• 제목/요약/키워드: (200) texture

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초전도 선재의 중간 반응 방지막으로써 Ni 기판위에 제조된 NiO 막의 특성 분석 (Fabrication and characterization of nickel oxide films on textured nickel substrate for a superconductor buffer layer)

  • Park, Eunchul;Inki Hong;Hyunsuk Hwang;Taehyun Sung;Kwangsoo No
    • Progress in Superconductivity
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    • 제3권1호
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    • pp.95-98
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    • 2001
  • Recently, NiO films have been studied as a buffer layer to fabricate the superconductor with preferred orientation and as a diffusion barrier to prevent the reaction between superconductor and textured nickel substrate . We fabricated NiO films on textured Ni substrate by thermal oxidation with various variables of temperature, oxidation time, atmosphere, and cooling rate. We investigated the alignment of NiO films by XRD and pole figure and the microstructures by SEM. (200) <001> alignment of NiO film was observed at the oxidation condition of $1200^{\circ}C$ far 10min and slow cooling in O2 atmosphere. During the process in Ar atmosphere, we could also observe the thermal faceting which affects the alignment of NiO alms on Ni substrate.

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국산재(國産材) 곡목가구(曲木家具) 제조(製造)를 위한 Microwave-heating System 활용(活用)에 관한 연구(硏究)(II) - Microwave-heating에 의한 서어나무의 소재(素材) 휨가공특성 - (Study on the Application of Microwave-heating System for Making Bent-wood Furniture(II) - Bending Processing Properties of Carpinus laxiflora BL. by Microwave-heating -)

  • 소원택
    • Journal of the Korean Wood Science and Technology
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    • 제11권2호
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    • pp.52-60
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    • 1983
  • Hornbeam trees(Carpinus laxiflora BL.) are growing in Korea and have good characteristics such as relatively high density, fine texture, split-resistance, and white colour. However, they have seldom been used as manufacturing materials This study was carried out to evaluate the possibility of using hornbeam wood as bent-wood furniture materials. Softening methods were steaming and micro-wave heating. The specimens of $15{\times}15{\times}350mm$ were used green or air-dried, and were steamed at $100^{\circ}C$ for 20min, or microwave heated for 60 seconds. The bending processing conditions are showed in Table 3. The minimum solid-bending radii of air-dried wood were 40mm for steaming and 200mm for micro-wave heating, respectively. And that of green wood were 40mm for micro-wave heating. In conclusion, both of the steamed wood and micro-wave heated green wood showed very good solid bending processing properties, but micro-wave heated air-dried wood were not sufficient for bent-wood furniture.

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양축 정렬된 Ni기판 위에 MOCVD법에 의한 YBCO 초전도 선재용 $CeO_2$ 완충층의 증착 (Deposition of $CeO_2$ buffer layer for YBCO coated conductors on biaxially textured Ni substrate by MOCVD technique)

  • 김호진;주진호;전병혁;정충환;박순동;박해웅;홍계원;김찬중
    • 한국초전도ㆍ저온공학회논문지
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    • 제4권2호
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    • pp.21-26
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    • 2002
  • Textured CeO2 buffer layers for YBCO coated conductors were deposited on biaxially textured Ni substrate by metalorganic chemical vapor deposition (MOCVD). The degree of texture of deposited $CeO_2$ films was strong1y dependent on the deposition temperature (Td) and oxygen Partial Pressure(PO2). ($\ell$00) textured $CeO_2$ films were well deposited at T=500~52$0^{\circ}C$. PO2=0.90~3.33 Torr. The surface morphology showed that the films consisted of columnar CeO2 films grown from the Ni substrates. The root mean square roughness of CeO$_2$ films estimated by atomic force microscopy(AFM) increased as the deposition temperature(Td) increa- sed. The growth rate of the $CeO_2$ films deposited at T=52$0^{\circ}C$ and PO2=2.30 Torr was 150~200 nm/min that was much faster than that of other Physical deposition methods.

Phase Orientation of TiC-$TiB_2$-SiC Ternary Eutectic Composite Prepared by an FZ Method

  • Tu, Rong;Li, Wenjun;Goto, Takashi
    • 한국분말야금학회:학술대회논문집
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    • 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part2
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    • pp.859-860
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    • 2006
  • TiC-$TiB_2$-SiC system was a ternary eutectic, whose eutectic composition was 34TiC-$22TiB_2$-44SiC (mol%). TiC-$TiB_2$-SiC ternary eutectic composite were synthesized by a floating zone method using TiC, $TiB_2$ and SiC powders as starting materials. The TiC-$TiB_2$-SiC eutectic composite showed a lamellar texture. TiC(022), $TiB_2(010)$ and SiC(111) of the eutectic composite were perpendicular to the growth direction. TiC-$TiB_2$-SiC ternary eutectic composite had specific relationship among the crystal planes: TiC[011]//$TiB_2[010]$//SiC[112], TiC(200)//$TiB_2$(001)//SiC(402) and $TiC(1\bar{1}1)$//$TiB_2(101)$//SiC(220).

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Preparation and Characterization of Poly(butyl acrylate)/Poly(methyl methacrylate) Composite Latex by Seeded Emulsion Polymerization

  • Ju, In-Ho;Hong, Jin-Ho;Park, Min-Seok;Wu, Jong-Pyo
    • 한국응용과학기술학회지
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    • 제19권2호
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    • pp.131-136
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    • 2002
  • As model waterborne acrylic coatings, mono-dispersed poly(butyl acrylate-methyl methacrylate) copolymer latexes of random copolymer and core/shell type graft copolymer were prepared by seeded multi-staged emulsion polymerization with particle size of $180{\sim}200$ nm using semi-batch type process. Sodium lauryl sulfate and potassium persulfate were used as an emulsifier and an initiator, respectively. The effect of particle texture including core/shell phase ratio, glass transition temperature and crosslinking density, and film forming temperature on the film formation and final properties of film was investigated using SEM, AFM, and UV in this study. The film formation behavior of model latex was traced simultaneously by the weight loss measurement and by the change of tensile properties and UV transmittance during the entire course of film formation. It was found that the increased glass transition temperature and higher crosslinking degree of latex resulted in the delay of the onset of coalescence of particles by interdiffusion during film forming process. This can be explained qualitatively in terms of diffusion rate of polymer chains. However, the change of weight loss during film formation was insensitive to discern each film forming stages-I, II and III.

Magnetic Properties and Microstructure of Nanocrystalline NdFeB Magnets Fabricated by a Modified Hot Working Process

  • Kim, Hyoung-Tae;Kim, Yoon-Bae;Jeon, Woo-Yong;Kim, Hak-Shin
    • Journal of Magnetics
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    • 제7권4호
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    • pp.138-142
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    • 2002
  • Magnetic properties, microstructure and texture of NdFeB magnets fabricated by a modified hot working process from commercial melt-spun powders (Magnequench; MQPA, MQPB and MQPB+) have been investigated. The hot-pressed isotropic magnet made from MQPA powder, which contains higher Nd content than that of MQPB or MQPB+, shows higher coercivity. The magnet also shows homogenous and fine grains with higher coercivity for higher consolidation pressure. The hot-deformed MQPA magnet shows a strong anisotropy along the press direction with homogeneous platelet Nd$_2$Fe$_{14}$B grains of 50∼100nm in thickness and 200∼500nm in length. The hot-deformed MQPB+ magnet, however, shows low remanence and low coercivity. The microstructure of the magnet consists of two areas; undeformed Nd$_2$Fe$_{14}$B grains and well-aligned but large grains with 3∼4 $\mu$m in length. Low Nd content attributes to the formation of the two different area.

Synthesis of Mesostructured Conducting Polymer-Carbon Nanocomposites and Their Electrochemical Performance

  • Choi, Moon-Jung;Lim, Byung-Kwon;Jang, Jyong-Sik
    • Macromolecular Research
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    • 제16권3호
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    • pp.200-203
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    • 2008
  • A conducting polymer layer was introduced into the pore surface of mesoporous carbon via vapor infiltration of a monomer and subsequent chemical oxidative polymerization. The polypyrrole, conducting polymer has attracted considerable attention due to the high electrical conductivity and stability under ambient conditions. The mesoporous carbon-polypyrrole nanocomposite exhibited the retained porous structure, such as mesoporous carbon with a three-dimensionally connected pore system after intercalation of the polypyrrole layer. In addition, the controllable addition of pyrrole monomer can provide the mesoporous carbon-polypyrrole nanocomposites with a tunable amount of polypyrrole and texture property. The polypyrrole layer improved the electrode performance in the electrochemical double layer capacitor. This improved electrochemical performance was attributed to the high surface area, open pore system with three-dimensionally interconnected mesopores, and reversible redox behavior of the conducting polypyrrole. Furthermore, the correlation between the amount of polypyrrole and capacitance was investigated to check the effect of the polypyrrole layer on the electrochemical performance.

발효숙성마늘 추출물 첨가 초콜릿 제조 조건의 최적화 (Processing Optimization of Chocolate with Fermented and Aged Garlic Extract)

  • 신지훈;주나미
    • 한국식생활문화학회지
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    • 제25권2호
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    • pp.216-224
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    • 2010
  • This study was conducted to aid in the development of the optimal recipe for chocolate with fermented and aged garlic extract (Allium sativum var. pekinense). We added garlic extract in order to increase the nutritional value of the chocolate. The optimal sensory composite recipe was determined, following Central Composites for chocolate with different levels of fermented and aged garlic extract (A) and cream (B), while analysis was performed by Response Surface Methodology, from the date that the sensory evaluation was performed. Ten experimental recipes, including 2 reference points in the composition, were selected. The compositional and functional properties were measured, and physical and sensory values were applied to the mathematical models. Perturbation plots showed the influence of each ingredient on the final product. Measurements showed significant values in lightness, sweetness, pH, hardness and cohesiveness, while sensory measurements showed significant values in color, texture, sourness, bitterness and overall quality. The optimum formulations were calculated by numerical and graphical methods, as being 34.61g fermented and aged garlic extract and 72.68g cream for each 200g chocolate. As well it was revealed that the aptitude of chocolate was more influenced by fermented garlic extract than it was by cream.

파프리카가루를 이용한 소스 개발에 관한 연구 (A Study on the Development of Sauce Using Paprika Powder)

  • 김하윤;최수근;김안나;최혜진;이종필
    • 한국조리학회지
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    • 제18권4호
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    • pp.243-254
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    • 2012
  • 본 연구에서는 파프리카 가루를 이용하여 단기속성 고추장을 제조 하였다. 고추장 제조 후 수분 함량, pH, 염도, 색도, Texture, 환원당, 아미노태 질소, 관능검사를 실시한 결과는 다음과 같다. 파프리카 가루를 이용한 고추장의 수분함량은 대조군이 26.31%, SP1 31.58%, SP2 31.40%, SP3 30.84%, SP4 24.08%를 나타냈다. pH 측정결과, 파프리카 가루 첨가량이 증가함에 따라 pH가 유의적으로 증가하는 경향을 나타냈다(p<0.001). 염도는 4.87~5.22%의 범위를 나타내어 기존의 연구와 비교해 매우 낮은 식염 농도를 보였다. 색도 측정결과, L값은 SP3에서 28.01로 가장 높은 값을 나타냈으며, a값, b값은 대조군이 가장 높은 값을 나타냈다(p<0.001). 텍스쳐 측정결과, 견고성은 시료간의 유의적(p<0.001)인 차이를 보이며 대조군에서 205.50으로 가장 높은 값을 나타냈고, SP3에서 106.53으로 가장 낮은 값을 나타냈다. 부착성에서는 견고성과 반대로 대조군에서 -704.17으로 가장 낮은 값을 나타냈으며, SP3에서 -348.93으로 가장 높은 값을 나타냈다. 환원당은 SP1, SP2에서 가장 높은 값을 나타냈다(p<0.01). 아미노태 질소 측정결과, SP1에서 가장 높은 값을 나타냈으며, SP4에서 가장 낮은 값을 나타냈다(p<0.001).기호도 검사결과, 외관과 향은 SP2에 서 가장 좋게 평가되었으나 유의적 차이는 나타내지 않았다. 질감 항목에서는 대조군과 SP1, SP2에서 가장 좋게 평가되었으며(p<0.05), 전체적 기호도 에서는 SP2가 가장 좋은 기호도를 나타냈으나 유의적인 차이를 보이지는 않았다. 이상의 결과, 파프리카 가루 200g, 콩 가루 150g, 조청 600g, 물 500g, 소금 75g을 넣어 제조한 SP2이 전반적으로 높은 관능 기호도를 나타내어 고추장 제조에 가장 적합하다고 사료된다.

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제초제에 의한 답리작맥 약해발생 요인구명에 관한 연구 (Studies on the Factors Affecting Barley Injury Caused by Herbicides in Drained Paddy Field)

  • 양환승
    • 한국작물학회지
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    • 제14권
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    • pp.147-157
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    • 1973
  • I. 보리 발아시 과습조건이 될 때 그 발아에 미치는 영향을 알고져 건토(LiC) 100g당 30cc, 40cc, 50cc, 60cc의 비율로 물을 가하여 수분함량을 각각 다르게 한 조건을 만들어 Check에 대비하여 Machete(Butachlor), TOK(Nitrofen)을 각각 150g, ai/10a 비율로 처리하였던바 그 결과를 요약하면 다음과 같다. 1. 보리 발아시 수분함량이 포장용수량 이상의 과습이 유지될 때는 무처리구에 있어서도 발아율이 급감하거나 발아되지 아니하며 일단 발아된 후에도 근신장 및 생육이 제대로 되지 못하였다. 2. Machete, TOK 등 약제처리구에 있어서도 1)과 경향은 같으나 무처리구 보다는 그 해가 더욱 증대되였다. II. 토성이 다른 4종류의 토양을 대상으로 하여 Machete (제형별 180 g ai/10a), TOK (약량별 150g, 200g ia/10a), saturn(150g ai/10a), HE314, (250g ai/10a)의 4약제를 사용하여 1cm 복토심하에서 완주 봄보리에 대한 약해차이실험을 실시하였든바 그 결과를 요약하면 다음과 같다. 1. Machete 제형별(180g ai/10a 수준) 약해는 토양의 종류에 따라 심한 차이가 있었으며 식양토에서는 제형에 관계없이 거의 안전하나 사질 식양토<화산회양토<사양토 순위로 약해가 증대되었다. 유제의 약해의 입제의 약해보다 더욱 심하였다. 2. TOK 수화제 150g-200g ai/10a Machete와 거의 동일의 경향이며 약량이 높을 때 약해는 더욱 심하였다. 3. Saturn 150g ai/10a 토성에 따른 약해차이가 있기는 하나 그 차가 심하지는 아니하였다. 4. HE314. 250g ai/10a 250g 시용수준에서는 토성에 따른 약해차가 거의 없었다. III. 2종류의 토양을 대상으로 9개약제(TOK. MO. HE314, Machete, Saturn, Simetryne, Simazine, Gesaran Lorox)을 사용하여 복토심별(4단계)로 약해발생차이를 구명하였던바 그 결과를 요약하면 다음과 같다. 1. 경식ㅌ조건 : 1) Check에 있어서 복토심별 생육상황은 1cm>1.5cm>0.5cm>0cm의 순위였으며 0-0.5cm 복토구에 있어서는 보리 생육이 매우 불량하였다. 2) 약제처리구에 있어서도 0-0.5cm구에 있어서는 심한 해를 나타내고 있으며 1cm 이상의 복토가 유지될 때 보리에 비교적 안전한 약제는 Saturn, Machete, MO, TOK의 100-150g ai/10a, HE314 375-205g ai/10a구 등이었다. 3) 1.5 cm 복토에 있어서도 징해를 나타낸 약제는 Simazine, Lorox, Simetryne 등이었다. 2. 사질토조건 : 1) Cheick에 있어서 생육상황은 1.5cm>0.5cm>0.5cm>3cm>5cm의 순위이었다. 2) 약제처리구에 있어 MO는 1.5 cm 구에서 안전하였고 TOK의 약해는 1.5cm인때 가장 가벼운 편이다. 3) 3cm이상 복토가 될 때 비교적 안전한 약제는 Machete, Saturn 100g ai/10a, HE314 250g ai/10a 이었다. 4) 복토심에 구애없이 불안전한 약제는 Simazine, Lorox, Simetryne Gesaran 등이었다.

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