Development of Analytical Method for Kasugamycin in Agricultural Products using LC-MS/MS |
Lee, Han Sol
(Pesticide and Veterinary Drug Residues Division, Food Safety Evaluation Department, National Institute of Food and Drug Safety Evaluation, Ministry of Food and Drug Safety)
Do, Jung-Ah (Pesticide and Veterinary Drug Residues Division, Food Safety Evaluation Department, National Institute of Food and Drug Safety Evaluation, Ministry of Food and Drug Safety) Park, Ji-Su (Pesticide and Veterinary Drug Residues Division, Food Safety Evaluation Department, National Institute of Food and Drug Safety Evaluation, Ministry of Food and Drug Safety) Cho, Sung Min (Pesticide and Veterinary Drug Residues Division, Food Safety Evaluation Department, National Institute of Food and Drug Safety Evaluation, Ministry of Food and Drug Safety) Shin, Hye-Sun (Pesticide and Veterinary Drug Residues Division, Food Safety Evaluation Department, National Institute of Food and Drug Safety Evaluation, Ministry of Food and Drug Safety) Jang, Dong Eun (Pesticide and Veterinary Drug Residues Division, Food Safety Evaluation Department, National Institute of Food and Drug Safety Evaluation, Ministry of Food and Drug Safety) Jung, Yong-hyun (Pesticide and Veterinary Drug Residues Division, Food Safety Evaluation Department, National Institute of Food and Drug Safety Evaluation, Ministry of Food and Drug Safety) Lee, Kangbong (Pesticide and Veterinary Drug Residues Division, Food Safety Evaluation Department, National Institute of Food and Drug Safety Evaluation, Ministry of Food and Drug Safety) |
1 | Umezawa, H., Okami, Y., Hashimoto, T., Suhara, Y., Hamada, M., Takeuchi, T.: A new antibiotic kasugamycin. J. Antibiot. Ser. A, 18, 101-104 (1965). |
2 | Wikipedia, Kasugamycin. Available at https://en.wikipedia.org/wiki/Kasugamycin (2019) (Accessed 18 April 2019). |
3 | Alechaga, E., Moyano, E., Galceran, M.T.: Simultaneous analysis of kasugamycin and streptomycin in vegetables by liquid chromatography-tandem mass spectrometry. Anal. Methods, 7, 3600-3607 (2015). DOI |
4 | The Japan Food Chemical Research Foundation, Maximum Residue Limits (MRLs) List of Agricultural Chemicals in Foods. Available at https://db.ffcr.or.jp/front/pesticide_detail?id=15600 (2019) (Accessed 18 April 2019). |
5 | Rural Development Administration (RDA), Pesticide registration status. Available at http://www.nongsaro.go.kr/portal/ps/psa/psab/psaba/openApiAgchmRegistInfoLst.ps?sAgPrdlstNm=%EA%B0%80%EC%8A%A4%EA%B0%80%EB%A7%88%EC%9D%B4%EC%8B%A0&sAgPrpos=&sAg-BrandNm=&sAgCropsYn1=Y&sAgCropsNm1=&sAgCropsYn2=Y&sAgCropsNm2=&sAgDbyhsYn=Y&sAgApplcDbyhs=&menuId=PS00116&pageIndex=1&pestiCode=&diseaseUseSeq=&sDcsnAt=Y (2019) (Accessed 18 April 2019). |
6 | Pubchem, Kasugamycin. Available at https://pubchem.ncbi.nlm.nih.gov/compound/kasugamycin#section=Top (2019) (Accessed 18 April 2019). |
7 | United States Environmental Protection Agency (US EPA), Regulation of Pesticide Residues on Food. Available at https://www.ecfr.gov/cgi-bin/text-idx?SID=40ea4c2379e88c6bb1c09d58b46d0099&mc=true&node=se40.26.180_1614&rgn=div8 (2019) (Accessed 18 April 2019). |
8 | Health Canada, Maximum Residue Limits for Pesticides. Available at http://pr-rp.hc-sc.gc.ca/mrl-lrm/results-eng.php (2019) (Accessed 18 April 2019). |
9 | Government of Canada, Residue definitions for chemicals with maximum residue limits regulated under the pest control products act. Available at https://www.canada.ca/en/health-canada/services/consumer-product-safety/pesticides-pest-management/public/protecting-your-health-environment/pesticides-food/residue-definitions-chemicals-maximum-residue-limits-regulated-under-pest-control-products-act.html (2019) (Accessed 18 April 2019). |
10 | Ministry of Food and Drug Safety (MFDS), Pesticide information. Available at https://www.foodsafetykorea.go.kr/residue/prd/info/list.do?currentPageNo=1&searchCode=&menuKey=1&subMenuKey=9&subChildMenuKey=&searchConsonantFlag=&searchFlag=prd&searchValue2=&searchConsonantFlag2=&excelSave=&excelSaveInput=&etcFlag=&searchValue=kasugamycin (2019) (Accessed 18 April 2019). |
11 | CODEX Alimentarius Commission, Guidelines on good laboratory practice in residue analysis. CAC/GL 40-1993 (2003). |
12 | Ministry of Food and Drug Safety (MFDS), Korea food code. pp. 1377-1382 (2018). |
13 | Wang, C., Li, H., Wang, N., Li, H., Fang, L., Dong, Z., Du, H., Guan, S., Zhu, Q., Chen, Z., Yang, G.: Simultaneous analysis of kasugamycin and validamycin-A in fruits and vegetables using liquid chromatography-tandem mass spectrometry and consecutive solid-phase extraction. Anal. Methods, 9, 634-642 (2017). DOI |
14 | Zhang, H., Wang, C., Li, H., Nie, Y., Fang, L., Chen, Z.:Simultaneous determination of kasugamycin and validamycin-A residues in cereals by consecutive solid-phase extraction combined with liquid chromatography-tandem mass spectrometry. Food Addit. Contam. Part A, 35, 487-497 (2018). DOI |
15 | Ministry of Food and Drug Safety (MFDS), Guidelines on standard procedures for preparing analysis method (2016). |
16 | Kang, Y. W., Joo, H. J., Kim, Y. S., Cho, Y. J., Kim, H. Y., Lee, G. H., Kim, M. H.: Analysis and monitoring of residues of aminoglycoside antibiotics in livestock products. Korean J. Food Sci. Technol., 43, 1-5 (2011). DOI |
17 | Ministry of Food and Drug Safety (MFDS), Pesticide analytical residues manual in food code. pp. 13-14 (2013). |
18 | Chemicalize, kasugamycin. Available at https://chemicalize.com/#/calculation (2019) (Accessed 19 June 2019). |
19 | Houda, B., Juan, C. M., Jordi, M., Guillermina, F.: Determination of aminoglycoside and macrolide antibiotics in meat by pressurized liquid extraction and LC-ESI-MS. J. Sep. Sci., 33, 1-8 (2010). DOI |