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http://dx.doi.org/10.13103/JFHS.2022.37.3.129

Development of Rapid Analytical Method for Heavy Metals (Cd, Pb) in Meju using fs LA-ICP-MS  

Shin, Hee-Chang (Division of Safety Analysis, Experiment&Research Institute, National Agricultural Products Quality Management Service)
Choi, Ji-Hye (Division of Safety Analysis, Experiment&Research Institute, National Agricultural Products Quality Management Service)
Kim, Yong-Kyoung (Division of Safety Analysis, Experiment&Research Institute, National Agricultural Products Quality Management Service)
Kim, Dae-Jung (Division of Safety Analysis, Experiment&Research Institute, National Agricultural Products Quality Management Service)
An, Jae-Min (Division of Safety Analysis, Experiment&Research Institute, National Agricultural Products Quality Management Service)
Kim, Sung-Youn (Division of Safety Analysis, Experiment&Research Institute, National Agricultural Products Quality Management Service)
Publication Information
Journal of Food Hygiene and Safety / v.37, no.3, 2022 , pp. 129-135 More about this Journal
Abstract
The official analytical method for the analysis of harmful heavy metals in Meju, distributed in Korea, employs a strong acid to decompose the organic components. This analysis is time consuming and harmful to the users and/or the environment. This study aimed to develop a new pre-treatment technology using laser ablation, to rapidly analyze harmful heavy metals without using strong acids. The results obtained from this method were validated by the National Institute of Food and Drug Safety Evaluation guideline (NIFDS, 2016). Moreover, a comparison of the two methods showed that the analytical time for 55 Meju samples was shortened by 96% or more in the new method. The results showed no significant difference in the recovery ranging from 90-120%. The proposed method proved suitable for detecting harmful heavy metals in Meju.
Keywords
fs LA-ICP-MS; ICP-MS; Heavy metal; Meju; Rapid analytical method;
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Times Cited By KSCI : 5  (Citation Analysis)
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