• 한국재료학회지
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• 제3권4호
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• pp.381-387
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• 1993

${Si_3}{N_4}$와 BN의 선택적 산화반응과 질소분위기 소결에 의하여 $Si_2N_2O$로 결합된$Si_3N_4-BN$복합재료를 개발하였으며, 이때 산화반응 온도와 CaO의 첨가가 $Si_2N_2O$의 생성에 미치는 영향을 고찰하였다. $Si_2N_2O$상이 도입된 $Si_3N_4-BN$복합재료는 내열충격성 및 용강에 대한 내침식성이 우수하여 연속제강새안의 부품인 break ring등의 소재로 사용될 수 있다.

• 한국세라믹학회지
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• 제36권10호
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• pp.1007-1015
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• 1999

The Si3N4 composites reinforced with carbon-coated SiC whiskers were fabricated by hot-pressing at 180$0^{\circ}C$ for 2 hours to examine the effects of carbon-coated whiskers on the mechanical properties of SiC whisker reinforced Si3N4 composites. The flexural strength of the Si3N4 composites and Si3N4 monolith respectively. The weak interfacial bond between carbon-coated SiC whiskers and Si3N4 matrix which enhances the crack deflection and whisker pull-out could contribute to the improvement of mechanical properties of the composites.

• Composites Research
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• 제25권5호
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• pp.141-146
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• 2012

본 논문에서는 Tsai-Wu 파손이론을 적용하여 Carbon/Epoxy 복합재 적층판으로 이루어진 자전거 휠의 경량화를 위한 적층수와 적층각에 대한 강도설계에 대하여 연구하였다. 복합재료는 적층수와 적층각에 따라 강도와 강성이 변하기 때문에 적용되는 설계 하중 조건에 따른 구조물의 최취약부에서 파손이 일어나지 않도록 최적의 적층각과 최소의 적층수를 찾아야한다. 따라서 유한요소해석을 이용하여 복합재 자전거 휠에 부가되는 수직, 복합하중조건에 대하여 가장 안정적인 적층수 및 적층각을 구하였다. 휠에 적용되는 적층각은 $[0]_{8n}$, $[90]_{8n}$, $[0/90]_{2ns}$, $[{\pm}45]_{2ns}$, $[0/{\pm}45/90]_{ns}$으로 적층수를 변화시켜가며 유한요소해석을 수행하였다. 해석 결과로부터 $[0/{\pm}45/90]_{3s}$의 적층각이 파손에 안정적인 적층각 임을 제안하였다. 또한 이를 통하여 휠의 최취약부를 알 수 있었다.

• 대한기계학회논문집
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• 제7권1호
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• pp.28-35
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• 1983

Quantitative analysis have been carried out on the micro-cracks on the surface and into the depth of unnotched smooth mild steel specimen under cyclic stains by rotating bending fatigue tests. Some of the results are; (1) Cracks initiate at the early stage of fatigue life N$_{I}$/ N$_{f}$=10 to 20%, and propagate during the rest of fatigue life. (2) Coalescence of highly crowded small fatigue cracks of random distribution seems to induce the final fracture at higher stress level. (3) The curves of crack initiation and the equal crack length on the graph of stress versus number of cycles are parallel to the S-N curve. (3) The curves of crack initiation and the equal crack length on the graph of stress versus number of cycles are parallel to the S-N curve. (4) The distributions of micro-surface crack length and depth show the composite Weibull distributions which are approximated to two straight lines separated by the value of transient region between stage I and stage II crack.k.k.

• Journal of Magnetics
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• 제11권4호
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• pp.164-166
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• 2006

We have investigated the dielectric and magnetic properties of ferroelectric-antiferromagnetic $BaTiO_{3}-LaMnO_{3}$ composite with changing relative mole percents. Due to high sintering temperature, i.e. $1150^{\circ}C$, the Ba ion in $BaTiO_{3}$ seems to diffuse into $LaMnO_{3}$; resulting in $BaTiO_{3}-(La,Ba)MnO_{3}$ ferroelectric-ferromagnetic composite. At room temperature, $0.9BaTiO_{3}-0.1LaMnO_{3}$ composite exhibits considerable magnetization (${\sim}0.7\;emu/g\;at\;2000\;Oe$) and low coercive field (${\sim}5\;Oe$). Also it exhibits high dielectric constant (${\sim}560$) and low loss (${\sim}0.08$) at 10 kHz. This result may imply that $BaTiO_{3}-LaMnO_{3}$ could be suitable for a low leakage multiferroic composite.

• 대한화학회지
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• 제62권4호
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• pp.269-274
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• 2018

금속산화물 고분자 복합재료전극 제조기법을 수소이온 감응성이 높은 $RuO_2$에 적용하여 표면연마가 가능한 나노 $RuO_2$ 복합재료 pH전극을 제조하였다. $RuO_2$ 함량 53 wt%을 가지는 나노 $RuO_2$ 복합재료 전극의 경우 나노 $IrO_2$ 복합재료 전극과 비슷한 수소이온 감응특성을 나타내었다. pH 1~9의 범위에서 이론치에 가까운 -58.7 mV/pH의 감응기울기, 1초 이하의 감응속도, 평균 $-57.0{\pm}0.3mV/pH$ (n=5)의 표면재생성, 장기 안정성 등 제반 특성과 전기화학적으로 활성이 높은 화학종에 의한 방해효과도 비슷하게 나타났다. 그러나 pH 10 이상의 염기성 용액에서의 감응기울기와 감응속도는 나노 $IrO_2$ 복합재료전극에 비하여 현저히 떨어지는 결과를 보였으며 이는 복합재료 매질 속의 금속산화물 함량에 따른 물리적 성질 차이에 따른 것으로 추측된다.

• Advances in concrete construction
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• 제9권4호
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• pp.387-395
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• 2020

This study has been carried out in two-phases to develop Fiber Reinforced Self-Compacting Concrete (FRSCC) performance. In the first phase, the composition of the quaternary composite binder compromised CEM I 42.5N (58-70%), Rice Husk Ash (25-37%), quartz sand (2.5-7.5%) and limestone crushing waste (2.5-7.5%) were optimized. And in the second phase, the effect of two fiber types (steel brass-plated and basalt) was investigated on the SCC optimized with the optimum CB as disperse reinforcement at 6 different ratios of 1, 1.2, 1.4, 1.6, 1.8, and 2.0% by weight of mix for each type. In this study, the theoretical principles of the synthesis of self-compacting dispersion-reinforced concrete have been developed which consists of optimizing structure-formation processes through the use of a mineral modifier, together with ground crushed cement in a vario-planetary mill to a specific surface area of 550 m2 / kg. The amorphous silica in the modifier composition intensifies the binding of calcium hydroxide formed during the hydration of C3S, helps reduce the basicity of the cement-composite, while reducing the growth of portlandite crystals. Limestone particles contribute to the formation of calcium hydrocarbonate and, together with fine ground quartz sand; act as microfiller, clogging the pores of the cement. Furthermore, the results revealed that the effect of fiber addition improves the mechanical properties of FRSCC. It was found that the steel fiber performed better than basalt fiber on tensile strength and modulus of elasticity; however, both fibers have the same performance on the first crack strength and sample destruction of FRSCC. It also illustrates that there will be an optimum percentage of fiber addition.

• Nuclear Engineering and Technology
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• 제55권5호
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• pp.1519-1526
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• 2023

For the first time Aluminium-BariumeZinc oxide nanocomposite (ZABONC) was synthesized by solution combustion method where calcination was carried out at low temperatures (600℃) to study the electromagnetic (EM) (X/γ) radiation shielding properties. Further for characterization purpose standard techniques like PXRD, SEM, UV-VISIBLE, FTIR were used to find phase purity, functional groups, surface morphology, and to do structural analysis and energy band gap determination. The PXRD pattern shows (hkl) planes corresponding to spinel cubic phase of ZnAl₂O4, cubic Ba(NO₃)₂, α and γ phase of Al₂O₃ which clearly confirms the formation of complex nano composite. From SEM histogram mean size of nano particles was calculated and is in the order of 17 nm. Wood and Tauc's relation direct energy band gap calculation gives energy gap of 2.9 eV. In addition, EM (X/γ) shielding properties were measured and compared with the theoretical ones using standard procedures (NaI (Tl) detector and multi channel analyzer MCA). For energy above 356 keV the measured shielding parameters agree well with the theory, while below this value slight deviation is observed, due to the influence of atomic/crystallite size of the ZABONC. Hence synthesized ZABONC can be used as a shielding material in EM (X/γ) radiation shielding.

• Journal of Periodontal and Implant Science
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• 제50권6호
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• pp.418-434
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• 2020

Purpose: The purpose of the present study was to evaluate the effect of silica-calcium phosphate composite (SCPC) granules on bone regeneration in extraction sockets. Methods: Ten patients were selected for a split-model study. In each patient, bone healing in SCPC-grafted and control ungrafted sockets was analyzed through clinical, radiographic, histomorphometric, and immunohistochemical assessments 6 months postoperatively. Results: A radiographic assessment using cone-beam computed tomography showed minimal ridge dimension changes in SCPC-grafted sockets, with 0.39 mm and 1.79 mm decreases in height and width, respectively. Core bone biopsy samples were obtained 6 months post-extraction during implant placement and analyzed. The average percent areas occupied by mature bone, woven bone, and remnant particles in the SCPC-grafted sockets were 41.3%±12%, 20.1%±9.5%, and 5.3%±4.4%, respectively. The percent areas of mature bone and woven bone formed in the control ungrafted sockets at the same time point were 31%±14% and 24.1%±9.4%, respectively. Histochemical and immunohistochemical analyses showed dense mineralized bundles of type I collagen with high osteopontin expression intensity in the grafted sockets. The newly formed bone was well vascularized, with numerous active osteoblasts, Haversian systems, and osteocytes indicating maturation. In contrast, the new bone in the control ungrafted sockets was immature, rich in type III collagen, and had a low osteocyte density. Conclusions: The resorption of SCPC granules in 6 months was coordinated with better new bone formation than was observed in untreated sockets. SCPC is a resorbable bone graft material that enhances bone formation and maturation through its stimulatory effect on bone cell function.

• 한국식품저장유통학회지
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• 제12권4호
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• pp.344-349
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• 2005

섬백리향의 항산화 기능성 성분에 대한 마이크로웨이브 추출특성을 확인하고자 microwave power($0{\sim}160\;W$)와 추출시간($1{\sim}5$분)을 독립변수($X_i$)로 하여 중심합성계획에 의해 10개구간의 추출조건을 설계하였다. 또한 추출물의 기능성분인 총 추출수율, 총 페놀 함량, 총 플라보노이드 함량 및 전자공여능을 종속변수($Y_n$)로 하여 반응표면분석을 실시하여 최적 추출조건을 예측하였다. 도출된 회귀식의 $R^2$는 총 페놀성분을 제외하고는 모두 0.93 이상을 나타내었으며, microwave power는 추출시간보다 영향이 큰 것으로 나타났다(p<0.05). 종속변수들의 최적 추출시간은 $3.36{\sim}4.97$분이었으나 microwave power는 넓은 분포를 보였으며, 기능성 성분들 모두를 추출하기 위한 추출조건 범위는microwave power $64{\sim}100\;W$, 추출시간 $2.9{\sim}4.0$분으로 나타났다.