• Title/Summary/Keyword: $MgB_4O_7$

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Creep Properties of Squeeze Infiltrated AS52 Mg/Al18B4O33w Composite (용탕가압침투 AS52 Mg/Al18B4O33w 복합재료의 크리프 특성)

  • Choi, Kye-Won;Park, Yong-Ha;Park, Bong-Gyu;Park, Yong-Ho;Park, Ik-Min;Cho, Kyung-Mox
    • Korean Journal of Metals and Materials
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    • v.46 no.7
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    • pp.412-419
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    • 2008
  • Creep behavior of the squeeze infiltrated AS52 Mg matrix composites reinforced with 15 vol% of aluminum borate whiskers($Al_{18}B_4O_{33}w$) fabricated squeeze infiltration method was investigated. Microstructure of the composites was observed as uniformly distributed reinforcement in the matrix without any particular defects of casting pores etc.. Creep test was carried out at the temperature of 150 and $200^{\circ}C$ under the applied stress range of 60~120 MPa. The creep resistance of the composite was significantly improved comparing with the unreinforced AS52 Mg alloy. The creep behavior of composites might be interpreted with the substructure invariant model successfully for the composite. Threshold stress of the composite exist for the creep deformation of the composite. The analysis of the creep behavior of the composite with threshold stress indicated that creep deformation was controlled by the lattice diffusion process of AS52 Mg matrix at given effective stresses and temperatures. Activation energy was also calculated to check lattice diffusion controlled creep behavior of the composite.

A Study on the Amount and Major Compositions of Excreta from Broilers (육계의 분뇨 배설량 및 분뇨 성분 조사 결과)

  • HwangBo, J.;Hong, E.C.;Chung, I.B.;Kang, K.H.;Park, H.D.;Suh, O.S.;Chung, W.T.;Jang, S.K.
    • Korean Journal of Poultry Science
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    • v.36 no.2
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    • pp.157-163
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    • 2009
  • This work was conducted to investigate the amount and major compositions of excreta from broilers. One hundred fifty 1-d-old male and female Ross broilers were used in this work and ten broilers were selected to measure excreta. Average amount of excreta per broiler was 85.4 g, and average moisture content was 76.9%. N, $P_2O_5$ and $K_2O$ in excreta were 1.19, 0.29 and 0.49%, respectively. pH, $BOD_5$, $COD_{mn}$, and SS were 7.80, 42,134 mg/L, 52,668 mg/L, and 106,669 mg/L, respectively. Pb in poultry excreta was 0.803 mg/kg and highly lowed compared with the standard contents (150 mg/kg). Cd was not founded in excreta. Hg was founded in excreta as 0.002 mg/kg, but it was low compared with the standard level (2 mg/kg).

Production of Cathepsin B Inhibitor by Steptomyces luteogriseus KT-10 (Streptomyces luteogriseus KT-10에 의한 Cathepsin B 저해물질의 발효생산)

  • 한길환;김상달
    • Microbiology and Biotechnology Letters
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    • v.27 no.6
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    • pp.458-465
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    • 1999
  • Streptomyces luteogriseus KT-10 isolated from Korean farm soil produced a strong cathepsin B inhibitor. Optimal conditions for the cathepsin B inhibitor production by s. luteogriseus KT-10 were evaluated. The cathepsin B inhibitor was produced with maximal yield in the cultural condition of pH 7.0 and $25^{\circ}C$ for 4 days. Optimal medium for the cathepsin B inhibitor production was determined to be a medium containing 20g, peptone 3g, yeast extract 1g, K2HPO4 0.5g, MgSO4.7H2O 0.5g, NaNO3 0.5g, NaCl 0.5g per l. The cathepsin B inhibitor produced by S. luteogriseus KT-10 could also inhibit the other proteinases such as trypsin, papain, and cathepsin D.

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The Simultaneous Determination of Chemical Ingredients in Silica Minerals by X-ray Fluorescence Spectrometry using Matrix Correction Method (매트릭스 보정법을 이용한 규산질 광물 중 화학성분의 X-선 형광분광법 분석)

  • Kim, Yeong Man;Choe, Beom Seok;Lee, Gyeong Mi;Kim, Seon Tae;Lee, Jong Uk
    • Journal of the Korean Chemical Society
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    • v.34 no.1
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    • pp.63-68
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    • 1990
  • The chemical ingredients such as $SiO_2,\;Al_2O_3,\;MgO,\;Fe_2O_3,\;CaO$ and $TiO_2$in silica minerals were determined by X-ray fluorescence spectrometry using a matrix correction method. The synthesized standards mixed with reagent grade oxides and the sample were diluted by fusing with 16 times $Li_2B_4O_7$. The matrix effects correlated among the ingredients were corrected by the empirical coefficient method based on the Lucas-Tooth and Pyne model. The analytical results showed relatively good agreement between the different sets of coefficients but were improved with increasing the number of standard. The accuracy of this method was also examined with the standard reference material of NIST.

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Decolorization of Azo Dyes by Aspergillus sojae B-10

  • Ryu, Beung-Ho
    • Journal of Microbiology and Biotechnology
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    • v.2 no.3
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    • pp.215-219
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    • 1992
  • Biodegradation of azo dyes such as Amaranth, Sudan III and Congo-Red by Aspergillus sojae B-10 was demonstrated using Aspergillus sojae B-10. Aspergillus sojae B-10 showed the greatest decolorization ability when it was cultivated in a nitrogen-limited medium containing, azo dyes(10 mg/l), 2.0% glucose, 0.06% sodium nitrate, 0.1% $KH_PO_4$, 0.5% MgSO_4$$7H_2O$ at pH 5.0 and $37^\circ{C}$ for 5 days. Under optimal conditions, Amaranth started being decolorized within 24 hr and was almost complete after decolorization of 4 days incubation. Sudan III was completely decolorized after a cultivation of 5 days. However, Congo-Red was not completely decolorized until 5 days of cultivation.

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Optimization of Medium Composition for Lipopeptide Production from Bacillus subtilis N7 using Response Surface Methodology

  • Luo, Yi;Zhang, Guoyi;Zhu, Zhen;Wang, Xiaohui;Ran, Wei;Shen, Qirong
    • Microbiology and Biotechnology Letters
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    • v.41 no.1
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    • pp.52-59
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    • 2013
  • The nutritional requirements for the maximum production of lipopeptides by Bacillus subtilis N7 (B. subtilis N7) were investigated and optimized using response surface methodology (RSM) under shake flask fermentation. A one-factor-at-a-time experimental setup was used to screen carbon and nitrogen sources. A Plackett-Burman design (PBD) was employed to screen the most critical variables for lipopeptides production amongst ten nutritional elements. The central composite experimental design (CCD) was finally adopted to elucidate the composition of the fermentation medium. Statistical analyses (analysis of variance, ANOVA) of the results showed that KCl, $MnSO_4$ and $FeSO_4{\cdot}6H_2O$ were important components and that their interactions were strong. Lipopeptide production was predicted to reach 709.87 mg/L after a 60 h incubation using an optimum fermentation medium composed of glucose 7.5 g/L, peanut oil 1.25 g/L, $MgSO_4$ 0.37 g/L, $KH_2PO_4$ 0.75 g/L, monosodium glutamate 6.75 g/L, yeast extract and $NH_4Cl$ (5:3 w/w) 10 g/L, KCl 0.16 g/L, $FeSO_4{\cdot}6H_2O$ 0.24 mg/L, $MnSO_4$ 0.76 mg/L, and an initial pH of 7.0. Lipopeptide production ($706.57{\pm}3.70$ mg/L) in the optimized medium confirmed the validity of the predicted model.

Screening and Optimal Culture Conditions of Antibiotic-Producing Actinomycetes B-51 for Multidrug Resistant Acinetobacter baumannii (다제내성 Acinetobacter baumannii에 유효한 방선균 B-51의 탐색 및 이 균주가 생산하는 항생물질 발효 최적 배양 조건)

  • Rhee, Moon-Soo;Kim, Gwan-Pil;Bang, Byung-Ho
    • The Korean Journal of Food And Nutrition
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    • v.23 no.1
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    • pp.63-69
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    • 2010
  • With the increase of the use of antibiotics and invasive procedures, infections caused by multidrug-resistant Acinetobacter baumannii(MRAB) are increasing. We screened the antibiotic producing strain B-51 for antibacterial activity against MRAB from the soils and studied the effects of culture medium on the antibiotic production of B-51. The medium conditions for maximum antibiotic productivity of B-51 was 2% glycerol, 0.5% soybean meal, 0.01% $CaCl_2$, 0.01% $MgSO_4{\cdot}7H_2O$ and 0.01% $KH_2PO_4$ at an initial pH of 6.0, at $30^{\circ}C$ for 76 h.

Examination of the Production of Extracellular $\alpha$-Amylase by Bacillus thuringiensis, 19 serotypes (Bacillus thuringiensis, 19 혈청형의 세포외 $\alpha$-Amylase 생산 검색)

  • 이건주;박동왕;이형환;이영주
    • Microbiology and Biotechnology Letters
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    • v.16 no.5
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    • pp.348-351
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    • 1988
  • The production of extracellular $\alpha$-amylase by Bacillus thuringiensis 19 serotypes was examined by the hydrolysis test of starch. Thirteen serotypes produced the amylase. B. thuringiensis serovar thuringiensis alesti, kurstaki, sotto, kenya, israelensis, morrisoni, entomocidus, tolworthi, thompsoni, toumanoffi, pakistani, and indiana produced tee enzyme. The amylase produced by B. thuringiensis serovar israelensis showed highest activity around pH 6.7 to 7.2 and 55$^{\circ}C$ to $65^{\circ}C$. The high production medium of the amylase was composed of 1% bactopeptone, 0.3% beef-extract, 0.3% yeast ex-tract, 0.5% NaCl, 0.3% $K_2$HPO$_4$, 0.1% KH$_2$PO$_4$, 0.2% Soluble Starch, 0.012% CaCl$_2$.2$H_2O$$_2$, 0.005% MnCl$_2$, and 0.03% MgCl$_2$.7$H_2O$. The highest production of the enzyme was observed at 4 hours culture in the soluble starch (0.6 units/$m\ell$) or glucose (0.43 units/$m\ell$) substrate.

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Characteristics of Fumarate Reductase from Enterococcus faecalis RKY1 (Enterococcus faecalis RKY1 이 생산하는 Fumarate Reductase의 특성)

  • 박미란;김도만;류화원;이진하
    • KSBB Journal
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    • v.15 no.3
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    • pp.318-322
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    • 2000
  • An oxygen-sensitive fumarate reductase has been purified from the cytosol fraction of the Enterococcus faecalis RKY1 grown anaerobically on a defined medium containing glycerol and fumarate. A major portion of the purification was performed with employing Triton X-100 and reducing agents by Phenyl-sepharose CL-4B DEAE-sepharose and Dephadex G-150 The final activity was 0.42 unit/mg. The deduced molecular mass of active band was 66 kDa. The optimal pH and temperature for the activity were 7.0 and 38$^{\circ}C$ respectively. The enzyme activity was not affected by 1mM metal ions such as bacl2 $.$2H2O HgCl2 MnCl2$.$4H2O ZnCl2 CuCl2$.$2H2O Mgcl2$.$6H2O FeSo4$.$7H2O and by EDTA. Partially purified enzyme ws yellow in color ; spectroscopic study indicated the presence of flavins as a cofactor.

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플라즈마 보조 전자빔 정련을 이용한 Si내의 불순물 제거

  • Kim, Tae-Hak;Choe, Ji-Seong;Ju, Jeong-Hun
    • Proceedings of the Korean Vacuum Society Conference
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    • 2011.02a
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    • pp.286-286
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    • 2011
  • 현재의 NEDO (New Energy and industrial technology Development Organization) style Si 정련은 두 단계로 구분되어 있다. 고출력 집속 전자빔을 이용한 금속 실리콘의 1차 용융과 대기압 근처의 플라즈마 아크 용해를 이용해서 B, P를 약간의 반응성 가스를 첨가 하여 제거하는 방법이다. 그러나 저가형 실리콘을 생산하려는 취지와 달리 두 가지의 고가 장비가 필요하다. E-beam melting 장치에서도 반응성이 높은 라디칼을 생성할 수 있다면 하나의 장비에서 두 가지의 정련 작업을 진행시킬 수 있다. 본 연구에서는 고진공에서(< 10-4 Torr) 동작하는 E-beam의 성능에 전혀 영향을 주지 않으면서 플라즈마를 용이하게 생성 시킬 수 있는 방법을 개발하고 이를 적용하여 실제 금속 순도 실리콘 내에 존재하는 B, P가 제거되는지 확인하는 것을 연구 내용으로 한다. 본 연구는 MG (Metal Grade) - Si 을 플라즈마 보조 전자빔 정련을 이용하여 정련한 Si 의 불순물 함량의 개선 효과를 조사하는 것이다. MG-Si 의 정련 방법 중에서 고출력 집속 전자빔을 이용하여 휘발성 오염물질을 제거 후, 플라즈마 아크 용해를 이용해서 B 를 제거하는 방법을 접목시켰다. MG-Si 에 DC power 와 전자빔을 집속시켜서 정련을 하면 챔버 내의 잔류 수증기가 플라즈마에 의해 분해되어 O를 생성하고, B와 반응을 하여 BO 형태로 제거가 된다. 방전 전압 700 V 와 전자빔 가속 전압이 4.5 kV, 방출 전류는 11 A, 진공 챔버 내의 압력은 $7.2{\times}10^{-4}$ Torr에서 정련을 진행하여 B를 제거했다.

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