적에 미치는 영향)

  • 김정철;최기춘;김광현;김우복
    • Journal of The Korean Society of Grassland and Forage Science
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    • v.13 no.4
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    • pp.257-267
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    • 1993
  • Optimum pasture management during the summer season is an important factor to maintain good regrowth and persistence of pasture. The field experiment was carried out to investigate the effects of cutting management on growth and reserve carbohydrates in stubble. and on dry matter yield of orchardgrass dominated pasture during the mid-summer season. Three different cutting times(July 15, 25 and August 5) as a main plot and three cutting heights(3, 6 and 10cm) as a sub plot were disigned with three replications. The experiment was done at pasture of Changsung Agricultural High School in 1988. The results obtained were summarized as follows: 1. Temperature of soil surface and underground in the cutting of July 15 and July 25 was not showed significantly different, because of low intensity of radiation with a run of wet weather, and that of August 5 cutting tends to be lowed in high cutting height during the mid-summer season. 2. Amount of soil moisture against cutting height showed that high cutting had a low content. 3. Growth rate against regrowth of plant height, lear length and leaf area showed to be fast in high cutting. 4. Rapid recovery period of carbohydrate content after cutting and large amount of carbohydrate accumulation were showed in the cutting of July 15 and 25 compared with August 5 cutting in the reserve carbohydrate content against cutting of time and height during the mid-summer season. 5. Dry matter yield of the 4th and 5th cutting showed to be remarkable in July 15 cutting compared to those of July 25 and August 5. From the above results, it is suggested that the 10cm cutting height during the mid-summer season is the most effective for good regrowth, reserve carbohydrates and dry matter yield of orchardgrass.

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Development of Thermoplastic Carbon Composite Bipolar Plates for High-temperature PEM Fuel Cells (고온 양성자 교환막 연료전지용 열가소성 탄소 복합재료 분리판 개발)

  • Lim, Jun Woo;Kim, Minkook;Lee, Dai Gil
    • Composites Research
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    • v.29 no.5
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    • pp.243-248
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    • 2016
  • Although thermoset carbon fiber composite bipolar plates not only have high mechanical properties but also high corrosion resistance in acid environment, high manufacturing cost and low bulk electrical conductivity are the biggest obstacle to overcome. In this research, thermoplastic polymer is employed for the matrix of carbon composite bipolar plate to increase both the manufacturing productivity and bulk electric conductivity of the bipolar plate. In order to increase the electrical conductivity and strength, plain type carbon fabric rather than chopped or unidirectional fibers is used. Also nano particles are embedded in the thermoplastic matrix to increase the bulk resistance of the bipolar plate. The area specific resistance and the mechanical strength of the developed bipolar plate are measured with respect to the environmental temperature and stack compaction pressure.

Carbon Fiber/Aluminum Composite Fabrication Using Wettability Control (젖음성 제어를 이용한 탄소섬유/알루미늄 복합재료 제조)

  • Lee, Yongbeom;Park, Sangjin;Han, Jun Hyun
    • Composites Research
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    • v.28 no.5
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    • pp.254-259
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    • 2015
  • Carbon fiber/aluminum (CF/Al) composites were successfully fabricated without pressure casting using wettability modification of carbon fiber. The wettability of liquid aluminum on carbon fibers was enhanced through electroless plating of copper on carbon fibers. Liquid aluminum was well infiltrated into carbon fiber bundles with Cu coating layer due to low wetting angle, and a lot of pores that existed in CF/Al composite without Cu coating on CF were greatly removed. However, a few tiny pores existed in carbon fiber bundles, which is due to not bad wettability between CF and Al but shrinkage cavity that was generated during cooling of CF/Al composite. The tiny pores could be effectively removed by a subsequent rolling.