• 제목/요약/키워드: %24V_2O_5%24

검색결과 308건 처리시간 0.034초

알루미늄 에치피트에 ZrO2 막의 졸-겔 코팅 및 양극산화 특성 (Sol-gel Coating of ZrO2 Film in Aluminium Etch Pit and Anodizing Properties)

  • ;박상식
    • 한국재료학회지
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    • 제24권5호
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    • pp.259-265
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    • 2014
  • $ZrO_2$ films were coated on aluminum etching foil by the sol-gel method to apply $ZrO_2$ as a dielectric material in an aluminum(Al) electrolytic capacitor. $ZrO_2$ films annealed above $450^{\circ}C$ appeared to have a tetragonal structure. The withdrawal speed during dip-coating, and the annealing temperature, influenced crack-growth in the films. The $ZrO_2$ films annealed at $500^{\circ}C$ exhibited a dielectric constant of 33 at 1 kHz. Also, uniform $ZrO_2$ tunnels formed in Al etch-pits $1{\mu}m$ in diameter. However, $ZrO_2$ film of 100-200 nm thickness showed the withstanding voltage of 15 V, which was unsuitable for a high-voltage capacitor. In order to improve the withstanding voltage, $ZrO_2$-coated Al etching foils were anodized at 300 V. After being anodized, the $Al_2O_3$ film grew in the directions of both the Al-metal matrix and the $ZrO_2$ film, and the $ZrO_2$-coated Al foil showed a withstanding voltage of 300 V. However, the capacitance of the $ZrO_2$-coated Al foil exhibited only a small increase because the thickness of the $Al_2O_3$ film was 4-5 times thicker than that of $ZrO_2$ film.

열산화법 및 PECVD 법에 의한 T$a_2O_5$ 유전 박막 (T$a_2O_5$Dielectric Thin Films by Thermal Oxidation and PECVD)

  • 문환성;이재석;한성욱;박상균;양승기;이재학;박형호;박종완
    • 한국재료학회지
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    • 제2권5호
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    • pp.353-359
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    • 1992
  • 열산화법과 PECVD법으로 p-type (100) Si 기판위에 T$a_2O_5$ 박막을 형성시킨 후 A1/T$a_2O_5$/p-Si capacitor를 제작하였다. 제작된 시편의 제반 물성은 XRD, AES, high frequency C-V analyzer, I-V meter, TEM 등을 사용하여 분석하였다. XRD 분석을 통해 T$a_2O_5$ 박막은 비정질임이 확인되었으며 65$0^{\circ}C$ 열처리의 경우에는 hexagonal $\delta$-T$a_2O_5$ 상으로 결정화가 일어남을 확인할 수 있었다. AES spectrum의 분석을 통해 T$a_2O_5$ 박막의 조성이 2:5의 stoichiometry에 근접해 있음이 관찰되었다. 열산화법에 의해 제작된 T$a_2O_5$는 산화온도 60$0^{\circ}C$의 조건에서 누설전류 5${ imes}10^{-6}$A/c$m^2와 유전상수 31.5로 가장 좋은 성질을 나타냈으며, PECVD로 제작한 T$a_2O_5$는 RF Power가 0.47W/c$m^2일 때 2.5${ imes}10^{-5}$A c$m^2and 24.0으로 가장 좋은 특성을 나타내었다. TEM 분석을 통해 제조된 박막과 계면을 관찰하였다.

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금강 하구의 Vibrio cholerae non-O1과 Vibrio mimicus의 선택 (Ecology of Vibrio cholerae non-O1 and Vibrio mimicus in Estuary of Kum River, Korea)

  • 장수현;송대진;양송주;신일식;김영만
    • 한국수산과학회지
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    • 제28권1호
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    • pp.15-22
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    • 1995
  • 새로운 식중독 원인균으로 알려지고 있는 V cholerae non-O1과 V mimicus의 분포와 서식 조건을 밝히고자 금강 하구에서 1993년 3월 26일부터 1994년 2월 22일까지 수질 환경과 V cholerae non-O1 및 V mimicus의 분포를 조사한 결과는 다음과 같다. 1. V cholerae non-O1은 해수 54개 시료에서 $16.7\%$, 뻘 49개 시료에서 $6.1\%$, 전체 $11.7\%$가 검출되었으며 V mimicus는 해수 54개 시료에서 $11.1\%$, 뻘 49개 시료에서 $10.2\%$, 전체 $10.7\%$가 검출되었다. 2. V cholerae non-O1과 V. mimicus는 수온 $24^{\circ}C$이상, 염도 $10\%o$ 이하의 기수에서 주로 검출되었으나, 수온이 $3.5^{\circ}C$인 1월에 뻘에서 검출되었다. 3. V cholerae non-O1과 V. mimicus의 서식에 영향을 주는 주요 인자는 온도, 염도 및 유기물질의 오염이며, V. cholerae non-O1은 V. mimicus보다 염도 변화에 대한 적응력이 더 높았다.

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Hansenula sp. MS-364의 생육과 Formate Dehydrogenase의 활성

  • 유병욱;권태종
    • 한국미생물·생명공학회지
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    • 제25권4호
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    • pp.403-407
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    • 1997
  • Medium components for maximum activity of NAD$^{+}$-dependent formate dehydrogenase (EC 1.2.1.2; FDH) were optimized with a methanol-assimilating yeast Hansenula sp. MS-364, preserved by our laboratory. The maximum activity of the enzyme was obtained when the strain was cultivated at 30$circ$C for 24 hours in a medium containing methanol 3%(v/v), yeast extract 0.8%(w/v), K$_{2}$HPO$_{4}$, 0.1%(w/v), KH$_{2}$PO$_{4}$ 0.1%(W/V), MgSO$_{4}$, 7H$_{2}$O 0.05%(w/v), and the pH of the culture broth was adjusted at 5.0.

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ZPCCL계 세라믹스의 바리스터 특성 (Varistor Properties of ZPCCL-based Ceramics)

  • 남춘우
    • 한국재료학회지
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    • 제16권7호
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    • pp.416-421
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    • 2006
  • The varistor properties of ZPCCL-based ceramics were investigated at different $La_2O_3$ contents in the range of $0{\sim}2.0$ mol%. As $La_2O_3$ content increased, the ceramic density greatly increased in the range of $4.71{\sim}5.77\;g/cm^3$ and the varistor voltage greatly decreased in the range of $503.5{\sim}9.4$ V. The varistor with 0.5 mol% $La_2O_3$ exhibited good nonlinearity, in which the nonlinear exponent is 81.6 and the leakage current is 0.2 ${\mu}A$. Furthermore, the varistors exhibited the high electrical stability, with $%{\Delta}V_{1mA}=-1.1%,%{\Delta}{\alpha}=-3.7%$, and $%{\Delta}I_L=+100%$ for DC accelerated aging stress condition of 0.95 $V_{1mA}/150^{\circ}C/24$ h.

EWOD 구조에서 상유전체 BZN에 의한 micro droplet의 이동 특성 (The Movement Characteristic of Micro Droplet by BZN in EWOD structure)

  • 김나영;홍성민;박순섭
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 2005년도 추계학술대회 논문집 전기물성,응용부문
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    • pp.36-38
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    • 2005
  • This study is about how to lower the driving voltage that enables to move the micro droplet by the EWOD (Electro Wetting On Dielectric) mechanism. EWOD is well known that it is used ${\mu}-TAS$ digital micro fluidics system. As the device which is fabricated with dielectric layer between electrode and micro droplet is applied voltage, the hydrophobic surface is changed into the hydrophilic surface by electrical property. Therefore, EWOD induces the movement of micro droplet with reducing contact angle of micro droplet. The driving voltage was depended on the dielectric constant of dielectric layer, thus it can be reduced by increase of dielectric constant. Typically, very high voltage ($100V{\sim}$) is used to move the micro droplet. In previous study, we used $Ta_{2}O_{5}$ as the dielectric layer and driving voltage was 23V that reduced 24 percent compared with $SiO_2$. In this study, we used $BZN(Bi_{2}O_{3}ZnO-Nb_{2}O_{5})$ layer which had high dielectric constant. It was operated the just 12V. And micro droplet was moved within Is on 15V. It was reduced the voltage until 35 percents compare with $Ta_{2}O_{5}$ and 50 percents compare with $SiO_2$. The movement of micro droplet within 1s was achieved with BZN (ferroelectrics)just on 15V.

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$V_2O_5$ 첨가가 $Zn_3Nb_2O_8$ 마이크로파 유전체 특성에 미치는 영향 (The Effect of $V_2O_5$ Addition on the Microwave Dielectric Properties of $Zn_3Nb_2O_8$ Ceramics)

  • 윤호병;이태근;황연
    • 한국결정학회지
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    • 제17권1호
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    • pp.24-32
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    • 2006
  • [ $Zn_3Nb_2O_8$ ]세라믹스에 액상소결제인 $V_2O_5$를 첨가하여 소결하여 고주파 대역에서의 유전특성의 변화를 조사하였다. $1100^{\circ}C$에서 2시간 하소한 결과 $Zn_3Nb_2O_8$를 합성할 수 있었고, $V_2O_5$를 첨가하여 소결한 $Zn_3Nb_2O_8$에서 $V_2O_5$의 mole%증가와 소결온도의 증가에 따라 상대밀도 95%의 소결특성을 확인 하였다. 유전율 특성은 $V_2O_5$ mole ratio가 $2{\sim}4%$의 시편에서 모두 ${\varepsilon}_r\;21$ 이상으로 증가됨을 확인하였고, 품질계수는 $900^{\circ}C$에서 소결한 $V_2O_5$ 2 mole% 시편에서 $Q{\times}f=40,000$을 나타내었다. 온도계수는 $900^{\circ}C$ 소결하고 $V_2O_5$ 1 mole% 첨가한 경우 0에 제일 가까운 $T_{cf}=-54ppm/^{\circ}C$를 나타내었고, 다른 보건에서는 $T_{cf}=-60{\sim}-80ppm/^{\circ}C$의 값을 나타내었다.

암 치료를 위한 188Re(V)-DMSA에 관한 연구: 방사성동위원소 표지와 생체내 분포 (Study of 188Re(V)-DMSA for Treatment of Cancer: Radiolabeling and Biodistribution)

  • 김영주;정재민;장영수;이동수;정준기;이명철;고창순
    • 대한핵의학회지
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    • 제32권1호
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    • pp.81-88
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    • 1998
  • 암 치료용 방사성의약품으로 $^{188}Re(V)$-DMSA의 사용가능성에 대하여 실험하였다. DMSA 키트($NaHCO_3$ 1.5 mg, meso-2,3-dimercaptosuccinic acid 1.0 mg, L(+)-ascorbic acid 0.7 mg, $SnCl_2{\cdot}2H_2O$ 0.34 mg, pH 2.9)를 제조하였다. 이 키트에 $^{188}ReO_4{^-}$ 5 mCi/2 ml을 넣어 $100^{\circ}C$에서 3시간 반응시킨 후 7% $NaHCO_3$을 사용하여 pH를 7.5로 조절하였다. $^{188}Re(V)$-DMSA의 표지효율은 98% 이상이었으며, $^{188}Re(V)$-DMSA의 안정성을 실온에서 측정한 결과 48시간 동안 95%이상으로 나타났다. 혈청 내에서의 안정성 시험 결과 $^{188}Re(V)$-DMSA의 양은 6시간 후 82%, 48시간 후에 85%로 나타났다. 암육종(Sarcoma 180) 이식 마우스의 꼬리정맥에 $^{188}Re(V)$-DMSA(111~185 kBq/0.1 ml)을 주사하고 1, 3, 13, 24, 48시간 후 장기를 적출하여 감마선계측기로 각 장기에 섭취된 방사능을 측정하였다. 종양(Satcoma 180)의 섭취는 $^{188}Re(V)$-DMSA 투여 후 1 시간에 $0.66{\pm}0.15$, 3시간에 $0.51{\pm}0.10$, 24시간에 $0.19{\pm}0.05$, 48시간에$0.13{\pm}0.02%ID/g$로 이 실험에 시용한 Sarcoma 180에 대하여는 별로 높지 않았다. 그려나 여러 문헌에 보고된 바 있는 $^{99m}Tc(V)$-DMSA와 약간의 차이가 있지만 생체내분포가 유사하여 표지후 생성된 이성체 연구 및 표지방법의 개선 등 후속연구가 뒤따를 경우 암이나 뼈 전이 통증 등의 치료용으로 사용할 가능성이 있음을 알았다.

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영유아 뇌성 운동발달 장애아에 대한 보이타치료법 조기적용의 효과 (The Effects of the Early Intervention of V{\ddot{o}}jta Therapy for the Infant with Central Coordination Disturbance)

  • 양우진;김중선;안수윤;김병조
    • The Journal of Korean Physical Therapy
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    • 제13권1호
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    • pp.49-59
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    • 2001
  • The purpose of this study was to examine the effect of treatment when the V{\ddot{o}}jta therapy applied to the infant with central coordination disturbance in early stage. The subject were 10 cases : each one with the V{\ddot{o}}jta therapy applied to the group of the infants before 6 months old and the group of the infants over 6 months old. When the V{\ddot{o}}jta therapy was applied I analized the papper which was written about the infants who were diagnosed as moderate CCD and divided two groups which were the infants before 6 months old and the infants over 6 months old. These collected data were analyzed by using t-test. The results of study were as follow; 1. When I compared the locomotion stage after the V{\ddot{o}}jta therapy. t-test showed significant differences. The group of infants before 6 months old had the result 7 to over stage 7 and the group of infants over 6months old had the result 2(p<.05). 2. When I compared the result of the postural reaction after the V{\ddot{o}}jta therapy, 1-test showed significant differences. The group of infants before 6 months old had 6 cases was normalizes and the group of infants over 6 months old had 1 case was normalized(p<.05). 3. When 1 compared the duration of the V{\ddot{o}}jta therapy between the group of infants before 6 months old and the group of infants over 6 months old. t-test showed significant differences. The group of the infants before 6 months old had 5 cases for 1-6 months and 4 cases for 7-15 months, 3 cases for 16-24 months and the group of infants over 6 months old had 6 cases for 7-15 months and cases for 16-24 months, 1 case for 25-30 months(p<.01).

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고열을 이용한 잔류 오존($O_3$) 처리에 관한 연구 (The study on the treatment of the remaining Ozone($O_3$) by the high heater)

  • 김재우
    • 환경위생공학
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    • 제16권2호
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    • pp.9-16
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    • 2001
  • If a pollutant invade at liguid and gas, it will be use ozone in order to remove or sterilize. Ozone excessively supply in order to receive satisfactory efficiency. If excessive ozone leave like that, second-problem will be occur. This study used high heater in order to treat occurred ozone. ; the results were as follow : 1. As initial ozone os supplied with $1.789{\;}g/m^3$ : For the 40, 50, 60, 70(V) of electric potential $O_3$ removal efficiency was treated 34.41, 73.78, 98.60, 98.97%(time of operation ; after 5min.). 2. As initial ozone is supplied with $3.645{\;}g/m^3$ : For the 40, 50, 60, 70(V) of electric potential, $O_3$ removal efficiency was treated 1.78, 69.27, 99.18, 98.68%(time of operation ; after 5min.). 3. As initial ozone is supplied with $4.759{\;}g/m^3$ : For the 50, 60, 70(V) of electric potential, $O_3$ removal efficiency was treated 61.29, 99.29, 99.18%(Time of operation ; after 5min.). 4. Used electric power is 15.38, 24.00, 35.29, 46.15(w/hr) at the 40, 50, 60, 70(V) of the electric potential. 5. Regarding electric power and $O_3$ removal efficiency, Used electric pote-ntial economized at 60(V).

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