• 제목/요약/키워드: $^{63}Ni$

검색결과 238건 처리시간 0.031초

고온자전합성법으로 제조된 다공성 TiNi 생체재료의 기공구조 및 기계적 특성 (Pore Structure and Mechanic:11 Property of Porous TiNi Biomaterial Produced by Self-Propagating High-Temperature Synthesis)

  • 김지순;강지훈;양석균;정순호;권영순
    • 한국분말재료학회지
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    • 제10권1호
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    • pp.34-39
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    • 2003
  • Porous TiNi bodies were produced by Self-propagating High-temperature Synthesis (SHS) method from a powder mixture of Ti and Ni. Porosity, pore size and structure, mechanical property, and transformation temperature of TiNi product were investigated. The average porosity and pore size of produced porous TiNi body are 63% and $216\mutextrm{m}$, respectively. XRD analysis showed that the major phase of produced TiNi body is B2 phase. Its average fracture strength and elastic modulus measured under dry condition were $22\pm2$ MPa and $0.18\pm0.01$GPa, respectively. It could be strained up to 7.3 %. The transformation temperatures determined by DSC showed the $M_s$ temperature of $67^{\circ}C$ and $A_f$ temperature of $99^{\circ}C$.

뉴칼레도니아 니켈 라테라이트 광석 내 가니어라이트의 광물학적 특징 (Mineralogy of Garnierite from New Caledonian Ni Lateritic Ore)

  • 조현구;김순오;김상배
    • 한국광물학회지
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    • 제24권4호
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    • pp.253-263
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    • 2011
  • 뉴칼레도니아 Nakety, Kouaoua, Ouaco 니켈 라테라이트 광상에서 수입하는 가니어라이트 광석의 광물학적 특성을 광학현미경 관찰, X-선 회절 분석과 전자현미분석에 의하여 연구하였다. 녹색 가니어라이트 광석은 교질상, 세포상, boxwork 조직 등 지표 부근의 저온에서 침전에 의한 조직을 잘 나타낸다. 이 광석의 니켈 광석광물은 대부분 니켈 함유 활석~윌렘사이트 계열 광물이며, 일부 리자다이트가 포함되어 있다. 니켈 함유 활석~윌렘사이트 계열 광물 내 NiO의 함량은 Ouaco (평균 40.63%), Nakety (평균 28.58%), Kouaoua (평균 24.90%) 순이며, Mg를 치환하는 Ni 백분율은 43.5~85.0%이다. 암갈색 가니어라이트 광석은 세포상이나 boxwork 조직을 가지며, 주 니켈 광석광물은 리자다이트~니켈 리자다이트 계열 광물에 일부 니켈 함유 활석~윌렘사이트 계열 광물로 구성된다. 리자다이트~니켈 리자다이트 계열 광물 내 NiO의 함량은 1.14~4.06 wt. %이며, Ni/(Mg+Ni) 백분율은 1.7~6.8%인데, 니켈의 함량이 낮은 이유는 팔면체 자리에서 Mg를 치환하는 Fe의 함량이 많은 것에 기인한다.

Alloy 600에 전기 도금한 Ni-P-Fe 및 Ni-P-B 층의 열적 안정성 연구 (Study on Thermal Stability of Ni-P-Fe and Ni-P-B Layers Electroplated on Alloy 600)

  • 김명진;김정수;김동진;김홍표
    • 한국표면공학회지
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    • 제43권2호
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    • pp.57-63
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    • 2010
  • In this study, thermal stability of the mechanical properties of Ni-P-B and Ni-P-Fe layers electroplated on Alloy 600 material was evaluated by measuring their microhardness, tensile strength, and elongation after heat treatment at $325^{\circ}C$ and $400^{\circ}C$. According to the results, there was no noticeable change in microhardness of the two electrodeposits before and after heat treatment at the temperatures for 30 days. In the case of a Ni-P-B electrodeposit, ultimate tensile strength (UTS) slightly increases with heat treatment time, while its elongation decreases, showing good thermal stability in the mechanical properties at high temperature. On the other hand, UTS and elongation of Ni-P-Fe decrease with heat treatment time, which is very unusual observation. This result was attributed to the bad microstructure of Ni-P-Fe having many defects in the deposit formed early stage of an electroplating process and their redistribution to link to become large ones during heat treatment.

제주도 토양 중 중금속의 화학적 형태 (Chemical Speciation of Heavy Metals in Soils of Jeju Island, Korea)

  • 현성수;김세라;이민규;감상규
    • 한국환경과학회지
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    • 제26권7호
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    • pp.847-858
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    • 2017
  • For 26 soil series distributed more than 1% among 63 soil series in Jeju Island, natural uncultivated soil samples were collected. For these soils, the chemical speciation of eight heavy metals (Cd, Cr, Cu, Mn, Ni, Pb, V, and Zn) was examined. Further, the Plant Bioavailability (PB) and Mobility Factor (MF) of these heavy metals were evaluated using Tessier's 5-step sequential extraction method (exchangeable, carbonate, reducible (bound to Fe/Mn oxides), oxidizable (bound to organic matter), and residual fraction). The main form present was residual fraction for Cd and Zn; residual and oxidizable fractions for Cr, Cu, Ni, and Pb; reducible fraction for Mn; and carbonate fraction for V. The average plant availability and average mobility factor were found to be V (57.37%) > Zn (12.49%) > Cd (11.76%) > Cu (11.19%) > Pb (9.37%) > Cr (9.09%) > Mn (3.13%) > Ni (2.63%), and Mn (61.04%) > V (59.94%) > Zn (31.54%) > Cd (17.65%) > Cr (15.66%) > Ni (13.89%) > Pb (13.80%) > Cu (13.53%), respectively.

수증기-메탄개질용 Ni 촉매의 유용도에 관한 수치적 연구 (A Numerical Study on the Effectiveness Factor of Ni Catalyst Pellets for Steam-Methane Reforming)

  • 최종균;남진현;신동훈;정태용;김영규
    • 한국신재생에너지학회:학술대회논문집
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    • 한국신재생에너지학회 2007년도 추계학술대회 논문집
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    • pp.63-66
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    • 2007
  • Reformers which produce hydrogen from natural gas are essential for the operation of residential PEM fuel cells. For this purpose, steam-methane reforming reactions with Ni catalysts is primarily utilized. Commercial Ni catalysts are generally made to have porous pellet shapes in which Ni catalyst particles are uniformly dispersed over Alumina support structures. This study numerically investigates the reduction of catalyst effectiveness due to the mass transport resistances posed by porous structures of spherical catalyst pellets. The multi-component diffusion through porous media and the accurate kinetics of reforming reaction is fully considered in the numerical model. The preliminary results on the variation of the effectiveness factor according to different operation conditions are presented, which is planned to be used to develop correlations in future studies.

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Ni-Fe 및 Fe 정밀 전주성형에 관한 연구 (Electroforming of Nickel-iron alloy and Iron)

  • 이흥렬;박재영;김균탁;김호형;황태진
    • 한국표면공학회:학술대회논문집
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    • 한국표면공학회 2011년도 춘계학술대회 및 Fine pattern PCB 표면 처리 기술 워크샵
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    • pp.63-64
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    • 2011
  • 니켈 알러지를 일으키지 않는 전주 부품 개발을 위해 Ni을 대체할 수 있는 전주 소재로 Ni-Fe 합금과 Fe에 대한 전주 공정을 개발하였다. Ni-Fe 합금 전주의 경우 전주품의 표면 내식성 강화를 위해 Cr 나노입자를 이용한 복합전주를 실시하여, Ni 전주품과 내부식성, 니켈 용출 비교 분석 실험을 하였다. 또한 Ni을 완전히 배제하기 위해 새로운 시도로서 순 Fe 전주 공정 기술을 개발하였다. 제조된 Fe 전주품의 내식성 향상을 위한 실리카 코팅 등의 표면처리에 대한 효과도 분석하였다.

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