• 소성∙가공
• /
• 제29권3호
• /
• pp.127-134
• /
• 2020

It is known that the difference of texture of the polycrystalline Al sheet is not a critical parameter for the formation of aligned nanopore arrays in anodic aluminum oxide (AAO). This will be related to the polycrystalline grain in the Al sheet. The texture of each grain in the polycrystalline Al sheet is different. The mixed textures of grains have the mixing effects on the nanopore structure of the AAO. Thus, the effect of Al texture on the nanopore structure of the AAO was investigated using three types of Al single crystals with (111), (200) and (220) textures in this paper. These three types of AAO layers were fabricated by the two-step anodizing method at 40 V and temperature of 0-5℃ in oxalic acid solution. In the nanopores formed on the AAO, the average area of one nanopore and the average roundness of one nanopore were measured were measured based on the SEM images. In the hexagon obtained by connecting nanopores on the AAO, the average standard deviation of one angle deviated from 120° was measured. In the AAO nanopores with texture of (111), (200) and (220) single crystal samples, the average area of one nanopore of (200) single crystal sample was the widest, followed by (111), (220) single crystals. The average circularity of one nanopore of (200) single crystal sample was the best, followed by (111), (220) single crystals. The average standard deviation of an angle from 120° of (220) single crystal sample was the largest, followed by (111) and (200) single crystals.

• Progress in Superconductivity
• /
• 제3권1호
• /
• pp.125-129
• /
• 2001

NiO buffer layers were deposited on texture Ni tapes fur YBCO coated conductors by MOCVD(metal organic chemical vapor deposition) method, using a single solution source. Variables were deposition temperature and flow rate of $0_2$carrier gas. At higher temperatures, The NiO(111) texture was well developed, but the NiO(200) texture was developed at low temperatures. The best result was obtained at the deposition temperature of$ 470^{\circ}C$ and the gas flow rate of 200 sccm. FWHM value of $\omega$-scan fur NiO(200) of the film and $\Phi$-scan for NiO(111) of the film was $4.2^{\circ}$ and $7^{\circ}$, respectively.

• 한국세라믹학회지
• /
• 제47권6호
• /
• pp.479-484
• /
• 2010

Microstructural and mechanical properties of the TiN films deposited on Si substrates under various substrate bias voltages by a reactive magnetron sputtering have been studied. It was found that the crystallographic texture, microstructural morphology and mechanical property of the TiN films were strongly depended on the substrate bias voltage. TiN films deposited without bias exhibited a mixed (200)-(111) texture with a strong (200) texture, which subsequently changed to a strong (111) texture with increasing bias voltage. It is also observed that the crystallite size decreases with increasing bias voltage, which corresponds to the increasing diffraction peak width of XRD patterns. The average surface roughness was calculated from AFM images of the films; these results indicated that the average surface roughness was increased with an increase in the bias voltage of the coatings.

• 한국전기전자재료학회:학술대회논문집
• /
• 한국전기전자재료학회 2003년도 춘계학술대회 논문집 초전도 자성체 연구회
• /
• pp.34-37
• /
• 2003

본 연구는 고온초전도 coated coductors의 기판으로 cube texture된 순수 Ni 기판을 개발하기 위하여 전체 가공율과 압연율에 따른 (100) texture의 변화와 1차적으로 열처리한 기판을 다시 압연한 후 재열처리 하였을 때의 전체 가공율과 압연율에 따른 (100) texture의 변화를 GADS XRD와 SEM을 이용하여 연구하고자 하였다. 그 결과, 압연 후에는 압연율에 관계없이 비교적 약한 강도의 (220)과 (200), (111), (311) peak가 나타났는데, 4%로 압연했을 경우 (220) peak가 가장 강한 peak로 나타난 반면, 10%로 압연한 경우에는 (200) peak가 비교적 강하게 나타났다. 그러나 이를 $900^{\circ}C$에서 열처리한 후에는 (200) peak 만 뚜렷이 발달되어 나타났는데, 전체 가공율과 압연율이 높을수록 (200) peak의 강도가 높게 나타나 압연을 통하여 발달한 결정립자의 (110) 면을 따른 배열이 열처리 과정을 통하여 회전하여 (100)면을 따른 배열로 바뀌는 것으로 추측할 수 있었다. 그러나 $900^{\circ}C$에서 열처리한 두께 0.2mm 판재를 다시 0.1mm까지 4%와 10%의 압연율로 압연하고 500~$900^{\circ}C$에서 1시간동안 최종 열처리한 후에는 상대적으로 낮은 2차 가공율에 의하여 집합조직의 전체 가공율과 압연율에의 의존성이 사라지는 것으로 나타났다.

• 소성∙가공
• /
• 제28권5호
• /
• pp.281-286
• /
• 2019

The plastic strain ratio is one of the factors of the deep drawability of metal sheets. The plastic strain ratio of Al sheet is low value. Therefore, it is necessary to increase the plastic strain ratio in order to improve the deep draw ability of the Al sheet. This study investigated the increase of the plastic strain ratio and the texture change of AA3003 sheet after the hot asymmetric rolling. The average plastic strain ratio of the initial AA3003 sheets was 0.69. After 83% hot asymmetric rolling at $200^{\circ}C$, the average plastic strain ratio was 0.83. The average plastic strain ratio of the 83% hot asymmetrically rolled AA3003 sheet at $200^{\circ}C$ is 1.2 times higher than that of the initial AA3003 sheet. The ${\mid}{\Delta}R{\mid}$ of 83% hot asymmetrically rolled AA3003 sheet at $200^{\circ}C$ is 0.83 times lower than that of the initial AA3003 sheet. This result is due to the development of the intensity of ${\gamma}-fiber$ texture and reduces the intensity of {001}<110> and {001}<100> textures after hot asymmetric rolling of AA3003 sheet.

• 한국소성가공학회:학술대회논문집
• /
• 한국소성가공학회 2009년도 추계학술대회 논문집
• /
• pp.354-357
• /
• 2009

The effect of texture of an extruded OFHC Cu rod on its sliding wear has been explored. Disk specimens with three different orientations were machined from the Cu rod for the wear test; surfaces of the disk were perpendicular ($0^{\circ}$), inclined with a specific angle ($45^{\circ}$), and parallel ($90^{\circ}$) to the extrusion axis of the rod. The texture was analyzed using an X-ray goniometer by measuring {111}, {200}, and {220} pole figures of each specimen. The analyzed texture was correlated with wear-test results of the Cu specimen. Dry sliding wear tests were performed at room temperature using a pin-on-disk wear tester against an Al2O3 ball. Applied load, sliding distance, sliding speed were fixed as 20 N, 200 m, and 0.5 m/sec, respectively. The $45^{\circ}$-inclined (to the extrusion axis) disk specimen showed the lowest wear resistance with the least data scatters. It has been found that distribution of cube texture strongly influences wear rate of the extruded Cu rod.

• 한국세라믹학회지
• /
• 제31권4호
• /
• pp.457-463
• /
• 1994

The growth condition of highly oriented textured diamond film on a (100) Si substrate was investigated as a function of texture orientation. The growth process consisted of biased enhanced nucleation (BEN) and texture growth. The substrate was under the plasma of 6% CH4-94% H2 with negative bias of 200V during the BEN which grounded during the texture growth. The texture orintation changed from <100> to <110> by increasing substrate temperature. The nearly perfect match between textured diamond grains and the Si substrate could be obtained under the condition of <100> texture. The degree of tilt mismatch increased with the increase of deviation of texture orientation from <100>. The degree of twist mismatch appeared to increase abruptly beyond the critical deviation of texture orientation from <100> because the nuclei having the same orientation as the substrate were no more preferred grains for texture formation.

• 대한원격탐사학회:학술대회논문집
• /
• 대한원격탐사학회 2004년도 Proceedings of ISRS 2004
• /
• pp.14-16
• /
• 2004

Although there have been wide range of studies to characterize forest stands based upon spectral information of satellite image, it was not fully understood the texture information of forest stand using high resolution data. The objective of this study is to evaluate several texture measures for characterizing forest stand structure, such as species composition, diameter at breast height(DBH), stand density, and age. High resolution IKONOS satellite imagery data were acquired in August 200 lover the forested area near Ulsan, Korea. Primary forest types were plantation pine, mixed forest, and natural deciduous forest of stand age ranging from 10 to 50 years old. Several GLCM-based texture measures were compared with forest stand characteristics. In overall, a texture measure (contrast) calculated using red band were better to differentiate species and age group than other texture measures and near infrared bands.

• 한국주조공학회지
• /
• 제15권4호
• /
• pp.397-407
• /
• 1995

The objectives of this study are first, to expand our understanding of relationship between magnetic properties and microstructural features such as grain size and texture, and second to reduce core loss of Fe-6.5%Si strip through optimizing heat treatment conditions. A rapid solidification technique, planar flow casting(PFC), was adopted to produce Fe-6.5%Si strips. The strips were heat treated under various conditions. The results show that heat treatment conditions can change not only grain size but also (200) texture formation on the strip surface. Variation in magnetic properties of Fe-6.5%Si strip is analyzed in terms of the change in grain size as well as (200) texture on the strip surface. The heat treatment conditions of $1100^{\circ}C$ over 2 hr or $1150^{\circ}C$ $1{\sim}2hr$ in $N_2+5%H_2$ appear to minimize core loss of Fe-6.5%Si strips.

• 한국표면공학회지
• /
• 제41권6호
• /
• pp.287-291
• /
• 2008

Reactively magnetron sputtered TiN films were deposited on Si wafers under varying bias voltage and characterized by X-ray diffraction, field-emission scanning electron microscopy and Nanoindentation. The films deposited under an Ar + $N_2$ atmosphere exhibited a mixed (200)-(111) orientation with a strong (200) texture, which subsequently changed to a strong (111) texture with increasing bias voltage. The changes in texture and grain size of the TiN thin films are due to one or a combination of factors such as strain energy, surface free energy, surface diffusivity and adatom mobility. The influence of each factor depends on the processing conditions. The average deposition rate and grain size were calculated from FE-SEM images of the films indicating that the deposition rate was lower at the films deposited under bias voltage.