• 제목/요약/키워드: $f_0$ variation

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GC에서 검출한계 결정을 위한 새로운 접근 방법에 대한 연구 (Study on the new approaching method to determine limit of detection by gas chromatography)

  • 오도석;신경애;이지아;임종호;신미선
    • 한국산업보건학회지
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    • 제20권4호
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    • pp.217-224
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    • 2010
  • The purity methods to determine LOD/LOQ using standard deviation of the residual, intercept and blank by IUPAC and ACS describe many of the pitfalls and pose significant challenges to analytical chemists. Therefore, the aim of this study is the development of the simple, easy, convenient and statistically significant method to determine LOD in quantitative analysis of organic solvents by GC. The new approaching method by linearization in the given concentration range used coefficient of variation ; ${\sigma}_{n-1}$/S(standard deviation, ${\sigma}_{n-1}$ and average, S) of sensitivity(Response/concentration). The comparison of results among the purity methods(IUPAC and ACS) and the linearization have been fulfilled the F-test for standard deviations and t-test for LOD range values. The results of F-test and t-test are satisfied within 95 % confidence level, respectably. The LOD values determined by the new procedure are n-Hexane 0.0116 mg/$m^3$, Toluene 0.0807 mg/$m^3$, and o-Xylene 0.0494 mg/$m^3$. Because the standard deviation of the residual, intercept and blank and the slope of calibration curve are not calculated and the new approaching method use the coefficient of variation of sensitivity by linearization, this new method is simple, easy, convenient and statistically significant. In future, many chemical analysts will expect to applicate and routinely use this method in the all quantitative analysis.

한국산 무미류에 대한 유전학적 연구 : 청개구리속 2종(Hyla japonira, H. suweonensis)에 대한 mtDNA의 크기 및 제한효소 인식위치의 변이 (Genetic Studies on Korean Anurans: Length and Restriction Site Variation in the Mitochondrial DNA of Tree Frogs, Hyla japonica and H. suweonensis)

  • 이혜영;박창신
    • 한국동물학회지
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    • 제35권2호
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    • pp.219-225
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    • 1992
  • The genetic variation in mitochondrial DNA (mtDNA) was analysed within and between two species of tree frogs. Hyla japonica and H. suweonensis from South Korea. Purified mtDNAs were digested with each of 11 restriction enLvmes which cleave at six base recognition sequences. The genome size of H. iaponica revealed ho types (20.0 $\pm$ 0.3 and 19.6 $\pm$ 0.3 kb) and this difference is explained by either addition or deletion of about 0.4 kb fragment. On the other hand, the genome sire of H. suueonensis was about 19.0 $\pm$ 0.4 kb only. For the analysis, level of fragment homology (F) and nucleotide sequence divergence (p) were estimated from comparisons of digestion profiles. Among four populations of H. iaponica, substantial mean sequence divergence was 0.017 (range 0.001-0.026); between identical types, 0.001 IslilaRl type) and 0.004 (Large type) respectively; between different ones, 0.024 (range 0.023-0.026). The level of sequence divergence between he species was 0.142 (range 0.131-0.146). This result suggested that he species ㅂwere distinctly differentiated species. The divergence time between ko species was estimated 7.1 million years.

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2002년 여름 북서태평양 표층 해수의 이산화탄소 분포 특성 (The Surface fCO2 Distribution of the Western North Pacific in Summer 2002)

  • 최상화;김동선;심정희;민홍식
    • Ocean and Polar Research
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    • 제28권4호
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    • pp.395-405
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    • 2006
  • We measured the fugacity of $CO_2$ $(fCO_2)$, temperature, salinity, nutrients and chlorophyll a in the surface water of the western North Pacific $(4^{\circ}30'{\sim}33^{\circ}10'N,\;144^{\circ}20'{\sim}127^{\circ}35'E)$ in September 2002. There were zonally several major currents which have characteristics of specific temperature and salinity (NECC, North Equatorial Counter Current; NEC, North Equatorial Current; Kuroshio etc.). Surface $fCO_2$ distribution was clearly distinguished into two groups, tropical and subtropical areas of which boundary was $20^{\circ}N$. In the tropical Int surface $fCO_2$ was mainly controlled by temperature, while in the subtropical area, surface $fCO_2$ was dependent on total inorganic carbon contents. Air-sea $CO_2$ flux showed a large spatial variation, with a range of $-0.69{\sim}0.79 mmole\;m^{-2}day^{-1}$. In the area of AE (Anticyclonic Eddy), SM(Southern Mixed region) and NM (Northern Mixed region), the ocean acted as a weak source of $CO_2$ $(0.6{\sim}0.79 mmole\; m^{-2}day^{-1})$. In NECC, NEC, Kuroshio and ECS (East China Sea), however, the fluxes were estimated to be $-0.3mmole\; m^{-2}day^{-1})$ for the first three regions and $-1.2mmole\; m^{-2}day^{-1})$ for ECS respectively, indicating that these areas acted as sinks of $CO_2$. The average air-sea flux in the entire study area was $0.15mmole\;m^{-2}day^{-1})$, implying that the western North Pacific was a weak source of $CO_2$ during the study period.

Relationships between Fecundity and Total Length, Body Weight, Ovary Length, and Ovary Weight of Hilsa Shad, Tenualosa ilisha Hamilton, in Patuakhali, Bangladesh

  • Mondal, Borun Kumar;Devnath, Sukumar;Shaha, Dinesh Chandra;Khan, Mohammed Nurul Absar;Choi, Jae-Suk
    • Fisheries and Aquatic Sciences
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    • 제11권2호
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    • pp.98-102
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    • 2008
  • Relationships between total length (TL) and fecundity, body weight and fecundity, ovary length and fecundity, and ovary weight and fecundity of hilsa shad, Tenualosa ilisha Hamilton, collected from Kuakata, Patuakhali, Bangladesh, were studied. During the sampling period, the fecundity of hilsa was found to range from 169,000 (fish TL=28.0cm, weight=250g) to 1,088,000 (fish TL=40.5cm, weight=955g) with a mean of $520{\pm}53{\times}1,000$. The number of eggs per gram of ovary for samples collected from the anterior, middle, and posterior regions of the ovary were also recorded, but no significant variation was found among ovary regions at the 5% level of significance. Fecundity increased with fish TL and weight. The regression equations obtained in arithmetic forms of relationships between TL and fecundity (F), body weight (BW) and fecundity, ovary length (OL) and fecundity, and ovary weight (OW) and fecundity were $F=-887,896+40,511{\times}TL(r=0.85)$, $F=67,577+755.44{\times}BW(r=0.85)$, $F=-562,070+87,668{\times}OL(r=0.75)$ and $F=124,815+6,596.7{\times}OW (r=0.84)$, respectively. The relationships between fecundity and TL, body weight, ovary length, and ovary weight were linear, and the 'r' values were highly significant (p<0.01). These results provide valuable data for the restoration of hilsa resources, which are economically important but have shown reduced productivity in nations adjacent to the Bay of Bengal.

5% 불화나트륨을 함유한 고분자 접착필름의 법랑질 재광화효과 (Effect of Polymer Adhesive Film Supplemented 5% NaF on Enamel Remineralization)

  • 지명관;이상호;이난영
    • 대한소아치과학회지
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    • 제41권3호
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    • pp.218-224
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    • 2014
  • 이 논문은 법랑질의 표면미세경도와 QLF의 ${\Delta}F$ 값의 변화를 분석하여 5% 불화나트륨을 함유한 고분자 접착 테잎(NaF-PVA)이 법랑질의 재광화에 미치는 영향을 평가하고자하였다. 시편을 탈회한 후 표면미세경도가 평균 50-100 KHN의 범위를 갖고 QLF의 ${\Delta}F$ 값이 -25에서 -15 범위를 갖는 60개의 시편들을 4그룹으로 나누었다 : 그룹1(대조군), 그룹2(NaF-PVA), 그룹3(불소바니쉬, FluoroDose$^{(R)}$ varnish), 그룹4(Casein phosphopeptide-amorphous calcium phosphate, Tooth mousse plus$^{TM}$). 시편들에 각 제제들을 적용하고 인공타액(artificial saliva)에 담근 후 표면미세경도계와 정량 광 형광기를 이용하여 재광화율을 측정하였다. 그 결과 불소를 함유한 고분자 접착 테잎(NaF-PVA)은 그룹1과 4보다 뛰어나며 그룹3과 견줄만한 재광화 효과를 나타냈다 (p<0.05).

뇌졸중 환자 대상 흡인 음성의 음향변수 변동 (Acoustic parameter delta of an aspirated voice in stroke patients)

  • 강영애;지성주;구본석;조철우
    • 말소리와 음성과학
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    • 제9권3호
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    • pp.85-91
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    • 2017
  • The present study aimed to investigate the changes of acoustic parameters of the aspirated voice in stroke patients. The eighty-eight subjects diagnosed with cerebro-vascular accident were divided into 32 penetration/aspiration (P/A) and 56 Non-P/A groups according to the videofluroscopic swallowing study (VFSS) results, and 26 control subjects participated. All subjects preformed VFSS and vowel /a/ was recorded three times pre- and post VFSS. Since the variation in the acoustic parameters within a single phonation has been observed, we proposed a delta formula for the acoustic parameters which can reflect the temporal changes of the each parameter in an utterance. We measured from the voice data eight acoustic parameters: fundamental frequency (F0), standard deviation of F0 (F0_SD), Jitter, relative average perturbation (RAP), Shimmer, amplitude perturbation quotient (APQ), harmonic to noise ration (HNR), noise to harmonic ratio (NHR). Then we found parameters which show the meaningful biggest temporal change in an utterance using the suggested delta parameter. Among them, the deltas of shimmer and APQ were significantly different pre- and post VFSS. These deltas of the P/A and the control group were increased after VFSS, while those of the Non-P/A group was descended. The variation patterns of the P/A and the control group were similar but the change width of the P/A group was larger. The large variations in an aspirated phonation of the P/A group are thought to be caused by irregular changes in air resistance due to residual food on the vocal cords.

FACTORS INFLUENCING FEED EFFICIENCY AND BACKFAT THICKNESS IN STATION TESTED BEEF BULLS

  • Liu, M.F.;Makarechian, M.;Price, M.A.;Huedepohl, C.
    • Asian-Australasian Journal of Animal Sciences
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    • 제8권5호
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    • pp.495-498
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    • 1995
  • Records taken on 372 young beef bulls tested at the Ellerslie Bull Test Station, Alberta, Canada from November 1981 to April 1987 were analyzed to quantify the effects of age of dam, on-test age, on-test liveweight and herd of origin of bull on feed efficiency (feed/gain, kg/kg) in the test period (n = 231) and ultrasonic measurement of bakcfat thickness (mm) at the end of the test (n = 372). The reduction in $R^2$ due to each influencing factor (i.e. the variation accounted for by the factor) was used to indicate the importance of the influencing factor. Age of dam and on-test age of bull were not important factors on feed/gain and ultrasonic backfat thickness, as they accounted for less than 0.5% of the variation in feed/gain and ultrasonic backfat thickness, respectively (p > 0.1). On-test liveweight had some influence on feed/gain and ultrasonic backfat thickness, accounting for 3.5% (p < 0.01) and 0.4% (p < 0.05) of the total variation, respectively. The regression coefficients of feed/gain and ultrasonic backfat thickness on on-test liveweight were 0.016 (kg/kg)/kg and .013 mm/kg, respectively, both being significant (p < 0.05), indicating that lighter bulls entering the test were generally more efficient in feed utilization in the test period and had less backfat at the end of the test than heavier entering bulls. Herd of origin of bull accounted for a substantial amount of the total variation (> 16%) in feed/gain and ultrasonic backfat thickness (p = 0.08), indicating that a prolonged aqjustment period was needed to reduce the influence of herd of origin when assessing aggregate genetic merit of beef bulls for growth rate, feed efficiency and lean meat production using a central station performance testing program.

STRAIN RATE CHANGE FROM 0.04 TO 0.004%/S IN AN ENVIRONMENTAL FATIGUE TEST OF CF8M CAST STAINLESS STEEL

  • Jeong, Ill-Seok;Kim, Wan-Jae;Kim, Tae-Ryong;Jeon, Hyun-Ik
    • Nuclear Engineering and Technology
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    • 제43권1호
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    • pp.83-88
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    • 2011
  • To define the effect of strain rate variation from 0.04% to 0.004%/s on environmental fatigue of CF8M cast stainless steel, which is used as a primary piping material in nuclear power plants, low-cycle fatigue tests were conducted at operating pressure and temperature condition of a pressurized water reactor, 15 MPa and $315^{\circ}C$, respectively. A high-pressure and high-temperature autoclave and cylindrical solid fatigue specimens were used for the strain-controlled low-cycle environmental fatigue tests. It was observed that the fatigue life of CF8M stainless steel is shortened as the strain rate decreases. Due to the effect of test temperature, the fatigue data of NUREG-6909 appears a slightly shorter than that obtained by KEPRI at the same stress amplitude of $1{\times}10^3$ MPa. The environmental fatigue correction factor $F_{en}$'s calculated with inputs of the test data increases with high strain amplitude, while the $F_{en}$'s of NUREG-6909 remain constant regardless of strain amplitude.

리브 간격 변화에 따른 열.유동 수치해석 및 압력 저하 특성 (Numerical Analysis of Thermal and Flow affected by the variation of rib interval and Pressure drop Characteristics)

  • 정한식;이경환;신용한;최순호;정효민
    • Journal of Advanced Marine Engineering and Technology
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    • 제35권5호
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    • pp.616-624
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    • 2011
  • 본 연구에서는 사각채널내에 주유속 방향에 가로지르게 배치된 반원 리브의 난류 유동에 대한 유동 특성과 열전달 증대에 관해 수치해석적으로 살펴보았다. 사각채널의 종횡비는 5이고, 수력직경 대비 리브 높이비는 0.07, 사각채널 높이 대비 리브 높이비는 0.117로서 리브 높이 대비 리브 피치비가 8~14인 리브를 주기적으로 배열하여 연구를 수행하였다. 난류 모델의 선정은 실제 현상과 근접한 벽 근처 유동 특성과 열전달을 위해 SST k-${\omega}$ 난류 모델과 v2-f 난류 모델을 이용하였다. 수치해석의 결과는 실험에 의 해 관찰된 난류 유동 특성, 열전달 및 마찰계수의 결과를 잘 예측함을 보여준다. 본 결과에서 난류 운동 에너지가 재순환류 영역의 확산과 밀접한 관련이 있음을 알 수 있고 v2-f 난류 모델이 SST k-${\omega}$ 난류 모델에 비해 실험결과를 더 잘 예측하였다.

Far-field 위상 변조량 측정법을 이용한 광학매질의 비선형 특성 측정 (Measurement of the Nonlinear Optical Properties by use of the Far-Field Phase Modulation Method)

  • 김성훈;양준목;김용평;이영우;신동주;정영붕
    • 한국광학회지
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    • 제9권3호
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    • pp.168-174
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    • 1998
  • 본 연구에서는 광학매질의 비선형 특징을 측정하기 위해, 자체집속현상을 이용하는 기존의 측정법과는 다르게, 매질을 통과한 광원의 위상섭동으로 인하여 far-field에 발생한 공간적 광장도 분포를 이용하는 far-field 위상 변조량 측정법을 사용하였다. 미선형 매질을 통과한 조사과의 위상 변화가 far-field 영역에서 나타나는 겅간적 위상 변조량을 실험적으로 측정아였고, 이를 전산시\ulcorner을 통하여 비교분석하였다. 파장 616nm, 펄스폭 106ps의 분포궤한 섹소레이저(DFDL)와 파장 308nm인 DFDL의 제2고조파를 조사광으로 사용하였고, 매질 $CS_2$$BaF_2$의 비선형 특성을 실험적으로 측정한후 이 값을 전산시늉값과 비교하였다. 이 실험에서 파장 616nm에 대해 $CS_2$$BaF_2$의 비선형 굴절률 $1.2{\times}10^{-11}$ esu와 $1.0{\times}10^{-13}$ esu를 각각 얻었고, 파장 308nm에 대해 $BaF_2$의 비선형 흡수계수 $5.0{\times}10^{-11}$cm/W를 얻었다. 이들 값은 지금까지 발표된 값들과 잘 일치한다.

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