• Proceedings of the Korean Institute of Surface Engineering Conference
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• 2018.06a
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• pp.110-110
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• 2018

여러 니켈합금 중 인코넬 600은 원전 가압경수로(PWR)의 튜브 재료로 널리 사용되는 재료이다. 스테인리스강과 비교하여 우수한 내식성과 기계적 특성으로 인해 화학설비, 발전설비, 그리고 해양설비 등과 같은 여러 산업분야에서도 널리 사용되고 있다. 그러나 가압경수로용 증기 발생기의 튜브 재료와 같은 특수 환경에서 예민화에 따른 입계부식 및 입계응력부식 등의 문제가 흔히 보고되고 있다. 이러한 내구성 문제는 설비 및 장비의 수명, 내구성 그리고 안정성 등의 치명적인 영향을 미친다. 따라서 용접, 열처리, 그리고 가공과정에서 발생하는 Inconel 600의 예민화 및 입계부식에 관한 연구가 활발히 진행되고 있다. 그러나 100시간 이상 장시간 열화된 시편에 대한 예민화 연구는 전무한 실정이다. 본 연구에서는 장시간 열화된 Inconel 600의 예민화를 평가하기 위해 최대 1,000시간까지 열화를 실시하였으며, 이에 대한 평가방법으로 Double-Loop Electrochemical Potentiokinetic Reactivation(DL-EPR) 시험법을 적용하였다. 본 실험에서 사용된 인코넬 600의 화학성분(wt, %)은 0.01 C, 0.05 Si, 0.14 Mn, 15.3 Cr, 0.5 Cu, 0.015 S, 그리고 나머지는 Ni 이다. 예민화 평가를 위한 등온 열화는 전기열처리로를 이용하여, $550^{\circ}C$와 $650^{\circ}C$에서 최대 1000시간까지 실시하였다. 열화에 따른 미세조직 변화는 scanning electron microscope와 energy dispersive x-ray spectroscopy를 이용하여 실시하였다. DL-EPR 실험은 $25^{\circ}C$의 0.1M $H_2SO_4$ + 0.001M KSCN(potasium thiocyanate) 수용액 하에서 실시하였으며, 분극은 OCP로부터 600 mV(SSE vs.)까지 1.67mV/s 주사속도로 forward scan을 실시 후, 동일한 속도로 OCP까지 reverse scan을 실시하였다. Degree Of Sensitization(DOS)값은 anodic scan peak($I_a$) 값과 reverse scan peak($I_r$) 값의 비로 산출하였다. $$i.e.\;DOS=I_r/I_a{\times}100$$. 그 결과, 온도 변수에 따른 Inconel 600강의 예민화 거동은 서로 상이한 경향을 나타내었다. $550^{\circ}C$의 경우, 열화가 진행됨에 따라 DOS값은 급격하게 증가하는 경향을 나타냈다. 반면, $650^{\circ}C$에서는 일정시간 이후부터 Cr 확산 현상에 의한 탈 예민화 현상이 관찰되었다.

• Proceedings of the Korean Institute of Surface Engineering Conference
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• 2018.06a
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• pp.112-112
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• 2018

알루미늄 합금은 내구성과 내식성이 우수한 경량 재료이다. 그 중 Al-Mg계 5083 Al 합금은 가공성 및 용접성이 우수하여 선체 재료로 널리 이용되고 있다. 이는 선체 중량의 경량화로 인해, 연료비 절감과 빠른 선속 등 다양한 이점을 지니기 때문이다. 그러나 선박의 고속화에 따라 선체에 가해지는 유체충격이 증가하고, 압력 저하에 기인하여 캐비테이션-침식 손상이 증가할 뿐만 아니라, 염소이온이 존재하는 해수환경에서는 침식과 부식의 시너지효과로 인하여 재료의 손상이 더욱 가속화된다. 이에 대한 다양한 방지책들이 제안되고 있으나, 강한 충격압을 동반한 캐비테이션 침식-부식 복합 손상 환경에서는 다소 한계가 있다. 따라서 본 연구에서는 알루미늄 5083에 대하여 캐비테이션 환경 하에서 일정 전위를 인가하며 침식-부식 손상이 최소화 되는 전위 구간을 규명하고자 하였다. 먼저, 분극 실험을 선행하여 재료의 전기화학적 거동을 파악 한 후 적용 전위구간을 선정하여, 해당 전위를 인가한 상태에서 캐비테이션 실험을 실시하였다. 전기화학적 분극실험과 캐비테이션-전기화학 복합 실험은 $25^{\circ}C$의 해수 하에서 실시하였으며, 시험편의 노출면적은 $3.24cm^2$으로 하였다. 분극 실험은 개로전위로부터 +3 V까지 2 mV/s의 분극속도로 전위를 인가하였고, 기준전극으로 Ag/AgCl, 대극으로 백금전극을 사용하였다. 캐비테이션-전기화학 복합 실험은 정전위를 인가한 상태에서 대향형 진동법으로 진동수 20 kHz, 진폭 $30{\mu}m$ 진동을 20분간 가하였으며, 혼팁과 시험편 사이의 거리는 1 mm로 일정하게 유지하였다. 실험 후 표면 손상의 정량적 분석을 위해 인가된 전위별 전류밀도를 비교하고, 무게감소량을 측정하였으며, 손상경향 파악을 위하여 3D광학현미경과 주사전자현미경(SEM)을 통해 표면을 분석하였다.

• Journal of the Korean Society for Aeronautical & Space Sciences
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• v.30 no.6
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• pp.107-115
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• 2002

A parametric study has been conducted to evaluate the effects of finite element modeling methods on the internal loads, sizing and the weight of the multi-spar aircraft wing structures. The wing is idealized into total 18finite element models and subjected to 4typical external load conditions. An automatic sizing algorithm based on MSC/NASTRAN and MSC/PATRAN is developed. The results show that the critical part affection the internal loads and weight of the structure is wing skin. Effect of modeling of the spar and rib on the structural behavior is not manifest. On the contrast to the general expectation, the models using the bending-resistant elements show the heavier weight than ones by the elements without bending stiffness. From this results, designers of multi-spar wing are recommended to construct the finite element model considering the bending stiffness, or to check the characteristics of the structure before modeling.

• Journal of Dairy Science and Biotechnology
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• v.26 no.2
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• pp.51-56
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• 2008

Using central composite design, we have designed optimization of the manufacturing of processed butter. And response surface analysis by least-square regression was used Statistical Analysis System(SAS). Central composite design can be achieved by response surface techniques that allow flexibility in modeling and analysis. Response surface methodology(RSM) was used to optimize hardness(%) using as independent variables; the content of butter($X_1$), ranging from 50 to 90(%), the content of soybean oil($X_2$), from 0 to 20(%), and the hydrogenated soybean oil($X_3$) from 0 to 4(%). The results on the regression coefficients calculated for overrun by response surface by least-square regression(RSREG) were followed. It was considered that the linear regression was significant(p<0.01). As for the processed butter, the regression model equation for the hardness(Y, %) to the change of an independent variable could be predicted as follow: $Y=60.88-8.92X_2-{29.3X_2}^2$. The optimal for the manufacturing of processed butter were determined at the content of butter of 88.22%, soybean oil of 6.71% and hydrogenated soybean oil of 2.36%, respectively. Optimum compositions were resulted in hardness of 65.78 N. Finally the reference sample(Butter in the morning, Seoul Dairy Co-op.) and processed butter manufacturing under the optimal conditions were compared with spreadability test. The spreadability scores result from reference sample and butter under optimal conditions was not found a significant difference.

• Korean Journal of Food Science and Technology
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• v.35 no.3
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• pp.532-535
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• 2003

Inhibition effects of enzymatic browning in medical herbs (Paeoniore radix rubra, Pueraria radix, Araliae cordatae radix) by organic acid were investigated. The inhibition effects were in the order of citric acid>ascorbic acid>isoascorbic acid>acetic acid in 1% compound, with no significant difference observed between 1% citric acid and 1% sodium metabisulfite. Results revealed that citric acid was the most effective sulfite substitute agent for the inhibition of enzymatic browning of medical herbs.

• Korean Journal of Food Science and Technology
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• v.4 no.4
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• pp.317-321
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• 1972

Octopus Octopus vulgaris was dried with open air at $17{\sim}20^{\circ}C$ for 90 hours. Nucleotides and related substances were collected by extraction with cold perchloric acid, and their amounts were determined by ion exchange column chromatography. The contents of inosine, hypoxanthine and ADP in raw sample were 9.4, 5.1 and 4.1 ${\mu}mole/g{\cdot}dry\;wt.$ respectively. ATP and AMP were very low in content. But IMP was not detected in Octopus muscle. ATP, ADP and inosine tended to degrade rapidly during sun drying while AMP and hypoxanthine were increased. Especially, hypoxanthine were increased about three times during sun drying and also it was increased about two times during three months storage after sun drying.

• Polymer(Korea)
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• v.31 no.3
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• pp.269-272
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• 2007

In this study, we investigated the effects of electron beam irradiation on the rheological properties of PLA for enhancing processability. The electron beam was irradiated onto the pure PLA, chemically modified PLA by reactive extrusion, and PLA containing functional monomer. The complex viscosity and log G'vs. log G" plot among dynamic rheological properties were chosen for comparison. The complex viscosity of irradiated pure and chemically modified PLA decreased significantly due to de-gradation of PLA molecules with increasing the E-beam dosages. Complex viscosity of irradiated PLA with functional monomer showed maximum value at moderate dosage, while at high dosage the complex viscosity was decreased by a prolonged irradiation.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.29 no.10 s.241
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• pp.1407-1415
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• 2005

Strength change of an over-aged A12024 material was studied after being subjected to stages of severe plastic deformation by ECAP (Equal Channel Angular Pressing). Various kinds of strength value were measured using the conventional tensile test, Rockwell and Vickers hardness and the SP (small punch) test Due to limitation of the specimen size, tension test in transverse direction could not be conducted. Hence, SP test was employed for assessing the strength in transverse direction. Based on TEM observation the measured strength characteristics were explained based on the relation between microstructure, dislocation and strength. As the number of ECAP pass increases, the strength of A12024 was also increased. However, considerable change of strength, which is generally predicted, was not observed in this study. For the strength in transverse direction even decrease of the strength was observed after 6 passes of ECAP. It was argued that this decrease was due to dynamic recovery of dislocation density during or after ECAP processes at $150^{\circ}C$. The strength assessment equation proposed by the authors in the previous paper was shown to be very accurate. This argument was supported by comparing the results of conventional tensile test with those of SP test. It was also pointed that the Rockwell har(3ness value seemed to be able to represent the strength in the transverse direction.

• Journal of Conservation Science
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• v.26 no.4
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• pp.417-427
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• 2010

This study is to examine the manufacturing technique based on scientific investigation and analysis on Steel-Plated Jewel Beetle's Adornment gilt-bronze openwork remains excavated from No. 100 site at Hwango-dong Gyeongju. As a result of the investigation on the manufacturing revealed that riveting was adopted to connect gilt-bronze openwork plates and steel plates, followed by mercury amalgam plating method and carving of the patterns by means of the dotted line engraving technique. There were some traces on the surface of Jewel Beetle wings that show the use of pins for fixing, which seems to be the result of recycling or processing. The sectional analysis shows the high possibilities that varnishing with lacquer was adopted for wing adhesion, and it was confirmed that varnishing with lacquer was used on the strap pendant plate to prevent corrosion.

• Journal of the Korea Society for Simulation
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• v.22 no.3
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• pp.7-14
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• 2013

In this paper, there is a research for providing environmental data to reflect environmental effects to the simulation for the aviation weapon systems by the construction of the synthetic battlefield. The results of the aviation engagement simulation are able to differ by environmental effect. This paper analyzes the real aviation battlefield and designs the synthetic battlefield based on the analysis. In order to construct the designed synthetic battlefield, we collects the real environmental data for the atmosphere and structures the collected data using GIS (Geographic information system interpolation). The main objective of this paper is to design the synthetic battlefield based on the derived environmental factors from the analysis of the real aviation battlefield, and it constructs the designed synthetic battlefield by the collection of real atmosphere data. The constructed synthetic battlefield provides the environmental data which are requested from the distributed simulation system, and it makes the system reflect environmental effects to the simulation.