• The korean journal of orthodontics
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• v.33 no.5 s.100
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• pp.359-370
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• 2003

The purpose of this study was to evaluate the bond strength of orthodontic brackets bonded to metal bar with chemically cured adhesive (Ortho-one, Bisco Co, USA) in various types and directions of force application. Three types of metal bracket with different bracket base configurations; Micro-Loc base(Tomy Co, Japan), Chessboard base(Daesung Co, Korea), Non-etched Foil-Mesh base(Dentaurum, Germany); were used in this study. Peel, shear, tensile bond strengths were measured by universal testing machine and compared each other. The peel force directions applied were $0^{\circ},\;15^{\circ},\;30^{\circ},\;45^{\circ},\;60^{\circ},\;75^{\circ},\;90^{\circ}$ And then, in consideration of the different surface area of the bracket bases, the bond strength Per unit area were calculated and compared. The results obtained were summarized as follows: 1. The bond strengths according to the types and the directions of the forces were greatest at the shear forces in all three bracket base configuration groups(p<0.01). 2. As the peel force direction grew higher in degree, peel bond strength decreased. The Patterns of peel bond strength change according to force direction was similar in all three bracket base configurations. The minimum bond strength was 60 degree-peel bond strengths in all three bracket base configurations. 3. In Micro-Loc base group, minimum peel bond strength$(_{60}PBS)$ was in $29\%$ level of shear bond strength and $52\%$ level of tensile bond strength. In Chessboard base group, $_{60}PBS$ was in $34\%$ level of shear bond strength and $61\%$ level of tensile bond strength. In Non-etched Foil-Mesh base group, $_{60}PBS$ was in $34\%$ level of shear bond strength and $55\%$ level of tensile bond strength. 4. The bond strengths per unit area were lowest in Non-etched Foil-Mesh base group and highest in Chessboard base group(p<0.05). However, there were no differences in shear bond strength, tensile bond strength, $75^{\circ}\;and\;90^{\circ}$ per unit area between Micro-Loc and Chessboard base groups.

• Journal of Technologic Dentistry
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• v.38 no.4
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• pp.273-280
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• 2016

연구목적: 본 연구의 목적은 통상적으로 사용되는 글라스 세라믹과 고분자를 침투시킨 지르코니아 소재로 제작된 코어와 레진 시멘트의 굴곡강도 및 결합강도를 비교하여 하이브리드 기술이 치과 재료의 물리적인 성질에 미치는 영향을 조사하기 위함이다. 연구방법: 본 두 가지의 통상적으로 사용되는 세라믹소재[Vita PM9(GC) and I-JAM(ZC)] 와 다른 두 가지 하이브리드 세라믹 소재 [CELTRA Duo(ZRC) and Vita Enamic(RIZ)] 를 평가하였다. 각 그룹의 소재를 선택하여 결합강도와 굴곡강도, 그리고 scanning electron microscopy(SEM)을 이용하여 표면분석을 시행하였다. 도출된 결과 데이터는 일원분산분석(One-way ANOVA)을 통해 분석되었으며, 제1종 오류의 수준은 0.05로 하였다. 연구결과: RIZ 그룹에서 가장 높은 결합강도를 보였으며(p<0.05), ZC 그룹이 가장 낮은 결과를 보였다. 상대적으로 굴곡강도는 ZC 그룹이 가장 높은 수치를 나타내었으며, RIZ 그룹이 가장 취약했다. 연구결론: 하이브리드 기술로 제작된 소재(RIZ 그룹)는 우수한 레진 시멘트와의 결합강도를 보였지만, 그에 비해 굴곡강도는 상대적으로 통상적인 지르코니아 소재보다 비교적 취약한 결과를 보였다.

• The korean journal of orthodontics
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• v.29 no.5 s.76
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• pp.599-611
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• 1999

The purpose of this study was to evaluate shear, tensile and shear/tensile combined bond strengths(SBS, TBS, S/TBS) in various orthodontic brackets bonded to human teeth with chemically cured adhesive (Ortho-one, Bisco, USA). Five types of metal brackets with various bracket base configurations (Micro-Loc base(Tomy, Japan), Chessboard base(Daesung, Korea), Non-Etched Foil Mesh base(Dentarum, Germany), Micro-Etched Foil Mesh base(Ortho Organiners, USA), Integral base(Unitek, USA)) were used in this study. Shear, tensile and shear/tensile combined bond strengths according to the direction of force were measured by universal testing machine. The bracket base surface after bond strength test were examined by stereoscope and scanning electron microscope. The assessment of resin remnant on bracket base surface was carried out by ARI(adhesive remnant index). The results obtained were summarized as follows, 1. In all brackets, SBS was in the greatest value(p<0.05), TBS was in 50% level and S/TBS was in 30% level of SBS. 2. In bond strength, Micro-Loc base bracket showed the maximum bond strength($SBS:22.86{\pm}1.37kgf,\;TBS:11.37{\pm}0.42kgf,\;S/TBS:6.69{\pm}0.34kgf$) and Integral base bracket showed the minimum bond strength($SBS:10.52{\pm}1.27kgf,\;TBS:4.27{\pm}1.08kgf,\;S/TBS:2.94{\pm}0.58kgf) (p<0.05). 3. In bond strength per unit area, Integral base bracket showed the minimum value, Micro-Loc base and Chessboard base brackets were in similar value(p>0.05). Non-Etched Foil Mesh base and Micro-Etched Foil Mesh base bracket were similar in SBS and TBS(p>0.05), but Micro-Etched Foil Mesh base bracket was greater than Non-Etched Foil Mesh base bracket in S/TBS(p<0.05). 4. Bond failure sites were mainly between bracket base and adhesive, therefore ARI scores were low.

• The Journal of the Korea Contents Association
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• v.15 no.9
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• pp.384-394
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• 2015

The purpose of this study was to evaluate the push-shear bond strength between five commercial zirconia veneering ceramics and zirconia core cylinder, and to investigate the effect of biaxial flexural strength and zirconia liner glass treatments. The biaxial flexural strengths of the veneering ceramics were evaluated by a piston-on-three-ball test. The bond strengths between the Y-TZP cylinder and zirconia veneering ceramics were evaluated using the push-shear bond strength test. The data was analyzed using two-way ANOVA and Scheffe's test. The biaxial flexural strength of Cercon ceram kiss (CE) was higher than those of the other groups. The glass-treated and Triceram zirconia groups showed the highest value and the Creation ZI(CR) showed the lowest. In all groups, the liner glass treatment groups showed significantly higher push-shear bond strength than those without(P<0.05). The liner glass treatments of zirconia can improve the bond strength between the zirconia ceramic core and veneering ceramics.

• The korean journal of orthodontics
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• v.30 no.5 s.82
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• pp.625-642
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• 2000

The purpose of this study is to evaluate the effects of mechanical and thermal fatigue stress on the shear, tensile and shear-tensile combined bond strengths(SBS, TBS, CBS) in various orthodontic brackets bonded to human premolars with chemically cured adhesive(Ortho-one, Bisco, USA). Five types of commercially available metal brackets with various bracket base configurations of Photoetched base(Tomy, Japan), Non-Etched Foil Mesh base(Dentaurum, Germany), Micro-Etched Foil Mesh base(Ortho Organizers, USA), Chessboard base(Daesung, Korea), and Integral base(3M Unitek, USA) were used. Samples were divided into 3 groups, the first group was acted with shear-tensile combined loads($45^{\circ}$) of 200g for 4 weeks(mechanical fatigue stress), the second group was subjected to the 5,000 thermocycles of 15 second dwell time each in $5^{\circ}C\;and\;55^{\circ}C$ baths(thermal fatigue stress), and the third group was the control. Bond strengths were measured at the crosshead speed of 0.5mm/min. The cross-section of bracket base/adhesive interface and the fracture surface were examined with the stereoscope and the scanning electron microscope. The resin remnant on bracket base surface was assessed by ART(Adhesive Remnant Index). The obtained results were summarized as follows, 1. In static bond strength, Photoetched base bracket showed the maximum bond strength and Integral base bracket showed the minimum bond strength(p<0.05). In all brackets, shear bond strength(SBS) was in the greatest value and shear-tensile combined strength(CBS) was in the least value(p<0.05). 2. After mechanical fatigue test, Photoetched base bracket showed the maximum bond strength and Integral base bracket showed the minimum bond strength(p<0.05). In Photoetched base bracket and Micro-Etched Foil Mesh base bracket, shear bond strength(SBS), tensile bond strength(TBS) and shear-tensile combined strength(CBS) were decreased after mechanical fatigue test(p

• Restorative Dentistry and Endodontics
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• v.29 no.1
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• pp.13-22
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• 2004

본 연구는 치수강 상아질 부위 및 상아질 접착제 종류에 따른 결합 강도를 측정하고 이들 사이의 상관관계를 구명하고자 시행되었다 45개의 대구치를 포매 후, 대조군에서는 교합면 법랑질 제거 후 ＃600 SiC paper까지 순차연마하여 상아질을 노출시켰고, 실험군에서는 치수강 개방 후 1시간동안 NaOCl에 보관 후 axial wall과 pulpal floor를 노출시켰다. 노출된 상아질 면에 상아질 접착제를 적용한 후 Z-100을 충전한 다음 40초간 광중합하였다. 사용된 상아질 접착제는 Scotchbond Multi-Purpose와 Single Bond, Clearfil SE Bond였다. $37^{\circ}C$ 증류수에 24시간 보관 후, 저속 diamond saw를 이용하여 0.7mm 두께로 수직절단하고 고속 diamond point(#104)로 단면적 $1{mm}^2$가 되도록 시편을 제작하고, Universal testing machine에서 미세인장 결합강도를 측정하였다. 1. 모든 상아질 접착제의 미세인장강도는 대조군, axial wall군, pulpal floor군 순으로 감소하는 경향을 보였다. 2. 대조군에서 SM과 BB는 SE에 비해 유의성 있게 높은 결합강도를 나타내었다(p<0.05). 3. SM과 SB는 대조군에 비해 axial wall군과 pulpal floor군에서 유의성있게 낮은 결합강도를 보였으나, SE에서는 pulpal floor군만이 유의성 있게 낮은 결합강도를 보였다(p<0.05). 4. Axial wall군과 pulpal floor군에서는 상아질 접착제의 종류에 따른 유의차를 보이지 않았다. 5. 전자현미경 소견에서는 대조군에 비해 axial wall군과 pulpal floor군이 더 부드러운 접착 계면을 나타내었다. 혼성층의 두께는 결합강도의 감소와는 관련이 없었다.

• Restorative Dentistry and Endodontics
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• v.36 no.1
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• pp.50-58
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• 2011

Objectives: The purpose of this study was to compare the microshear bond strength (uSBS) of two totaletch and four self-etch adhesive systems and a flowable resin to enamel. Materials and Methods: Enamels of sixty human molars were used. They were divided into one of six equal groups (n = 10) by adhesives used; OS group (One-Step Plus), SB group (Single Bond), CE group (Clearfil SE Bond), TY group (Tyrian SPE/One-Step Plus), AP group (Adper Prompt L-Pop) and GB group (G-Bond). After enamel surfaces were treated with six adhesive systems, a flowable composite resin (Filek Z 350) was bonded to enamel surface using Tygon tubes. the bonded specimens were subjected to uSBS testing and the failure modes of each group were observed under FE-SEM. Results: 1. The uSBS of SB group was statistically higher than that of all other groups, and the uSBS of OS, SE and AP group was statistically higher than that of TY and GB group (p < 0.05). 2. The uSBS for TY group was statistically higher than that for GB group (p < 0.05). 3. Adhesive failures in TY and GB group and mixed failures in SB group and SE group were often analysed. One cohesive failure was observed in OS, SB, SE and AP group, respectively. Conclusions: Although adhesives using the same step were applied the enamel surface, the uSBS of a flowable resin to enamel was different.

• 대한치과보철학회:학술대회논문집
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• 1996.11a
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• pp.103-103
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• 1996

• Restorative Dentistry and Endodontics
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• v.29 no.1
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• pp.1-12
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• 2004

이 연구는 발거 소구치에서 5급 와동을 형성하여 접착 시스템 및 와동 위치에 따른 상아질에 대한 접착시스템의 미세 인장결합강도의 차이를 비교, 연구하였다. 접착방법은 resin-modified glass ionomer(Gl), compomer(부식여부에 따라 DE 및 DN군으로 분류), 그리고 상아질 접착제인 Single Bond(SB) 및 Cleayfil SE Bond(SE)와 복합레진(Clearfil AP-X)을 사용한 5개의 실험군으로 분류하였다. 소구치 협측 치경부에 wedge형태의 와동을 형성하고 5종의 접착 시스템을 제조자의 지시에 따라 적용, 충전하여 시편을 제작하여 미세인장결합강도를 측정하고, One-way ANOVA / Duncan's test로 통계분석하였다. SEM 검사는 미세인장결합강도의 시편제작과 동일한 방법으로 시편을 제작한 후 관찰하였다. 실험 결과, 상아질 접착제 및 복합레진(SB, SE)의 미세인장결합강도가 GI보다 높게 나타났고(p<0.05), 치은측이 교합측보다 더 낮게 나타났으며, CI, DE, SE에서 유의성 있게 낮게 나타났다(p<0.05). Compomer에서 conditioning 여부(DN, DE)에 따른 변화는 치은측에서만 유의차 있는 것으로 나타났다. SEM 관찰에서, 교합측의 상아세관은 결합 계면과 평행하게 주행하였고, 치은측에서는 결합계면에 수직으로 주행하는 것으로 관찰되었다.

• Journal of the Korean Wood Science and Technology
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• v.33 no.6 s.134
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• pp.38-45
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• 2005

This research was investigated on the increase in strength capacity among different five wood-to-wood connections. Group using small diameter bolts with equal area loss has the highest increase in strength capacity, secondly the group inserted plywood, thirdly the group used glued bolt, and lastly the group inserted rubber plate. These groups showed at least 10% increase in strength capacity more than existing connection groups. Therefore, these results can be applied to develop the new highly efficient connection. To select suitable connection configuration and materials, however, economical advantage and increase in strength capacity and the difficulty should be considered by the additional works.